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inquiry11-Mercapto-1-undecanol CAS:73768-94-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry11-mercapto-1-undecanolAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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11-mercapto-1-undecanol
Conditions | Yield |
---|---|
With sodium hydroxide Yield given; |
thioacetic acid S-(11-hydroxy-undecyl) ester
A
11-mercapto-1-undecanol
B
11-hydroxyundecyldisulfide
Conditions | Yield |
---|---|
With sodium methylate Yield given; |
1-Bromo-11-hydroxyundecane
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Na / methanol / 6 h / Heating 2: CH3ONa View Scheme | |
Multi-step reaction with 2 steps 1: ethanol 2: 10percent aq. NaOH View Scheme | |
Stage #1: 1-Bromo-11-hydroxyundecane With thiourea In dimethyl sulfoxide at 20℃; for 21h; Stage #2: With potassium hydroxide In water; dimethyl sulfoxide at 80℃; for 0.0833333h; | 7.2 g |
Stage #1: 1-Bromo-11-hydroxyundecane With thiourea In ethanol Heating; Inert atmosphere; Stage #2: With sodium hydroxide In water Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium hydroxide; Hg In ethanol; water |
11-mercapto-1-undecanol
11-hydroxyundecyldisulfide
Conditions | Yield |
---|---|
With iodine In ethanol for 1h; Ambient temperature; | 100% |
With iodine In dichloromethane | 100% |
With N-chloro-succinimide In dichloromethane for 0.166667h; Inert atmosphere; | 98% |
1-[(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)disulfanyl]dodecane
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 0.25h; | 99% |
1-[(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)trisulfanyl]dodecane
11-mercapto-1-undecanol
11-(dodec-1-yl-trisulfanyl)undecan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 0.25h; air; | 99% |
(5,5-dimethyl-2-thiono-1,3,2-dioxophosphorinanyl) sulfenyl bromide
11-mercapto-1-undecanol
11-[(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)di-sulfanyl]undecan-1-ol
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; | 95% |
In dichloromethane at -30 - 20℃; for 0.5h; Inert atmosphere; | 4.42 g |
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; | 4.42 g |
bis-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yl)disulfide
11-mercapto-1-undecanol
11-[(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)di-sulfanyl]undecan-1-ol
Conditions | Yield |
---|---|
Stage #1: bis-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yl)disulfide With bromine In dichloromethane at -30℃; for 0.25h; Inert atmosphere; Stage #2: 11-mercapto-1-undecanol In dichloromethane at 20℃; for 0.5h; | 95% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 0℃; for 0.0833333h; Solvent; | 89% |
Stage #1: bis-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinan-2-yl)disulfide With bromine Stage #2: 11-mercapto-1-undecanol |
11-mercapto-1-undecanol
1-(4'-methoxyphenyl)-2-<4'-(benzyloxy)phenyl>ethanol
Conditions | Yield |
---|---|
With zinc(II) iodide In 1,2-dichloro-ethane for 1.5h; Ambient temperature; | 93% |
5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane
11-mercapto-1-undecanol
11-[(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)di-sulfanyl]undecan-1-ol
Conditions | Yield |
---|---|
Stage #1: 5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane With bromine In dichloromethane at -30℃; for 0.25h; Inert atmosphere; Stage #2: 11-mercapto-1-undecanol In dichloromethane at 20℃; for 0.5h; | 93% |
Stage #1: 5,5-dimethyl-2-thiolo-2-thiono-1,3,2-dioxaphosphorinane With bromine Stage #2: 11-mercapto-1-undecanol |
dichloromethane
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
With triethylamine at 30℃; for 24h; Inert atmosphere; | 67% |
With triethylamine; RhCl(PPh3)3 at 20℃; for 24h; | 63% |
ethanol
chloranil
11-mercapto-1-undecanol
A
2,3,6-tris((11-undecanol)sulphanyl)-5-ethoxy-1,4-benzoquinone
B
2,3,5,6-tetrakis((11-undecanol)sulphanyl)-1,4-benzoquinone
Conditions | Yield |
---|---|
With sodium carbonate for 24h; | A 27% B 63% |
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 20℃; for 24h; | 57% |
2,3-Dichloro-1,4-naphthoquinone
ethanol
11-mercapto-1-undecanol
A
2-((11-undecanol)sulphanyl)-3-ethoxy-1,4-naphthoquinone
B
2,3-bis((11-undecanol)sulphanyl)-1,4-naphthoquinone
Conditions | Yield |
---|---|
With sodium carbonate for 24h; | A 34% B 53% |
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
Stage #1: 11-mercapto-1-undecanol With sulfur trioxide-N,N-dimethylformamide complex In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Stage #2: With sodium hydroxide In ethanol Inert atmosphere; | 53% |
11-mercapto-1-undecanol
1,2-bis<4'-(tetrahydro-2''H-pyran-2''-yloxy)phenyl>ethanol
Conditions | Yield |
---|---|
With zinc(II) iodide In 1,2-dichloro-ethane for 4h; Ambient temperature; | A 11% B 52% |
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 20℃; for 24h; | 51% |
5-bromovaleric acid methyl ester
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
48% |
11-mercapto-1-undecanol
1-(4'-methoxyphenyl)-2-<4'-(tetrahydro-2''H-pyran-2''-yloxy)phenyl>ethanol
Conditions | Yield |
---|---|
With zinc(II) iodide In 1,2-dichloro-ethane for 1.5h; Ambient temperature; | A 40% B 46% |
poly(methacrylic acid)
11-mercapto-1-undecanol
11-mercaptoundecyl methacrylate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate In dichloromethane at 20℃; for 24h; Inert atmosphere; | 45% |
With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate In dichloromethane at 20℃; for 24h; Inert atmosphere; | 45% |
5,5',6,6'-tetraphenyl-bis(1,2,4-triazine)-3,3'-disulfide
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane for 1h; | 23% |
11-mercapto-1-undecanol
A
[Os3(CO)10(μ-H)(μ-O(CH2)11SH)]
B
[Os3(CO)10(μ-H)(μ-S(CH2)11OH)]
C
[Os3(CO)10(μ-H)(μ,μ-O(CH2)11S)Os3(CO)10(μ-H)]
Conditions | Yield |
---|---|
With HBF4 In diethyl ether; toluene (Ar or N2); using Schlenk techniques; addn. of excess of HS(CH2)11OH andHBF4/ether (one drop) to soln. of Os3(CO)10(μ-H)(μ-OH) in toluene ; reflux for 5 h; removal of solvent in vac., chromy. using hexane/CH2Cl2 as eluent; elem.anal.; | A 8% B 10% C 1% |
menadione
11-mercapto-1-undecanol
Conditions | Yield |
---|---|
In methanol; isopropyl alcohol at 20℃; for 24h; | 8% |
11-mercapto-1-undecanol
trifluoroacetic anhydride
11-mercaptoundecyl trifluoroacetate
Conditions | Yield |
---|---|
In hexane for 0.00833333h; |
11-mercapto-1-undecanol
1,10-iododecanethiol
11-(10-Iodo-decyldisulfanyl)-undecan-1-ol
Conditions | Yield |
---|---|
With iodine In ethanol |
11-mercapto-1-undecanol
12-Iodo-dodecane-1-thiol
11-(12-Iodo-dodecyldisulfanyl)-undecan-1-ol
Conditions | Yield |
---|---|
With iodine In ethanol |
11-mercapto-1-undecanol
9-(2-carboxyethyl)adenine p-nitrophenyl ester
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane; N,N-dimethyl-formamide at 25℃; for 48h; Substitution; oxidation; Title compound not separated from byproducts.; |
11-mercapto-1-undecanol
α-bromopropionyl bromide
methacrylic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: 11-mercapto-1-undecanol With Si and Au implanted silicon for 24h; Solid phase reaction; Stage #2: α-bromopropionyl bromide With triethylamine Condensation; solid phase reaction; Stage #3: methacrylic acid methyl ester Polymerization; solid phase reaction; Further stages.; |
11-mercapto-1-undecanol
α-bromopropionyl bromide
acrylic acid methyl ester
poly(methyl acrylate), prepared by three-stage surface-initiated atom transfer radical polymerization, thick film 389 Angstroem, Mn = 41600, PDI = 1.32; monomer(s): 2-bromo-propionic acid, 11-mercapto-1-undecanol; methyl acrylate
Conditions | Yield |
---|---|
Multistep reaction.; |
11-mercapto-1-undecanol
α-bromopropionyl bromide
methacrylic acid methyl ester
poly(methyl methacrylate), prepared by three-stage surface-initiated atom transfer radical polymerization, thick film 381 Angstroem, Mn = 37400, PDI = 1.48; monomer(s): 2-bromo-propionic acid, 11-mercapto-1-undecanol; methyl methacrylate
Conditions | Yield |
---|---|
Multistep reaction.; |
11-mercapto-1-undecanol
α-bromopropionyl bromide
methacrylic acid methyl ester
poly(methyl methacrylate), prepared by single step surface-initiated atom transfer radical polymerization, thick film 370 Angstroem; monomer(s): 2-bromo-propionic acid, 11-mercapto-1-undecanol; methyl methacrylate
Conditions | Yield |
---|---|
Multistep reaction.; |
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