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Solanid-5-en-3-ol, (3b)- cas 80-78-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
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High pure standard, Quick shippment COA with HPLC, MS and NMR spectra. Package:10mg Application:pharmaceutical industry, food industry, research
high purity Application:Drug intermediates Materials intermediates and active molecules
solanidine
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 50℃; for 2h; | 99% |
With tetrabutyl ammonium fluoride In tetrahydrofuran at 50℃; for 2h; | 99% |
3β-Hydroxy-7'-oxo-3'α,6'α-dimethyl-1'αH,3aαH-indolizidino<1',2';16,17>androst-5-en
solanidine
Conditions | Yield |
---|---|
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 0 - 20℃; for 3.5h; Inert atmosphere; | 73% |
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 0 - 20℃; for 3.5h; Inert atmosphere; | 73% |
C30H47NO5S
A
solanidine
B
camtschatcanidine
C
camtschatcanidine monomesylate
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 1h; Heating; | A 63.8% B 20% C 15.7% |
Conditions | Yield |
---|---|
With ethanol; sodium |
solanidine
Conditions | Yield |
---|---|
With ethanol; sodium ethanolate at 200 - 210℃; |
solanidine 3-O-α-L-rhamnopyranosyl-(1<*>2)-O-<β-D-glucopyranosyl-(1<*>4)>-β-D-glucopyranoside
solanidine
Conditions | Yield |
---|---|
With hesperidinase In acetic acid at 37℃; for 24h; | |
Multi-step reaction with 2 steps 1: 38 mg / 1 N H2SO4 / 2 h / Heating 2: hesperidinase / aq. acetic acid / 24 h / 37 °C View Scheme |
Conditions | Yield |
---|---|
With hesperidinase In acetic acid at 37℃; for 24h; |
solanidine
Conditions | Yield |
---|---|
With hesperidinase In acetic acid at 37℃; for 24h; |
α-chaconine
A
solanidine 3-O-β-D-glucopyranoside
B
L-rhamnose
C
solanidine
Conditions | Yield |
---|---|
With water In 1,4-dioxane at 120℃; for 70h; | A 25 mg B 20 mg C 9 mg |
α-chaconine
A
solanidine 3-O-β-D-glucopyranoside
B
solanidine
C
solanidine 3-O-α-L-rhamnopyranosyl-(1->4)-β-D-glucopyranoside
D
solanidine 3-O-α-L-rhamnopyranosyl-(1->2)-β-D-glucopyranoside
Conditions | Yield |
---|---|
at 300℃; | A 27 mg B 15 mg C 19 mg D 31 mg |
Conditions | Yield |
---|---|
With Gibberella pilicaris; MacIlvain buffer at 30℃; Product distribution; various strains of G. pulicaris; |
solanidine
Conditions | Yield |
---|---|
With hydrogenchloride; methanol; water |
solanidine
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol; water |
solanidine
Conditions | Yield |
---|---|
With hydrogenchloride; water |
Conditions | Yield |
---|---|
With hydrogenchloride | |
With hydrogenchloride; water |
Conditions | Yield |
---|---|
With ethanol; sodium |
A
solanidine
Conditions | Yield |
---|---|
With ethanol; sodium |
A
solanidine
Conditions | Yield |
---|---|
With ethanol; sodium |
camtschatcanidine monomesylate
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: 63.8 percent / LiAlH4 / diethyl ether / 1 h / Heating View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Inert atmosphere; Reflux 2: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 3.5 h / 0 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / ethanol / 2 h / 20 °C / Inert atmosphere 2: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 3.5 h / 0 - 20 °C / Inert atmosphere View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / -70 °C 2.1: dmap; pyridine / dichloromethane / 9 h / 0 - 20 °C 3.1: acetonitrile / 7 h / Reflux 3.2: 10 h / 20 °C 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: dmap; pyridine / dichloromethane / 9 h / 0 - 20 °C 2.1: acetonitrile / 7 h / Reflux 2.2: 10 h / 20 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1.1: tetra-(n-butyl)ammonium iodide; boron trifluoride diethyl etherate; acetic anhydride / dichloromethane / 7 h 2.1: sodium azide / N,N-dimethyl-formamide / 65 °C 3.1: potassium carbonate / methanol / 45 °C 4.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C 5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / -70 °C 6.1: dmap; pyridine / dichloromethane / 9 h / 0 - 20 °C 7.1: acetonitrile / 7 h / Reflux 7.2: 10 h / 20 °C 8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: acetonitrile / 7 h / Reflux 1.2: 10 h / 20 °C 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: sodium azide / N,N-dimethyl-formamide / 65 °C 2.1: potassium carbonate / methanol / 45 °C 3.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / -70 °C 5.1: dmap; pyridine / dichloromethane / 9 h / 0 - 20 °C 6.1: acetonitrile / 7 h / Reflux 6.2: 10 h / 20 °C 7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: potassium carbonate / methanol / 45 °C 2.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / -70 °C 4.1: dmap; pyridine / dichloromethane / 9 h / 0 - 20 °C 5.1: acetonitrile / 7 h / Reflux 5.2: 10 h / 20 °C 6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / -70 °C 3.1: dmap; pyridine / dichloromethane / 9 h / 0 - 20 °C 4.1: acetonitrile / 7 h / Reflux 4.2: 10 h / 20 °C 5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
solanidine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: dmap; triethylamine / dichloromethane / 20 °C 2.1: sodium azide / N,N-dimethyl-formamide / 6 h / 60 °C 3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C 3.2: 0.5 h / 0 - 20 °C 4.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol; tetrahydrofuran / 2.5 h / 0 °C 5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C View Scheme |
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride In chloroform at 4℃; for 72h; | 88% |
Conditions | Yield |
---|---|
With pyridine for 1.5h; | 84% |
solanidine
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at -10℃; for 168000h; Oxidation; | 80% |
solanidine
3β-hydroxy-5α-chlorosolanidane
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; chloroform at 4℃; for 96h; | 73% |
solanidine
toluenesulfonic acid 3-azidopropyl ester
Conditions | Yield |
---|---|
Stage #1: solanidine With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Stage #2: toluenesulfonic acid 3-azidopropyl ester In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; | 71% |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane for 1h; Ambient temperature; | A 56% B 39% |
solanidine
p-toluenesulfonyl chloride
A
3β(p-toluenesulfonyloxy)-22αH,25βH-solanid-5-en-3-ol
B
3α,5-cyclo-5α,22αH,25βH-solanidan-6β-ol
Conditions | Yield |
---|---|
With pyridine 1.) 0 deg C, 1 h, 2.) room temp., 24 h; | A 37% B 35% |
Conditions | Yield |
---|---|
With water |
Conditions | Yield |
---|---|
at 360℃; |
Conditions | Yield |
---|---|
With pyridine; chloroform |
solanidine
p-toluenesulfonyl chloride
3β(p-toluenesulfonyloxy)-22αH,25βH-solanid-5-en-3-ol
Conditions | Yield |
---|---|
With pyridine at -10℃; |
aluminum isopropoxide
solanidine
acetone
benzene
Δ4-Solaniden-3-one
aluminum tri-tert-butoxide
solanidine
acetone
benzene
Δ4-Solaniden-3-one
Conditions | Yield |
---|---|
Im Druckgefaess auf dem Dampfbad; | |
With xylene at 130 - 140℃; |
Conditions | Yield |
---|---|
at 150℃; |
Conditions | Yield |
---|---|
With acetic acid; platinum Hydrogenation; |
solanidine
Leptinidin, Δ5-Solanidendiol-(3β,23β), 23β-Hydroxysolanidin
Conditions | Yield |
---|---|
With n-octyl glucopyranoside; NADPH In water at 25℃; for 2h; Mechanism; 14C labeled study on hydroxylation by microsomal fractions from solanum chacoense;; |
solanidine
C27H45NO3
Conditions | Yield |
---|---|
With Peroxyformic acid; dihydrogen peroxide 1.) 75 deg C, 5 min; 2.) 35 deg C, 30 min; Yield given. Multistep reaction; |
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