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(2-Butyl-5-chloro-1H-imidazol-4-yl)methanol cas 79047-41-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry2-n-butyl-4-chloro-1H-imidazol-5-carboxaldehyde
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 20℃; for 2h; | 90% |
With hydrogen; magnesium In methanol at 20℃; under 258.574 - 413.718 Torr; for 0.583333h; |
5-benzyloxymethyl-2-butyl-4-chloro-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With methanesulfonic acid In chloroform at 20℃; for 1h; | 90% |
2-butyl-5-hydroxymethyl-1H-imidazole
A
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With N-chloro-succinimide In tetrahydrofuran | A 65% B 10% |
1,4-dioxane
2-n-butyl-4,5-di-(hydroxymethyl)-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With N-chloro-succinimide In ethanol | 51% |
2-n-butyl-4,5-di-(hydroxymethyl)-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
In 1,4-dioxane; ethanol | 50% |
2-butyl-5-hydroxymethyl-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With N-chloro-succinimide | |
Multi-step reaction with 2 steps 1: Et3N / tetrahydrofuran; acetonitrile / 2 h / 0 °C 2: 1.) NCS, 2.) Zn, AcOH / 1.) THF, acetonitrile, from -5 deg C to 0 deg C, 0.75 h, 2.) frp, -5 deg C to 0 deg C, 1.5 h View Scheme | |
With N-chloro-succinimide In water; ethyl acetate |
2-Butyl-5-trimethylsilanyloxymethyl-1H-imidazole
A
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With N-chloro-succinimide; acetic acid; zinc 1.) THF, acetonitrile, from -5 deg C to 0 deg C, 0.75 h, 2.) frp, -5 deg C to 0 deg C, 1.5 h; Yield given. Multistep reaction. Title compound not separated from byproducts; |
N-(2-benzyloxy-1-cyanoethyl)pentanamide
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 81 percent / CCl4; PPh3 / acetonitrile / 4 h / 45 °C 2: 90 percent / methanesulfonic acid / CHCl3 / 1 h / 20 °C View Scheme |
methyl pentanimidate
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: NaOH / H2O; methanol; toluene 1.2: 55 percent / POCl3 / toluene / 2 h / 100 °C 2.1: 90 percent / NaBH4 / methanol / 2 h / 20 °C View Scheme |
ethyl 2-butyl-1H-imidazole-4(5)carboxylate
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 88 percent / DIBAL / toluene 2: NCS View Scheme |
ethyl methyl ether
2-butyl-5-hydroxymethyl-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With N-chloro-succinimide In tetrahydrofuran; diethyl ether | 16 g (52%) |
sode de l'acide trichloroisocyanurique
2-n-butyl-4,5-di-(hydroxymethyl)-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
In 1,4-dioxane; ethanol |
N-chloro-succinimide
2-butyl-5-hydroxymethyl-1H-imidazole
B
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
In tetrahydrofuran; 2-methoxy-ethanol; water |
2-methoxy-ethanol
2-butyl-5-hydroxymethyl-1H-imidazole
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With N-chloro-succinimide In 1,4-dioxane; water; ethyl acetate |
dichloromethane
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-n-butyl-4-chloro-1H-imidazol-5-carboxaldehyde
Conditions | Yield |
---|---|
With potassium hydroxide In water; acetic acid | 92% |
In water; acetic acid |
4-hydroxy[1]benzopyran-2-one
2-n-butyl-4-chloro-5-hydroxymethylimidazole
malononitrile
Conditions | Yield |
---|---|
With dimethyl sulfoxide; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 20℃; for 9h; | 81% |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
tert-butyldimethylsilyl chloride
2-butyl-4-chloro-5-[(t-butyldimethylsilyloxy)methyl]imidazole
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 3.5h; Ambient temperature; | 80% |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole
2-n-butyl-4-chloro-1-[(2'-(2-triphenylmethyl-2H-tetrazol-5-yl)-1,1'-biphenyl-4-yl)methyl]-1H-imidazole-5-methanol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 10h; | 80% |
Conditions | Yield |
---|---|
With dimethyl sulfoxide; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 20℃; for 12h; | 79% |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-n-butyl-4-chloro-1H-imidazol-5-carboxaldehyde
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In acetic acid at 25℃; for 3h; | 77% |
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; iodine; sodium hydrogencarbonate In water; toluene at 20℃; for 16h; | 690 mg |
With oxygen; Pt/Bi on graphite In methanol at 60℃; under 2250.23 Torr; for 6h; Product distribution; Further Variations:; Reagents; | |
With manganese dioxide In dichloromethane | 12.81 g (86%) |
Conditions | Yield |
---|---|
With dimethyl sulfoxide; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 20℃; for 14h; | 74% |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile
2-n-Butyl-4-chloro-1-[(2'-cyanobiphenyl-4-yl)-methyl]-5-(hydroxymethyl)imidazole
Conditions | Yield |
---|---|
Stage #1: 2-n-butyl-4-chloro-5-hydroxymethylimidazole With sodium methylate In N,N-dimethyl-formamide at 25℃; for 0.5h; Stage #2: 4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile In N,N-dimethyl-formamide at 20℃; for 24h; | 40% |
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) DMF, 40 deg C, 4 h; Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
methyl 4'-(bromomethyl)-3'-fluorobiphenyl-2-carboxylate
methyl 3'-fluoro-4'-<<2-butyl-4-chloro-5-(hydroxymethyl)-1H-imidazol-1-yl>methyl>biphenyl-2-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 3h; | 30% |
methanol
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-butyl-4-chloro-1H-imidazole-5-carboxylic acid,methyl ester
Conditions | Yield |
---|---|
With manganese(IV) oxide; sodium cyanide; acetic acid 1.) THF; Multistep reaction; |
1,4-bis(bromomethyl)benzene
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) methanol, 0 deg C, 2.) DMF, 25 deg C; Multistep reaction; |
6-bromomethyl-2-naphthalenecarbonitrile
2-n-butyl-4-chloro-5-hydroxymethylimidazole
A
6-(2-Butyl-5-chloro-4-hydroxymethyl-imidazol-1-ylmethyl)-naphthalene-2-carbonitrile
B
2-n-butyl-4-chloro-5-(hydroxymethyl)-1-<(2-cyanonaphthalen-6-yl)methyl>imidazole
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 25 deg C, 1 h, 2.) DMF, RT, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
4-(bromomethyl)benzaldehyde
2-n-butyl-4-chloro-5-hydroxymethylimidazole
A
4-(2-Butyl-5-chloro-4-hydroxymethyl-imidazol-1-ylmethyl)-benzaldehyde
B
1-(4-formylbenzyl)-2-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) methanol, 0 deg C, 2.) DMF, 25 deg C; Multistep reaction; |
methyl 4'-(bromomethyl)-[1,1'-biphenyl]-3-carboxylate
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-butyl-1-<(3'-carbomethoxybiphenyl-4-yl)methyl>-4-chloro-5-(hydroxymethyl)imidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) 40 deg C, 4 h; Yield given. Multistep reaction; |
methyl 2-[4-(bromomethyl)benzoyl]benzoate
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-butyl-1-<4-(2-carbomethoxybenzoyl)benzyl>-4-chloro-5-(hydroxymethyl)imidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) 40 deg C, 4 h; Yield given. Multistep reaction; |
methyl 2-[4-(bromomethyl)phenoxy]benzoate
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-butyl-4-chloro-1-[4-(2-carbomethoxyphenoxy)benzyl]-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) 40 deg C, 4 h; Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) 40 deg C, 4 h; Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
methyl 4-(bromomethyl)-3-fluorobenzoate
4-(2-Butyl-4-chloro-5-hydroxymethyl-imidazol-1-ylmethyl)-3-fluoro-benzoic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 3h; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
4'-bromomethyl-2-nitrobiphenyl
2-butyl-4-chloro-5-(hydroxymethyl)-1-<(2'-nitrobiphenyl-4-yl)methyl>imidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) DMF, 40 deg C, 4 h; Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Methyl 4'-(bromomethyl)biphenyl-2-carboxylate
2-butyl-4-chloro-5-hydroxymethyl-1-[(2'-methoxycarbonyl-1,1'-biphenyl-4-yl)methyl]-1H-imidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) DMF, 40 deg C, 4 h; Yield given. Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) DMF, 40 deg C, 4 h; Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
methyl 4'-methyl-2',6'-dimethoxy<1,1'-biphenyl>-2-carboxylate
A
4'-<<2-butyl-4-chloro-5-(hydroxymethyl)-1H-imidazolyl>methyl>-2',6'-dimethoxy<1,1'-biphenyl>-2-carboxylic acid methyl ester
B
4'-<<2-butyl-4-(hydroxymethyl)-5-chloro-1H-imidazolyl>methyl>-2',6'-dimethoxy<1,1'-biphenyl>-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
2-butyl-4-chloro-1-<<2'-(5-cyano-1,2,3-triazol-4-yl)biphenyl-4-yl>methyl>-5-(hydroxymethyl)imidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) DMF, 40 deg C, 4 h; Multistep reaction; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole
A
2-n-butyl-4-chloro-1-[(2'-(2-triphenylmethyl-2H-tetrazol-5-yl)-1,1'-biphenyl-4-yl)methyl]-1H-imidazole-5-methanol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide Product distribution; Ambient temperature; various ratios of reagents; | |
With potassium carbonate In N,N-dimethyl-formamide Ambient temperature; |
2-n-butyl-4-chloro-5-hydroxymethylimidazole
Conditions | Yield |
---|---|
With sodium methylate 1.) DMF, 25 deg C, 0.25 h, 2.) DMF, 40 deg C, 4 h; Multistep reaction; |
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