CAS No.7496-02-8,6-NITROCHRYSENE Suppliers,MSDS download

Dayang Chem (Hangzhou) Co.,Ltd.

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Chrysene, 6-nitro-

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

6-Nitrochrysene

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Hangzhou Fandachem Co.,Ltd

Chrysene, 6-nitro- cas 7496-02-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Chrysene, 6-nitro- cas 7496-02-8

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Henan Kanbei Chemical Co.,LTD

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6-NITROCHRYSENE

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7496-02-8

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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6-NITROCHRYSENE

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Best price/ 6-Nitrochrysene CAS NO.7496-02-8

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Synthetic route

: 218-01-9
chrysene

: 7496-02-8
6-nitrochrysene

Conditions

Conditions	Yield
With bismuth(III) nitrate; Montmorillonite KSF for 0.25h; Nitration;	92%
With sulfuric acid; nitric acid; silica gel In dichloromethane at 25℃; for 24h; Nitration;	82%
With methanesulfonic acid; dinitrogen tetraoxide In dichloromethane at 20℃; for 0.25h; Product distribution; Rate constant; various additivities, nitration of polycyclic aromatic hydrocarbons by N2O4, selectivity, relative reactivities, effect of acid, base; synthetic and mechanistic study;

: 218-01-9
chrysene

A: 7496-02-8
6-nitrochrysene

B: 7496-02-8
6-nitrochrysene

C: 4-nitrochrysene

Conditions

Conditions	Yield
With nitric acid In acetic anhydride at 20℃; for 120h; Yield given. Yields of byproduct given;

...Expand

: 218-01-9
chrysene

: 7697-37-2
nitric acid

: 64-19-7
acetic acid

: 7496-02-8
6-nitrochrysene

Conditions

Conditions	Yield
at 100℃;
at 100℃;

...Expand

: 218-01-9
chrysene

: 7664-93-9
sulfuric acid

: 7697-37-2
nitric acid

: 64-19-7
acetic acid

: 7496-02-8
6-nitrochrysene

Conditions

Conditions	Yield
at 40℃;
at 40℃;

...Expand

: 7496-02-8
6-nitrochrysene

: 2642-98-0
6-aminochrysene

Conditions

Conditions	Yield
With ammonium acetate; zinc In water Product distribution; Ambient temperature; influence of ammonium acetate; the lenght of the reducer column;;	99%
With samarium; iodine In methanol for 8h; Heating;	94%
With samarium; iodine In methanol for 8h; Heating;	90%

: 7496-02-8
6-nitrochrysene

: 114451-10-4
6-hydroxylaminochrysene

Conditions

Conditions	Yield
With 5%-palladium/activated carbon; hydrazine hydrate In tetrahydrofuran at -3℃; for 0.166667h; Inert atmosphere;	80%

: 7496-02-8
6-nitrochrysene

: 108-24-7
acetic anhydride

: 7499-59-4
6-acetoxychrysene

Conditions

Conditions	Yield
Stage #1: 6-nitrochrysene With perhydrodibenzo-18-crown-6 In N,N-dimethyl-formamide at 20℃; for 4h; Oxidation; Stage #2: acetic anhydride With pyridine Acetylation;	65%

: 7496-02-8
6-nitrochrysene

: 32703-90-5
12-nitro-chrysene-5,6-dione

Conditions

Conditions	Yield
With sodium dichromate; acetic acid

: 7496-02-8
6-nitrochrysene

: 6-chloro-12-nitro-chrysene

Conditions

Conditions	Yield
With sulfuryl dichloride; sodium acetate; nitrobenzene at 60℃;

: 7496-02-8
6-nitrochrysene

: 6-bromo-12-nitro-chrysene

Conditions

Conditions	Yield
With bromine; nitrobenzene at 60℃;

: 7496-02-8
6-nitrochrysene

: 10034-85-2
hydrogen iodide

: 64-19-7
acetic acid

red phosphorus: red phosphorus

: 2642-98-0
6-aminochrysene

...Expand

: 7647-01-0
hydrogenchloride

: 7496-02-8
6-nitrochrysene

: 64-19-7
acetic acid

tin: tin

: 2642-98-0
6-aminochrysene

Conditions

Conditions	Yield
at 100℃;

...Expand

: 7791-25-5
sulfuryl dichloride

: 7496-02-8
6-nitrochrysene

: 6-chloro-12-nitro-chrysene

: 7496-02-8
6-nitrochrysene

: 7726-95-6
bromine

: 98-95-3
nitrobenzene

: 6-bromo-12-nitro-chrysene

Conditions

Conditions	Yield
at 60℃;

...Expand

: 7496-02-8
6-nitrochrysene

: 64-19-7
acetic acid

CrO3: CrO3

: 32703-91-6
5-nitro-benzo[a]naphtho[2,1-c]phenazine

Conditions

Conditions	Yield
Umsetzung des Reaktionsprodukts mit o-Phenylendiamin;

...Expand

: 218-01-9
chrysene

: 7664-93-9
sulfuric acid

: 7496-02-8
6-nitrochrysene

: 7697-37-2
nitric acid

: 64-19-7
acetic acid

: 7495-99-0
6,12-dinitro-chrysene

Conditions

Conditions	Yield
at 45 - 50℃; zuletzt bei 100grad;

...Expand

: 7496-02-8
6-nitrochrysene

: N-chrysen-6-yl-4-(7-methoxy-5-oxo-2,3,5,11a-tetrahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-8-yloxy)-butyramide

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 80 percent / SnCl22H2O / ethyl acetate / 3 h 2: isobutyl chloroformate; triethylamine / 12 h / 20 °C 3: 72 percent / SnCl22H2O / ethyl acetate / 3 h / Heating 4: HgCl2; CaCO3 / acetonitrile; H2O / 12 h / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 5-(7-methoxy-5-oxo-2,3,5,11a-tetrahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-8-yloxy)-pentanoic acid chrysen-6-ylamide

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 80 percent / SnCl22H2O / ethyl acetate / 3 h 2: isobutyl chloroformate; triethylamine / 12 h / 20 °C 3: 72 percent / SnCl22H2O / ethyl acetate / 3 h / Heating 4: HgCl2; CaCO3 / acetonitrile; H2O / 12 h / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 625457-62-7
4-{4-[2-(bis-ethylsulfanyl-methyl)-pyrrolidine-1-carbonyl]-2-methoxy-5-nitro-phenoxy}-N-chrysen-6-yl-butyramide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 80 percent / SnCl2*2H2O / ethyl acetate / 3 h 2: isobutyl chloroformate; triethylamine / 12 h / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 625457-64-9
4-{5-amino-4-[2-(bis-ethylsulfanyl-methyl)-pyrrolidine-1-carbonyl]-2-methoxy-phenoxy}-N-chrysen-6-yl-butyramide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 80 percent / SnCl22H2O / ethyl acetate / 3 h 2: isobutyl chloroformate; triethylamine / 12 h / 20 °C 3: 72 percent / SnCl22H2O / ethyl acetate / 3 h / Heating View Scheme

: 7496-02-8
6-nitrochrysene

: 625457-65-0
5-{5-Amino-4-[(S)-2-(bis-ethylsulfanyl-methyl)-pyrrolidine-1-carbonyl]-2-methoxy-phenoxy}-pentanoic acid chrysen-6-ylamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 80 percent / SnCl22H2O / ethyl acetate / 3 h 2: isobutyl chloroformate; triethylamine / 12 h / 20 °C 3: 72 percent / SnCl22H2O / ethyl acetate / 3 h / Heating View Scheme

: 7496-02-8
6-nitrochrysene

: 625457-63-8
5-{4-[(S)-2-(Bis-ethylsulfanyl-methyl)-pyrrolidine-1-carbonyl]-2-methoxy-5-nitro-phenoxy}-pentanoic acid chrysen-6-ylamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 80 percent / SnCl2*2H2O / ethyl acetate / 3 h 2: isobutyl chloroformate; triethylamine / 12 h / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 219121-13-8
N-chrysen-6-yl-4-oxo-4-piperidin-1-yl-butyramide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: isobutylchloroformate; TEA / CH2Cl2 / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 219121-14-9
N-chrysen-6-yl-4-(4-methyl-piperazin-1-yl)-4-oxo-butyramide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: isobutylchloroformate; TEA / CH2Cl2 / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 347142-85-2
N-(6'-chryseneyl)-propane-3'-carboxy-1'-carboxamide

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: 90 percent / TEA / CH2Cl2 / 4 h / 20 °C 3: 90 percent / NaOH / methanol / 3 h / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: 28616-00-4
N-(6'-chryseneyl)-propane-1'-carboxamide-3'-ethylcarboxylate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: 90 percent / TEA / CH2Cl2 / 4 h / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: chrysen-6-yl-(4-morpholin-4-yl-butyl)-amine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: isobutylchloroformate; TEA / CH2Cl2 / 20 °C 3: 80 percent / LiAlH4 / tetrahydrofuran / 12 h / Heating View Scheme

: 7496-02-8
6-nitrochrysene

: N-chrysen-6-yl-3-oxo-3-piperidin-1-yl-propionamide

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: 90 percent / TEA / CH2Cl2 / 4 h / 20 °C 3: 90 percent / NaOH / methanol / 3 h / 20 °C 4: HOBT; BOP; N-methylmorpholine / dimethylformamide / 20 °C View Scheme

: 7496-02-8
6-nitrochrysene

: chrysen-6-yl-[4-(4-methyl-piperazin-1-yl)-butyl]-amine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 90 percent / Sm; I2 / methanol / 8 h / Heating 2: isobutylchloroformate; TEA / CH2Cl2 / 20 °C 3: 80 percent / LiAlH4 / tetrahydrofuran / 12 h / Heating View Scheme

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