As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences,
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $600.0 / 800.0
Type:Manufacturers
inquiryProduct Description Product website: http://www.finerchem.com Product Name 4-N-BOC-Aminopiperidine CAS No. 7
Cas:73874-95-0
Min.Order:1 Gram
FOB Price: $8.0
Type:Lab/Research institutions
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:73874-95-0
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry4-N-BOC-Aminopiperidine Basic information Product Name: 4-N-BOC-Aminopiperidine Synonyms: 4-(TERT-BUTOXYCARBONYLAMINO)PIPERIDINE;4-N-TERT-BOC-AMINO PIPERIDINE;4-N-(TERT-BUTOXYCARBONYL)AM
Cas:73874-95-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryAppearance:Off-white solid Storage:Room temperature Package:25kg/drum Application:Intermediates of biologically active compounds Transportation:Express/Sea/Air Port:Any port in china
Cas:73874-95-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:73874-95-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:73874-95-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Product Name: 4-N-BOC-Aminopiperidine Synonyms: 73874-95-0;TERT-BUTYL PIPERIDIN-4-YLCARBAMATE;PIPERIDIN-4-YL-CARBAMIC ACID TERT-BUTYL ESTER;tert-Butyl 4-piperidinylcarbamate;4-Tert-Boc-AminoPiperdine;4-Tert-Boc-Amino-Piperidine;4-N-1-BOC-AMINOPI
Cas:73874-95-0
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:73874-95-0
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:73874-95-0
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:73874-95-0
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryCompany Profile SHENGZHIKAI TECHNOLOGY INDUSTRY CO., LTD is a high-tech enterprise dedicated to the fields of fine chemical products.The scope of products covers pharmaceutical intermediates, plant extracts, chemical reagent, animal p
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $177.0 / 190.0
Type:Trading Company
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:73874-95-0
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:Used as Pharmaceutical Intermediates Transporta
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:73874-95-0
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $8.2 / 8.8
Type:Trading Company
inquiryProduct name: 4-N-(Tert-Butoxycarbonyl)Aminopiperidine CAS No.:73874-95-0 Molecule Formula:C10H20N2O2 Molecule Weight:200.27 Purity: 98% Package: 25kg/drum Description:White to off-white powder Manufacture Standards:Enterprise Standard
Cas:73874-95-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $2.0 / 6.0
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:73874-95-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry4-N-BOC-Aminopiperidine Basic information Product Name: 4-N-BOC-Aminopiperidine Synonyms: 4-(TERT-BUTOXYCARBONYLAMINO)PIPERIDINE;4-N-TERT-BOC-AMINO PIPERIDINE;4-N-(TERT-BUTOXYCARBONYL)AMINOPIPERIDINE;4-BOC-AMINOPIPERIDINE;4-AMINOPIPERIDINE, 4-
Cas:73874-95-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:73874-95-0
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:73874-95-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:73874-95-0
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryProductName:4-Boc-aminopiperidine Synonyms:tert-butyl N-piperidin-4-ylcarbamate CAS:73874-95-0 Molecular Formula: C10H20N2O2 Molecular Weight:200.27800 Purity:≥98% Appearance and character: gray white solid Density: 1.0
Cas:73874-95-0
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquirytert-butyl (1-benzylpiperidin-4-yl)carbamate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With hydrogen; palladium 10% on activated carbon In methanol for 12h; | 99% |
With hydrogen; palladium 10% on activated carbon In methanol for 12h; | 99% |
With hydrogen; palladium on activated charcoal In methanol under 2585.74 Torr; for 18h; | 97% |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 70℃; under 6000.6 - 7500.75 Torr; for 4h; Reagent/catalyst; Temperature; | 90.7% |
1-benzyloxycarbonyl-4-tert-butoxycarbonylaminopiperidine
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol under 2068.59 Torr; | |
palladium In ethanol | 1.8 g (100%) |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98 percent / NaOH / 2-methyl-propan-2-ol / 20 °C 2: 95 percent / H2 / Pd/C / methanol / 20 °C View Scheme |
di-tert-butyl dicarbonate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98 percent / NaOH / 2-methyl-propan-2-ol / 20 °C 2: 95 percent / H2 / Pd/C / methanol / 20 °C View Scheme |
4-amino-1-benzylpiperidine
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / acetonitrile / 1 h / 20 °C 2: 92 percent / cyclohexene / 20 percent Pd(OH)2/C / ethanol / 3.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 99 percent / CH2Cl2 / 18 h / Ambient temperature 2: 97 percent / H2 / 10 percent Pd/C / methanol / 18 h / 2585.74 Torr View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / dichloromethane / 4 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / ethanol View Scheme |
di-tert-butyl dicarbonate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / acetonitrile / 1 h / 20 °C 2: 92 percent / cyclohexene / 20 percent Pd(OH)2/C / ethanol / 3.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / dichloromethane / 4 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / ethanol View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / water; 1,4-dioxane / 25 h / 5 - 20 °C 2: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / 65 °C / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / tetrahydrofuran / 12 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 24 h View Scheme |
benzyl 4-isocyanatotetrahydro-1(2H)-pyridinecarboxylate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CuCl2 / 20 °C 2: H2 / 10 percent Pd/C / methanol / 2068.59 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 99 percent / CH2Cl2 / 18 h / Ambient temperature 2: 97 percent / H2 / 10 percent Pd/C / methanol / 18 h / 2585.74 Torr View Scheme |
4-amino-1-benzylpiperidine
di-tert-butyl dicarbonate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine; palladium dihydroxide; hydrogen In dichloromethane; water | |
Stage #1: 4-amino-1-benzylpiperidine; di-tert-butyl dicarbonate With triethylamine Stage #2: With palladium on activated charcoal; hydrogen | |
Multi-step reaction with 2 steps 1: triethylamine / tetrahydrofuran / 12 h / 20 °C 2: palladium 10% on activated carbon; hydrogen / methanol / 24 h View Scheme | |
Multi-step reaction with 2 steps 1: chloroform 2: acetic acid / palladium-carbon catalyst / methanol View Scheme |
4-amino-1-benzylpiperidine
di-tert-butyl dicarbonate
tert-butyl (1-benzylpiperidin-4-yl)carbamate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran; palladium-carbon; ethanol; n-heptane |
3,5-dichlorobenzyl alcohol
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; 1,1'-carbonyldiimidazole In ethyl acetate; N,N-dimethyl-formamide |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 5 °C / Reflux; Inert atmosphere 2: triethylamine / dichloromethane / 20 °C 3: formic acid; potassium hydroxide; / ethanol / 1 h / 70 °C View Scheme |
1-phenylmethyl-4-piperidone
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium carbonate; hydroxylamine hydrochloride / methanol / 4 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 5 °C / Reflux; Inert atmosphere 3: triethylamine / dichloromethane / 20 °C 4: formic acid; potassium hydroxide; / ethanol / 1 h / 70 °C View Scheme |
2-(4-chloro-7-methylquinazolin-2-yl)-phenol
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 6h; | 100% |
With triethylamine In dichloromethane at 20℃; | 69% |
benzoyl chloride
(piperidin-4-yl)carbamic acid tert-butyl ester
tert-butyl N-(1-benzoylpiperidin-4-yl)carbamate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Ice cooling; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 96% |
With triethylamine In dichloromethane for 18h; | 91% |
With triethylamine In dichloromethane at 20℃; for 2h; | |
With triethylamine In dichloromethane at 20℃; for 2h; |
4-chlorothieno[3,2-d]pyrimidine
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In butan-1-ol at 100℃; for 48h; | 100% |
cyclopentyl iodide
(piperidin-4-yl)carbamic acid tert-butyl ester
4-(N-(tert-butyloxycarbonyl)amino)piperidine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 48h; | 100% |
(7-fluoro-2-oxo-1(2H)-quinolinyl)acetaldehyde
(piperidin-4-yl)carbamic acid tert-butyl ester
1,1-dimethylethyl {1-[2-(7-fluoro-2-oxo-1(2H)-quinolinyl)ethyl]-4-piperidinyl}carbamate
Conditions | Yield |
---|---|
Stage #1: (7-fluoro-2-oxo-1(2H)-quinolinyl)acetaldehyde; (piperidin-4-yl)carbamic acid tert-butyl ester In methanol; chloroform at 20℃; for 1h; Stage #2: With sodium tris(acetoxy)borohydride In methanol; chloroform at 20℃; for 2.83333h; | 100% |
dimethylaminoacetic acid
(piperidin-4-yl)carbamic acid tert-butyl ester
tert-butyl [1-(2-dimethylaminoacetyl)piperidin-4-yl]carbamate
Conditions | Yield |
---|---|
Stage #1: dimethylaminoacetic acid; (piperidin-4-yl)carbamic acid tert-butyl ester With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 46h; Stage #2: With sodium hydroxide In water; ethyl acetate; N,N-dimethyl-formamide; sodium chloride at 20℃; for 0.5h; | 100% |
With sodium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 46h; | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
2-bromoethanol
[1-(2-hydroxyethyl)-piperidin-4-yl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 5h; Inert atmosphere; Reflux; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 6h; Inert atmosphere; | 97% |
With potassium carbonate In acetonitrile for 5h; Heating; | 94% |
(piperidin-4-yl)carbamic acid tert-butyl ester
4-chloro-5-phenyl-thieno[2,3-d]pyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In ethylene glycol at 110℃; for 3h; | 100% |
With triethylamine In isopropyl alcohol for 2h; Heating / reflux; | 75% |
In ethylene glycol at 110℃; for 4h; |
3-(Trifluoromethyl)benzoyl chloride
(piperidin-4-yl)carbamic acid tert-butyl ester
C18H23F3N2O3
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 25℃; for 3.25h; | 100% |
1,4-difluoro-2-nitrobenzene
(piperidin-4-yl)carbamic acid tert-butyl ester
tert-butyl 1-(4-fluoro-2-nitrophenyl)piperidin-4-ylcarbamate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 70℃; for 3.5h; | 100% |
pyridine-2-carbaldehyde
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: pyridine-2-carbaldehyde; (piperidin-4-yl)carbamic acid tert-butyl ester With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; Stage #2: With hydrogenchloride In methanol; diethyl ether at 20℃; | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
4-chloro-2-(2'-hydroxyphenyl)quinazoline
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane | 100% |
methyl 5-[6-(chloromethyl)-1H-benzimidazol-1-yl]-3-({(1R)-1-[2-(trifluoromethyl)phenyl]ethyl}oxy)thiophene-2-carboxylate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane at 20℃; for 18h; | 100% |
9-fluoro-1-(hydroxymethyl)-4-oxo-1,2-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-1-yl 4-methylbenzenesulfonate
(piperidin-4-yl)carbamic acid tert-butyl ester
1,1-dimethylethyl {1-[(9-fluoro-1-hydroxy-4-oxo-1,2-dihydro-4H-pyrrolo[3,2,1-ij]quinolin-1-yl)methyl]-4-piperidinyl}carbamate
Conditions | Yield |
---|---|
With sodium carbonate In ethanol; water | 100% |
With sodium carbonate In ethanol at 20℃; for 16h; | 100% |
With sodium carbonate In ethanol at 20℃; for 16h; | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
In ethylene glycol at 110℃; for 6h; | 100% |
In ethylene glycol at 110℃; for 4h; |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 40℃; | 100% |
4-(benzofuran-3-ylmethoxy)-1H-indole-2-carboxylic acid
(piperidin-4-yl)carbamic acid tert-butyl ester
4-{[4-(benzofuran-3-ylmethoxy)-1H-indole-2-carbonyl]-amino}-piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 4-(benzofuran-3-ylmethoxy)-1H-indole-2-carboxylic acid With N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 0℃; for 0.166667h; Stage #2: (piperidin-4-yl)carbamic acid tert-butyl ester With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate In DMF (N,N-dimethyl-formamide) at 20℃; | 100% |
styrene oxide
(piperidin-4-yl)carbamic acid tert-butyl ester
[1-(2-Hydroxy-2-phenyl-ethyl)-piperidin-4-yl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
100% |
3,5-dichloro-2-hydroxybenzenesulfonyl chloride
(piperidin-4-yl)carbamic acid tert-butyl ester
C16H22Cl2N2O5S
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
acrylonitrile
[1-(2-cyano-ethyl)-piperidin-4-yl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
In ethanol at 80℃; for 2h; | 100% |
(2R,3S)-N-((3S)-1-methyl-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-3-yl)-2,3-bis(3,3,3- trifluoropropyl)succinamide
(piperidin-4-yl)carbamic acid tert-butyl ester
tert-butyl 1-(((2S,3R)-6,6,6-trifluoro-3-((S,Z)-1-methyl-2-oxo-5-phenyl 2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamoyl)-2-(3,3,3-trifluoropropyl)hexanamido)methyl)piperidin-4-yl carbamate
Conditions | Yield |
---|---|
With formaldehyd In ethanol at 75℃; for 18h; | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 4-(2,4-difluorophenoxy)-3-(7-methoxy-1-methyl-1H-pyrrolo[2,3-c]pyridin-3-yl)benzaldehyde; (piperidin-4-yl)carbamic acid tert-butyl ester With acetic acid In dichloromethane at 50℃; for 1h; Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 2h; Cooling with ice; | 100% |
o-bromobenzenesulfonyl chloride
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1.5h; Inert atmosphere; | 100% |
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
6-methyl-2-nitropyridin-3-yl trifluoromethanesulfonate
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 8h; Reflux; | 100% |
6-chloropyridazine-3-carbonitrile
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In ethanol at 20℃; | 100% |
With triethylamine In ethanol at 20℃; | 100% |
With triethylamine In ethanol at 20℃; | 100% |
3-bromo-4-chloro-5-nitropyridine
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 1h; Cooling with ice; | 100% |
With triethylamine In tetrahydrofuran for 1h; Cooling with ice; | 59.7 g |
With triethylamine In tetrahydrofuran for 1h; Cooling with ice; | 59.78 g |
p-Methoxybenzyl bromide
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 1h; | 81% |
With triethylamine In ethanol |
4-chloro-2-methoxynicotinic aldehyde
(piperidin-4-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 100℃; for 0.666667h; | 100% |
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