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Cas:75853-49-5
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inquiry75853-49-5 12-Methyltridecanal Now we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate (
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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12-Methyltridecanal cas 75853-49-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:Almost colourless to very slightly yellow Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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12-methyl-1-tridecanol
12-methyltridecan-1-al
Conditions | Yield |
---|---|
With pyridinium chlorochromate In dichloromethane at 20℃; for 24h; | 98% |
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -78 - 0℃; for 4h; | 85% |
With pyridinium chlorochromate In dichloromethane for 2h; | 84% |
With dipyridinium dichromate; 3 A molecular sieve In dichloromethane for 2h; Ambient temperature; | |
With Dess-Martin periodane In dichloromethane at 20℃; for 1h; |
13-methyltetradec-1-ene
12-methyltridecan-1-al
Conditions | Yield |
---|---|
With ozone In dichloromethane at -55℃; Temperature; | 93.5% |
1,2-epoxy-13-methyltetradecane
12-methyltridecan-1-al
Conditions | Yield |
---|---|
With periodic acid In tetrahydrofuran; diethyl ether for 4h; | 66.04% |
methyl 12-methyltridecanoate
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / LiAlH4 / diethyl ether / 2 h / 0 °C 2: 98 percent / pyridinium chlorochromate / CH2Cl2 / 24 h / 20 °C View Scheme |
1-undecen-11-ylbromide
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) Mg, 2.) dilithium tetrachlorocuprate / 1) THF, 2.) THF, -10 deg C, 4 h 2: 1.) NaBH4, Hg(OAc)2, 2.) aq. H2O2, aq. NaOH / 1) THF, 16 h, room temperature; 2) THF, 70 deg C, 1 h 3: 84 percent / pyridinium chlorochromate / CH2Cl2 / 2 h View Scheme |
12-methyltridec-1-ene
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaBH4, Hg(OAc)2, 2.) aq. H2O2, aq. NaOH / 1) THF, 16 h, room temperature; 2) THF, 70 deg C, 1 h 2: 84 percent / pyridinium chlorochromate / CH2Cl2 / 2 h View Scheme |
ethyl 12-methyltridecanoate
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 100 percent / LiAlH4 / tetrahydrofuran 2: pyridinium dichromate (PDC), molecular sieves 3A / CH2Cl2 / 2 h / Ambient temperature View Scheme |
ethyl E-12-methyltridec-2-enoate
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 74 percent / H2 / 10percent Pd/C / ethanol / Ambient temperature 2: 100 percent / LiAlH4 / tetrahydrofuran 3: pyridinium dichromate (PDC), molecular sieves 3A / CH2Cl2 / 2 h / Ambient temperature View Scheme |
1,10-Decanediol
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen bromide / water; toluene / 48 h / Reflux 2: dilithium tetrachlorocuprate / tetrahydrofuran / 20 h / -78 °C 3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 4 h / -78 - 0 °C View Scheme |
1-bromo-10-decanol
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dilithium tetrachlorocuprate / tetrahydrofuran / 20 h / -78 °C 2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 4 h / -78 - 0 °C View Scheme |
10-undecenoic acid
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: thionyl chloride / dichloromethane / 10 °C 2: dichloromethane / 5 - 10 °C 3: tetrahydrofuran / 25 - 50 °C 4: potassium hydroxide; hydrazine hydrate / diethylene glycol / 70 - 190 °C 5: ozone / dichloromethane / -55 °C View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: palladium on activated carbon; hydrogen / methanol / 3 h / 20 °C 2: Dess-Martin periodane / dichloromethane / 1 h / 20 °C View Scheme |
13-methyltetradecanoic acid
12-methyltridecan-1-al
Conditions | Yield |
---|---|
With α‑dioxygenase from Crocosphaera subtropica In aq. phosphate buffer pH=7.5; Enzymatic reaction; |
trimethylsilyl cyanide
12-methyltridecan-1-al
(+/-)-2-trimethylsilyloxy-13-methyltetradecanonitrile
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 25℃; for 2h; | 96% |
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at -78℃; for 42h; | A n/a B 87% |
N,N-dimethylthioacetamide
12-methyltridecan-1-al
(S)-3-hydroxy-N,N,14-trimethylpentadecanethioamide
Conditions | Yield |
---|---|
With 2,2,5,7,8-pentamethylchroman-6-ol; mesitylcopper(I); (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane In tetrahydrofuran; N,N-dimethyl-formamide at -60℃; for 40h; Inert atmosphere; | 69% |
Conditions | Yield |
---|---|
With magnesium 1) ether, 2) ether, a) 0 deg C to rt, 4 h, b) overnight; Yield given. Multistep reaction; |
ethylmagnesium bromide
12-methyltridecan-1-al
14-methylpentadecan-3-ol
Conditions | Yield |
---|---|
In tetrahydrofuran |
12-methyltridecan-1-al
methyl (triphenylphosphoranylidene)acetate
Conditions | Yield |
---|---|
In benzene Ambient temperature; Yield given; |
12-methyltridecan-1-al
(+/-)-2-hydroxy-13-methyltetradecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 96 percent / Et3N / CH2Cl2 / 2 h / 25 °C 2: aq. HCl / 1,2-dimethoxy-ethane / 24 h / 90 °C 3: aq. NaOH / 1,2-dimethoxy-ethane / 2 h / 90 °C View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 96 percent / Et3N / CH2Cl2 / 2 h / 25 °C 2: aq. HCl / 1,2-dimethoxy-ethane / 24 h / 90 °C View Scheme |
12-methyltridecan-1-al
14-methylpentadecan-3-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrahydrofuran 2: pyridinium chlorochromate / CH2Cl2 View Scheme | |
Multi-step reaction with 2 steps 1: 1) Mg / 1) ether, 2) ether, a) 0 deg C to rt, 4 h, b) overnight 2: 83.33 percent / pyridinium chlorochromate / CH2Cl2 / 3 h View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere 2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C 3: diethyl ether / 4.5 h / 0 - 20 °C View Scheme |
12-methyltridecan-1-al
A
(S)-3-((tert-butyldiphenylsilyl)oxy)-14-methylpentadecanal
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere 2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C 3: diethyl ether / 4.5 h / 0 - 20 °C 4: Li(1+)*AlH4(1-)*3C4H10O / tetrahydrofuran; dichloromethane / 4 h / -78 °C View Scheme |
12-methyltridecan-1-al
(S)-3-((tert-butyldiphenylsilyl)oxy)-14-methylpentadecanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere 2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C 3: diethyl ether / 4.5 h / 0 - 20 °C 4: Li(1+)*AlH4(1-)*3C4H10O / tetrahydrofuran; dichloromethane / 4 h / -78 °C 5: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C View Scheme |
12-methyltridecan-1-al
(S)-3-((tert-butyldiphenylsilyl)oxy)-N,N,14-trimethylpentadecanethioamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,2,5,7,8-pentamethylchroman-6-ol; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; mesitylcopper(I) / tetrahydrofuran; N,N-dimethyl-formamide / 40 h / -60 °C / Inert atmosphere 2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C View Scheme |
N,N-diallylmethylmethanethioamide
12-methyltridecan-1-al
A
(S)-N,N-diallyl-3-hydroxy-14-methylpentadecanethioamide
Conditions | Yield |
---|---|
With 2,2,5,7,8-pentamethylchroman-6-ol; mesitylcopper(I); (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane In tetrahydrofuran; N,N-dimethyl-formamide at -60℃; for 40h; Concentration; Solvent; Inert atmosphere; Overall yield = 92 %; Overall yield = 67.6 mg; | A n/a B n/a |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: titanium tetrachloride / dichloromethane / 42 h / -78 °C 2: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C 3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: titanium tetrachloride / dichloromethane / 42 h / -78 °C 2: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C 3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C 4: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: titanium tetrachloride / dichloromethane / 42 h / -78 °C 2.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C 3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C 4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C 5.1: osmium(VIII) oxide; pyridine / 2.5 h / 20 °C 5.2: 20 h / 20 °C 6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1.1: titanium tetrachloride / dichloromethane / 42 h / -78 °C 2.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C 3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C 4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C 5.1: osmium(VIII) oxide; pyridine / 2.5 h / 20 °C 5.2: 20 h / 20 °C 6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C 7.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C 8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 20 °C View Scheme |
12-methyltridecan-1-al
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1.1: titanium tetrachloride / dichloromethane / 42 h / -78 °C 2.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 19 h / 20 °C 3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C 4.1: triethylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; dmap / dichloromethane / 17 h / 20 °C 5.1: osmium(VIII) oxide; pyridine / 2.5 h / 20 °C 5.2: 20 h / 20 °C 6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C 7.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C 8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 21 h / 20 °C 9.1: Dess-Martin periodane / dichloromethane / 4 h / 20 °C 10.1: triethylamine; zinc trifluoromethanesulfonate; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 19 h / 20 °C View Scheme |
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