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JINING XINHE CHEMICAL CO., LTD

Advantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit

12-Methyltridecanal 75853-49-5

Cas:75853-49-5

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

12-Methyltridecanal Manufacturer/High quality/Best price/In stock

Cas:75853-49-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 12-Methyl Tridecanal supplier in China

Cas:75853-49-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

Hebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable

12-methyltridecanal,12-methyl-tridecanal

Cas:75853-49-5

Min.Order:1 Metric Ton

FOB Price: $1.0 / 2.0

Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

12-Methyltridecanal

Cas:75853-49-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

12-Methyltridecanal / LIDE PHARMA- Factory supply / Best price

Cas:75853-49-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

75853-49-5 12-Methyltridecanal Now we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate (

75853-49-5 12-Methyltridecanal

Cas:75853-49-5

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 75853-49-5 with best quality

Cas:75853-49-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

12-Methyl tridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Manufacturers

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

12-Methyltridecanal

Cas:75853-49-5

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

12 Methyltridecanal

Cas:75853-49-5

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 75853-49-5 12-Methyltridecanal

Cas:75853-49-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 12-Methyltridecanal

Cas:75853-49-5

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Manufacturers

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

12-Methyltridecanal

Cas:75853-49-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

NIGNXIA XINDACHANG TECHNOLOGY CO.,LTD

Donglian as a factory and supplier of aroma chemicals in China, We can provide different quantities of custom synthesis chemicals in food flavor scale more than fourteen years.in addition, our company has researched and developed four series

12-Methyltridecanal

Cas:75853-49-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Hubei Vanz Pharm Co.,Ltd

ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Other

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

12-Methyl Tridecanal

Cas:75853-49-5

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

12-Methyl Tridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Our own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

12-Methyltridecanal cas 75853-49-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

12-Methyltridecanal cas 75853-49-5

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low priceAppearance:Almost colourless to very slightly yellow Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an

12-Methyltridecanal manufature

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

12-Methyltridecanal

Cas:75853-49-5

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

12-methyl-1-tridecanol
21987-21-3

12-methyl-1-tridecanol

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
With pyridinium chlorochromate In dichloromethane at 20℃; for 24h;98%
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -78 - 0℃; for 4h;85%
With pyridinium chlorochromate In dichloromethane for 2h;84%
With dipyridinium dichromate; 3 A molecular sieve In dichloromethane for 2h; Ambient temperature;
With Dess-Martin periodane In dichloromethane at 20℃; for 1h;
13-methyltetradec-1-ene
107841-96-3

13-methyltetradec-1-ene

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
With ozone In dichloromethane at -55℃; Temperature;93.5%
1,2-epoxy-13-methyltetradecane
107841-97-4

1,2-epoxy-13-methyltetradecane

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
With periodic acid In tetrahydrofuran; diethyl ether for 4h;66.04%
methyl 12-methyltridecanoate
5129-58-8

methyl 12-methyltridecanoate

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 93 percent / LiAlH4 / diethyl ether / 2 h / 0 °C
2: 98 percent / pyridinium chlorochromate / CH2Cl2 / 24 h / 20 °C
View Scheme
1-undecen-11-ylbromide
7766-50-9

1-undecen-11-ylbromide

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) Mg, 2.) dilithium tetrachlorocuprate / 1) THF, 2.) THF, -10 deg C, 4 h
2: 1.) NaBH4, Hg(OAc)2, 2.) aq. H2O2, aq. NaOH / 1) THF, 16 h, room temperature; 2) THF, 70 deg C, 1 h
3: 84 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
View Scheme
12-methyltridec-1-ene
156991-32-1

12-methyltridec-1-ene

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) NaBH4, Hg(OAc)2, 2.) aq. H2O2, aq. NaOH / 1) THF, 16 h, room temperature; 2) THF, 70 deg C, 1 h
2: 84 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
View Scheme
ethyl 12-methyltridecanoate
88591-29-1

ethyl 12-methyltridecanoate

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 100 percent / LiAlH4 / tetrahydrofuran
2: pyridinium dichromate (PDC), molecular sieves 3A / CH2Cl2 / 2 h / Ambient temperature
View Scheme
ethyl E-12-methyltridec-2-enoate
157922-16-2

ethyl E-12-methyltridec-2-enoate

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 74 percent / H2 / 10percent Pd/C / ethanol / Ambient temperature
2: 100 percent / LiAlH4 / tetrahydrofuran
3: pyridinium dichromate (PDC), molecular sieves 3A / CH2Cl2 / 2 h / Ambient temperature
View Scheme
1,10-Decanediol
112-47-0

1,10-Decanediol

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrogen bromide / water; toluene / 48 h / Reflux
2: dilithium tetrachlorocuprate / tetrahydrofuran / 20 h / -78 °C
3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 4 h / -78 - 0 °C
View Scheme
1-bromo-10-decanol
53463-68-6

1-bromo-10-decanol

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dilithium tetrachlorocuprate / tetrahydrofuran / 20 h / -78 °C
2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 4 h / -78 - 0 °C
View Scheme
10-undecenoic acid
112-38-9

10-undecenoic acid

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: thionyl chloride / dichloromethane / 10 °C
2: dichloromethane / 5 - 10 °C
3: tetrahydrofuran / 25 - 50 °C
4: potassium hydroxide; hydrazine hydrate / diethylene glycol / 70 - 190 °C
5: ozone / dichloromethane / -55 °C
View Scheme
C21H34O

C21H34O

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium on activated carbon; hydrogen / methanol / 3 h / 20 °C
2: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
View Scheme
13-methyltetradecanoic acid
2485-71-4

13-methyltetradecanoic acid

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

Conditions
ConditionsYield
With α‑dioxygenase from Crocosphaera subtropica In aq. phosphate buffer pH=7.5; Enzymatic reaction;
trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

(+/-)-2-trimethylsilyloxy-13-methyltetradecanonitrile
671756-90-4

(+/-)-2-trimethylsilyloxy-13-methyltetradecanonitrile

Conditions
ConditionsYield
With triethylamine In dichloromethane at 25℃; for 2h;96%
C18H33NO3Si

C18H33NO3Si

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

A

C26H47NO4

C26H47NO4

B

C26H47NO4

C26H47NO4

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at -78℃; for 42h;A n/a
B 87%
N,N-dimethylthioacetamide
631-67-4

N,N-dimethylthioacetamide

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

(S)-3-hydroxy-N,N,14-trimethylpentadecanethioamide
1402050-26-3

(S)-3-hydroxy-N,N,14-trimethylpentadecanethioamide

Conditions
ConditionsYield
With 2,2,5,7,8-pentamethylchroman-6-ol; mesitylcopper(I); (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane In tetrahydrofuran; N,N-dimethyl-formamide at -60℃; for 40h; Inert atmosphere;69%
ethyl bromide
74-96-4

ethyl bromide

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

14-methylpentadecan-3-ol
107841-98-5

14-methylpentadecan-3-ol

Conditions
ConditionsYield
With magnesium 1) ether, 2) ether, a) 0 deg C to rt, 4 h, b) overnight; Yield given. Multistep reaction;
ethylmagnesium bromide
925-90-6

ethylmagnesium bromide

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

14-methylpentadecan-3-ol
107841-98-5

14-methylpentadecan-3-ol

Conditions
ConditionsYield
In tetrahydrofuran
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

methyl (triphenylphosphoranylidene)acetate
21204-67-1

methyl (triphenylphosphoranylidene)acetate

methyl E-14-methylpentadec-2-enoate

methyl E-14-methylpentadec-2-enoate

Conditions
ConditionsYield
In benzene Ambient temperature; Yield given;
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

(+/-)-2-hydroxy-13-methyltetradecanoic acid
22226-24-0

(+/-)-2-hydroxy-13-methyltetradecanoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 96 percent / Et3N / CH2Cl2 / 2 h / 25 °C
2: aq. HCl / 1,2-dimethoxy-ethane / 24 h / 90 °C
3: aq. NaOH / 1,2-dimethoxy-ethane / 2 h / 90 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

2-hydroxy-13-methyl-tetradecanoic acid amide

2-hydroxy-13-methyl-tetradecanoic acid amide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 96 percent / Et3N / CH2Cl2 / 2 h / 25 °C
2: aq. HCl / 1,2-dimethoxy-ethane / 24 h / 90 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

14-methylpentadecan-3-one
90965-32-5

14-methylpentadecan-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrahydrofuran
2: pyridinium chlorochromate / CH2Cl2
View Scheme
Multi-step reaction with 2 steps
1: 1) Mg / 1) ether, 2) ether, a) 0 deg C to rt, 4 h, b) overnight
2: 83.33 percent / pyridinium chlorochromate / CH2Cl2 / 3 h
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

C35H58NOSSi(1+)*CF3O3S(1-)

C35H58NOSSi(1+)*CF3O3S(1-)

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere
2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C
3: diethyl ether / 4.5 h / 0 - 20 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

A

(S)-3-((tert-butyldiphenylsilyl)oxy)-14-methylpentadecanal
1402050-29-6

(S)-3-((tert-butyldiphenylsilyl)oxy)-14-methylpentadecanal

B

C32H50O2Si

C32H50O2Si

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere
2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C
3: diethyl ether / 4.5 h / 0 - 20 °C
4: Li(1+)*AlH4(1-)*3C4H10O / tetrahydrofuran; dichloromethane / 4 h / -78 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

(S)-3-((tert-butyldiphenylsilyl)oxy)-14-methylpentadecanoic acid
1402050-38-7

(S)-3-((tert-butyldiphenylsilyl)oxy)-14-methylpentadecanoic acid

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere
2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C
3: diethyl ether / 4.5 h / 0 - 20 °C
4: Li(1+)*AlH4(1-)*3C4H10O / tetrahydrofuran; dichloromethane / 4 h / -78 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide
1402050-28-5

(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere
2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C
View Scheme
N,N-diallylmethylmethanethioamide
1182707-33-0

N,N-diallylmethylmethanethioamide

12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

A

(S)-N,N-diallyl-3-hydroxy-14-methylpentadecanethioamide
1402050-25-2

(S)-N,N-diallyl-3-hydroxy-14-methylpentadecanethioamide

B

C22H41NOS

C22H41NOS

Conditions
ConditionsYield
With 2,2,5,7,8-pentamethylchroman-6-ol; mesitylcopper(I); (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane In tetrahydrofuran; N,N-dimethyl-formamide at -60℃; for 40h; Concentration; Solvent; Inert atmosphere; Overall yield = 92 %; Overall yield = 67.6 mg;A n/a
B n/a
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

C26H49NO4

C26H49NO4

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: titanium tetrachloride / dichloromethane / 42 h / -78 °C
2: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

C35H65N2O9P

C35H65N2O9P

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: titanium tetrachloride / dichloromethane / 42 h / -78 °C
2: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C
4: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

C35H65N2O11P

C35H65N2O11P

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: titanium tetrachloride / dichloromethane / 42 h / -78 °C
2.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C
4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C
5.1: osmium(VIII) oxide; pyridine / 2.5 h / 20 °C
5.2: 20 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

C40H78N3O12PSi

C40H78N3O12PSi

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1.1: titanium tetrachloride / dichloromethane / 42 h / -78 °C
2.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C
4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C
5.1: osmium(VIII) oxide; pyridine / 2.5 h / 20 °C
5.2: 20 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C
7.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 20 °C
View Scheme
12-methyltridecan-1-al
75853-49-5

12-methyltridecan-1-al

C36H65N3O8Si

C36H65N3O8Si

Conditions
ConditionsYield
Multi-step reaction with 10 steps
1.1: titanium tetrachloride / dichloromethane / 42 h / -78 °C
2.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C
4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C
5.1: osmium(VIII) oxide; pyridine / 2.5 h / 20 °C
5.2: 20 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C
7.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 20 °C
9.1: Dess-Martin periodane / dichloromethane / 4 h / 20 °C
10.1: triethylamine; zinc trifluoromethanesulfonate; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 19 h / 20 °C
View Scheme

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