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inquiryProduct Name: 1-Bromo-4-(trans-4-pentylcyclohexyl)benzene Synonyms: 1-Bromo-4-(4-pentylpropyl-cyclohexyl)-benzene;1-BROMO-4-(TRANS-4-N-PENTYLCYCLOHEXYL)BENZENE;4-PENTYL-CYCLOHEXYL BROMO PHENOL;1-Bromo-4-(4-Pentyl-Cyclohexyl)-Benzene,5PcbrC17H25
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiry1-Bromo-4-(Trans-4-N-Pentylcyclohexyl)BenzeneAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiry1.4-dibromobenzene
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In diethyl ether Ambient temperature; | 86% |
trans-4-pentylcyclohexylbenzene
iron
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
With bromine; iodine In dichloromethane |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
(3,4-difluorophenyl)boronic acid
3,4-difluoro-4'-(4-pentylcyclohexyl)-1,1'-biphenyl
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; potassium carbonate In ethanol; water at 80℃; for 0.5h; Suzuki Coupling; | 97% |
4-fluoroboronic acid
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; potassium carbonate In ethanol; water at 80℃; for 0.5h; Suzuki Coupling; | 95% |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
phenylboronic acid
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; potassium carbonate In ethanol; water at 80℃; for 0.166667h; Suzuki Coupling; | 93% |
4-trifluoromethylphenylboronic acid
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4-(4-pentylcyclohexyl)-4'-(trifluoromethyl)-1,1'-biphenyl
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; potassium carbonate In ethanol; water at 80℃; for 1.25h; Suzuki Coupling; | 93% |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
3,4,5-trifluorophenylboronic acid
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; potassium carbonate In ethanol; water at 80℃; for 2.5h; Suzuki Coupling; | 91% |
cyclopent-3-enyl bromide
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Stage #1: cyclopent-3-enyl bromide With magnesium In diethyl ether Stage #2: 1-bromo-4-(trans-4-pentylcyclohexyl)benzene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In diethyl ether at 20℃; for 12h; Further stages.; | A n/a B n/a C 75% |
4-methoxyphenylboronic acid
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
With sodium carbonate In ethanol; water; toluene at 90℃; for 6h; Inert atmosphere; | 73% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water for 4h; Inert atmosphere; Reflux; | 82 g |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4-methoxyphenylacetylen
1-methoxy-4-((4-(4-pentylcyclohexyl)phenyl)ethynyl)benzene
Conditions | Yield |
---|---|
With Ph2P(CH2CH2O)22CH3; triethylamine; palladium dichloride In water at 80℃; for 8h; Sonogashira coupling; Inert atmosphere; | 71% |
Trimethyl borate
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4-(trans-4-pentylcyclohexyl)phenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 1-bromo-4-(trans-4-pentylcyclohexyl)benzene With magnesium In tetrahydrofuran at 20℃; for 3h; Stage #2: Trimethyl borate In tetrahydrofuran at 20 - 78℃; for 24h; | 70% |
With magnesium In tetrahydrofuran (Ar); dissolving Mg and aryl bromide in dry THF, stirring for 2 h at room temp., addn. of borate deriv. at -78°C, stirring for 5 h at room temp.; washing with HCl, water and chloroform, recrystn. (hexane); | 52% |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
(2,3-difluorophenyl)boronic acid
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water; benzene for 6h; Heating / reflux; | 69.9% |
1-allyl-4-fluorobenzene
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
bis(pinacol)diborane
Conditions | Yield |
---|---|
With [nickel(II)dichloride(dimethoxyethane)]; quinoline; lithium methanolate In 1,4-dioxane at 30℃; Inert atmosphere; Sealed tube; regioselective reaction; | A n/a B 68% |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4-(trans-4-pentylcyclohexyl)phenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 1-bromo-4-(trans-4-pentylcyclohexyl)benzene With magnesium In tetrahydrofuran at 20℃; for 2h; Stage #2: With Trimethyl borate In tetrahydrofuran at 20℃; for 5h; Further stages.; | 52% |
(-)-dimethy-2,3-O-isopropylidene-L-tartrate
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Stage #1: 1-bromo-4-(trans-4-pentylcyclohexyl)benzene With magnesium In tetrahydrofuran at 80℃; for 1h; Inert atmosphere; Stage #2: (-)-dimethy-2,3-O-isopropylidene-L-tartrate In tetrahydrofuran at 80℃; for 11.5h; Inert atmosphere; | 51% |
3-methyl-4-propyl-1-(4-bromophenyl)cyclohexane
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
3r-methyl-4t-propyl-1c-<4'-(trans-4-amylcyclohexyl)-4-biphenylyl>cyclohexane
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; magnesium 2.) THF, reflux, 1 h; Yield given. Multistep reaction; |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
With lithium; zinc dibromide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride 1.) THF, toluene, ultrasonic irradiation, 0-10 deg C, 3.3 h, 2.) THF, toluene, r.t., 3 d; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
3,4,5-trifluoro-1-bromobenzene
Conditions | Yield |
---|---|
Multistep reaction; |
(2,6-difluoropyridin-3-yl)boronic acid
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
2,6-difluoro-3-[4-(trans-4-pentylcyclohexyl)phenyl]-pyridine
Conditions | Yield |
---|---|
Pd(PPh3)4 In ethanol; toluene |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4-n-pentylcyclohexanone
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
With ammonium chloride; magnesium In tetrahydrofuran; ice-water; ethanol; potassium tert-butylate; water; palladium; dimethyl sulfoxide |
sodium carbonate
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
In ethanol; toluene |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Pd(PPh3)4 In ethanol; toluene |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4-(4-n-pentylcyclohexyl)benzeneboronic acid
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
4'-(trans-4-pentylcyclohexyl)-[1,1‘-biphenyl]-4-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium carbonate / toluene; ethanol; water / 6 h / 90 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water / 4 h / Inert atmosphere; Reflux 2: pyridine hydrochloride salt / 1 h / 200 °C View Scheme |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium carbonate / toluene; ethanol; water / 6 h / 90 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere 3: sodium hydroxide / tetrahydrofuran; water; N,N-dimethyl-formamide / 4 h / 20 - 25 °C View Scheme |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sodium carbonate / toluene; ethanol; water / 6 h / 90 °C / Inert atmosphere 2: boron tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere 3: sodium hydroxide / tetrahydrofuran; water; N,N-dimethyl-formamide / 4 h / 20 - 25 °C 4: hydrogen; platinum(IV) oxide / 1,4-dioxane / 19 h / 20 - 80 °C View Scheme |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water / 4 h / Inert atmosphere; Reflux 2.1: pyridine hydrochloride salt / 1 h / 200 °C 3.1: potassium carbonate; potassium iodide / N,N-dimethyl acetamide / 90 °C / Inert atmosphere 3.2: 40 h / 90 °C / Inert atmosphere View Scheme |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water / 4 h / Inert atmosphere; Reflux 2.1: pyridine hydrochloride salt / 1 h / 200 °C 3.1: potassium carbonate; potassium iodide / N,N-dimethyl acetamide / 90 °C / Inert atmosphere 3.2: 40 h / 90 °C / Inert atmosphere 4.1: pyridine / dichloromethane / 24 h / 20 °C View Scheme |
1-bromo-4-(trans-4-pentylcyclohexyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water / 4 h / Inert atmosphere; Reflux 2.1: pyridine hydrochloride salt / 1 h / 200 °C 3.1: potassium carbonate; potassium iodide / N,N-dimethyl acetamide / 90 °C / Inert atmosphere 3.2: 40 h / 90 °C / Inert atmosphere 4.1: pyridine / dichloromethane / 24 h / 20 °C 5.1: potassium carbonate / acetone / 2 h / 70 °C / Inert atmosphere View Scheme |
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