CAS No.77189-99-2,Benzenethiol, 2,4,6-trimethoxy- Suppliers

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Benzenethiol, 2,4,6-trimethoxy-Appearance:Off white to slight yellow solid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier

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Benzenethiol, 2,4,6-trimethoxy-

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Synthetic route

: 77189-97-0
Bis(2,4,6-trimethoxyphenyl) Trisulfide

: 77189-99-2
2,4,6-trimethoxybenzenethiol

Conditions

Conditions	Yield
With hydrogenchloride; zinc In benzene	80%

: 621-23-8
1,2,3-trimethoxybenzene

: 77189-99-2
2,4,6-trimethoxybenzenethiol

Conditions

Conditions	Yield
Stage #1: 1,2,3-trimethoxybenzene With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere; Stage #2: With sulfur In tetrahydrofuran; toluene at 20℃; for 6h; Inert atmosphere;	68%
Stage #1: 1,2,3-trimethoxybenzene With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran; hexane at 0 - 20℃; for 1h; Stage #2: With sulfur In tetrahydrofuran; hexane; toluene at 20℃;	60%
With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sulfur In hexane 1.) reflux, 2 h, 2.) reflux, 3 h;	49%

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2-fluoro-N-phenethylacetamide

: C19H23NO4S

Conditions

Conditions	Yield
With tris(2-carboxyethyl)phosphine; 2-amino-2-hydroxymethyl-1,3-propanediol; sodium hydroxide In N,N-dimethyl-formamide at 37℃; pH=8.5; Kinetics;	83%

: 18321-15-8
1,2-dithiane 1,1-dioxide

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 111848-91-0
Sodium; 4-(2,4,6-trimethoxy-phenyldisulfanyl)-butane-1-sulfinate

Conditions

Conditions	Yield
With sodium methylate In methanol at 25℃; for 0.0833333h;	78%

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 135248-89-4
Nα-fluoren-9-ylmethoxycarbonyl-L-cysteine

: 1403834-74-1
Fmoc-Cys(S-TMP)-OH

Conditions

Conditions	Yield
With N-chloro-succinimide In tetrahydrofuran; dichloromethane at -78 - 25℃;	77%
With N-chloro-succinimide In tetrahydrofuran; dichloromethane at -78℃; for 1.5h; Inert atmosphere; Irradiation;	76%

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2,4,6-trimethoxyphenyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
Stage #1: 3,4,6-tri-O-benzyl-D-glucal With Oxone; sodium hydride; sodium hydrogencarbonate In dichloromethane; water; acetone at 0℃; for 0.75h; Stage #2: 2,4,6-trimethoxybenzenethiol In dichloromethane at -78℃; for 0.25h; Molecular sieve; Inert atmosphere; Stage #3: With zinc(II) chloride In diethyl ether; dichloromethane Molecular sieve; Inert atmosphere;	76%

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 172847-87-9
2',4',6'-Trimethoxyphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
With sodium hydride In N,N-dimethyl-formamide 1.) r.t., 10 min, 2.) 3 h;	73%

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 77189-92-5
2-(4-chlorophenylsulfanyl)-1,3,5-trimethoxybenzene

Conditions

Conditions	Yield
With silver hexafluoroantimonate; copper(II) acetate monohydrate In 1,2-dichloro-ethane at 100℃; for 12h; Inert atmosphere; regioselective reaction;	73%

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 77189-97-0
Bis(2,4,6-trimethoxyphenyl) Trisulfide

Conditions

Conditions	Yield
With sulfur dichloride In diethyl ether at 0℃;	70%

: 3,4,6-tri-O-(4-chlorobenzyl)-D-glucal

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2,4,6-trimethoxyphenyl 3,4,6-tri-O-(4-chlorobenzyl)-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
Stage #1: 3,4,6-tri-O-(4-chlorobenzyl)-D-glucal With Oxone; sodium hydride; sodium hydrogencarbonate In dichloromethane; water; acetone at 0℃; for 0.75h; Stage #2: 2,4,6-trimethoxybenzenethiol In dichloromethane at -78℃; for 0.25h; Molecular sieve; Inert atmosphere; Stage #3: With zinc(II) chloride In diethyl ether; dichloromethane Molecular sieve; Inert atmosphere;	61%

: 3,4,6-tri-O-(4-chlorobenzyl)-β-D-galactal

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2,4,6-trimethoxyphenyl 3,4,6-tri-O-(4-chlorobenzyl)-1-thio-β-D-galactopyranoside

Conditions

Conditions	Yield
Stage #1: 3,4,6-tri-O-(4-chlorobenzyl)-β-D-galactal With Oxone; sodium hydride; sodium hydrogencarbonate In dichloromethane; water; acetone at 0℃; for 0.75h; Stage #2: 2,4,6-trimethoxybenzenethiol In dichloromethane at -78℃; for 0.25h; Molecular sieve; Inert atmosphere; Stage #3: With zinc(II) chloride In diethyl ether; dichloromethane Molecular sieve; Inert atmosphere;	60%

: 80040-79-5
3,4,6-tri-O-benzyl-D-galactal

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2,4,6-trimethoxyphenyl 3,4,6-tri-O-benzyl-1-thio-β-D-galactopyranoside

Conditions

Conditions	Yield
Stage #1: 3,4,6-tri-O-benzyl-D-galactal With Oxone; sodium hydride; sodium hydrogencarbonate In dichloromethane; water; acetone at 0℃; for 0.75h; Stage #2: 2,4,6-trimethoxybenzenethiol In dichloromethane at -78℃; for 0.25h; Molecular sieve; Inert atmosphere; Stage #3: With zinc(II) chloride In diethyl ether; dichloromethane Molecular sieve; Inert atmosphere;	59%

: 64-18-6
formic acid

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: S-(2,4,6-trimethoxy)phenyl thioformate

Conditions

Conditions	Yield
Stage #1: formic acid With acetic anhydride at 45℃; for 2.5h; Schlenk technique; Stage #2: 2,4,6-trimethoxybenzenethiol With pyridine at 30℃; for 24h; Schlenk technique;	55%

: 3,4,6-tri-O-(2,4-dichlorobenzyl)-D-glucal

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2,4,6-trimethoxyphenyl 3,4,6-tri-O-(2,4-dichlorobenzyl)-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
Stage #1: 3,4,6-tri-O-(2,4-dichlorobenzyl)-D-glucal With Oxone; sodium hydride; sodium hydrogencarbonate In dichloromethane; water; acetone at 0℃; for 0.75h; Stage #2: 2,4,6-trimethoxybenzenethiol In dichloromethane at -78℃; for 0.25h; Molecular sieve; Inert atmosphere; Stage #3: With zinc(II) chloride In diethyl ether; dichloromethane Molecular sieve; Inert atmosphere;	50%

: 3,4,6-tri-O-(2,4-dichlorobenzyl)-β-D-galactal

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 2,4,6-trimethoxyphenyl 3,4,6-tri-O-(2,4-dichlorobenzyl)-1-thio-β-D-galactopyranoside

Conditions

Conditions	Yield
Stage #1: 3,4,6-tri-O-(2,4-dichlorobenzyl)-β-D-galactal With Oxone; sodium hydride; sodium hydrogencarbonate In dichloromethane; water; acetone at 0℃; for 0.75h; Stage #2: 2,4,6-trimethoxybenzenethiol In dichloromethane at -78℃; for 0.25h; Molecular sieve; Inert atmosphere; Stage #3: With zinc(II) chloride In diethyl ether; dichloromethane Molecular sieve; Inert atmosphere;	50%

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 80279-40-9
di(2,4,6-trimethoxyphenyl) disulphide

Conditions

Conditions	Yield
In dimethyl sulfoxide for 24h; Ambient temperature; Yield given;
With iodine

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 172847-88-0
2',4',6'-Trimethoxyphenyl 1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 73 percent / NaH / dimethylformamide / 1.) r.t., 10 min, 2.) 3 h 2: 91 percent / NaOMe / methanol / 3 h / Ambient temperature View Scheme

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 172847-89-1
2',4',6'-Trimethoxyphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 73 percent / NaH / dimethylformamide / 1.) r.t., 10 min, 2.) 3 h 2: 91 percent / NaOMe / methanol / 3 h / Ambient temperature 3: 67 percent / NaH / dimethylformamide / 1.) r.t., 10 min, 2.) 80 deg C, 10 h View Scheme

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 80279-38-5
Bis(2,4,6-trimethoxyphenyl)sulfid Radikalkation

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: I2 2: AlCl3 / CH2Cl2 View Scheme

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: 1403834-78-5
C36H44N4O8S2

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: N-chloro-succinimide / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Irradiation 2.1: diisopropyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 1.08 h / 20 °C / Inert atmosphere 2.2: rink amide resin / Inert atmosphere View Scheme

: 77189-99-2
2,4,6-trimethoxybenzenethiol

: C21H34N4O6S2

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: N-chloro-succinimide / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Irradiation 2.1: diisopropyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 1.08 h / 20 °C / Inert atmosphere 2.2: rink amide resin / Inert atmosphere 3.1: dichloromethane; N,N-dimethyl-formamide / Inert atmosphere 3.2: Inert atmosphere View Scheme

Yield

Multi-step reaction with 3 steps
1.1: N-chloro-succinimide / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C / Inert atmosphere; Irradiation
2.1: diisopropyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 1.08 h / 20 °C / Inert atmosphere
2.2: rink amide resin / Inert atmosphere
3.1: dichloromethane; N,N-dimethyl-formamide / Inert atmosphere
3.2: Inert atmosphere
View Scheme

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