CAS No.88023-83-0,Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]- Suppliers

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Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]-

Cas:88023-83-0

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Zibo Hangyu Biotechnology Development Co., Ltd

home-produced Application:medicine

Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]-

Cas:88023-83-0

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Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]-

Cas:88023-83-0

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Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

4-methoxybenzyl methylthiomethyl ether

Cas:88023-83-0

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Shanghai chamflyer chemicals Co., Ltd

High quality Application:Pharmaceutial

Benzene, 1-Methoxy-4-[[(Methylthio)Methoxy]Methyl]-

Cas:88023-83-0

Min.Order:0

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Synthetic route

: 2373-51-5
chloro-methylsulfanyl-methane

: 105-13-5
4-Methoxybenzyl alcohol

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

Conditions

Conditions	Yield
Stage #1: 4-Methoxybenzyl alcohol With sodium hydride; sodium iodide In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Stage #2: chloro-methylsulfanyl-methane In tetrahydrofuran at 0 - 20℃; for 12h;	95%
Stage #1: 4-Methoxybenzyl alcohol With sodium hydride; sodium iodide In tetrahydrofuran; mineral oil at 0 - 20℃; for 1h; Inert atmosphere; Stage #2: chloro-methylsulfanyl-methane In tetrahydrofuran; mineral oil at 0 - 20℃; for 12h; Inert atmosphere;	95%
With sodium hydride; sodium iodide In tetrahydrofuran; mineral oil at 0 - 20℃; for 20h; Inert atmosphere;	86%

: 75-18-3
dimethylsulfide

: 105-13-5
4-Methoxybenzyl alcohol

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

Conditions

Conditions	Yield
With Perbenzoic acid In acetonitrile at 0℃; for 3h;	81%

: 2373-51-5
chloro-methylsulfanyl-methane

: 53942-86-2
4-methoxybenzyl alcohol sodium salt

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 4779-31-1
Z-Asp-OBn

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: (S)-2-Benzyloxycarbonylamino-succinic acid 1-benzyl ester 4-(4-methoxy-benzyloxymethyl) ester

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In N,N-dimethyl-formamide at 0℃; for 28h;	100%

: 20806-43-3
Z-Ser(Bzl)-OH

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: (S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionic acid 4-methoxy-benzyloxymethyl ester

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 0℃; for 27h;	100%

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 150-76-5
4-methoxy-phenol

: C16H18O4

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 0℃; for 5h;	95%

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: (3aR,5R,5aS,8aS,8bR)-5-(4-Methoxy-benzyloxymethoxymethyl)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In N,N-dimethyl-formamide at 20℃; for 1h; Product distribution; Further Variations:; Reaction partners; Solvents; Temperatures;	92%

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 99-94-5
p-Toluic acid

: 4-methyl-benzoic acid 4-methoxy-benzyloxymethyl ester

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 20℃; for 4h;	88%

: 25018-67-1
1,2;4,5-di-O-isopropylidene-β-D-(-)-fructopyranose

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: C21H30O8

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In 1,2-dichloro-ethane; N,N-dimethyl-formamide at 20℃; for 2h;	84%

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 88023-78-3
para-methoxybenzyl chloride

Conditions

Conditions	Yield
With acetyl chloride In dichloromethane Inert atmosphere;	80%
With sulfuryl dichloride In dichloromethane at -78℃; for 0.5h;	70%
With sulfuryl dichloride In dichloromethane at -78℃;

: 617-94-7
1-methyl-1-phenylethyl alcohol

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 1-Methoxy-4-(1-methyl-1-phenyl-ethoxymethoxymethyl)-benzene

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 0℃; for 4h;	80%

: 4530-20-5
BOC-glycine

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: tert-butoxycarbonylamino-acetic acid 4-methoxy-benzyloxymethyl ester

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In N,N-dimethyl-formamide at 0℃; for 24h;	78%

: 590-67-0
1-Methylcyclohexanol

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 1-methoxy-4-(1-methyl-cyclohexyloxymethoxymethyl)-benzene

Conditions

Conditions	Yield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 0℃; for 3h;	68%

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 104-93-8
4-Methylanisole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: lithium; 4,4'-di-tert-butylbiphenyl / tetrahydrofuran / 1 h / 0 °C View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 1515-81-7
1-methoxy-4-(methoxymethyl)benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: lithium; 4,4'-di-tert-butylbiphenyl / tetrahydrofuran / 1 h / -78 °C View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 702-23-8
2-(4-Methoxyphenyl)ethanol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 22 percent / lithium; 4,4'-di-tert-butylbiphenyl / tetrahydrofuran / 1 h / -40 °C View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: Acetic acid (1R,4S,5R,6S)-4,5,6-tris-benzyloxy-1-(4-methoxy-benzyloxymethyl)-cyclohex-2-enyl ester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: SO2Cl2 / CH2Cl2 / 0.5 h 2.1: Mg; HgCl2 / tetrahydrofuran / 1 h / 0 °C 2.2: tetrahydrofuran / 0.5 h / 0 °C 2.3: tetrahydrofuran / 0.17 h View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 180524-82-7
(+)-(1S,4S,5S)-4,5-dihydroxy-4,5-O-isopropylidene-1-(p-methoxybenzyloxy)methylcyclopent-2-en-1-ol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SO2Cl2 / CH2Cl2 / 0.5 h / -78 °C 2: 1.) nBu3SnH, LDA, 2.) nBuLi View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 180524-83-8
Acetic acid (3aS,4S,6aS)-4-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-4,6a-dihydro-3aH-cyclopenta[1,3]dioxol-4-yl ester

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: SO2Cl2 / CH2Cl2 / 0.5 h / -78 °C 2: 1.) nBu3SnH, LDA, 2.) nBuLi 3: 96 percent / Et3N, DMAP / CH2Cl2 / 48 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 180524-84-9
Acetic acid (3aS,4S,6aR)-6-(4-methoxy-benzyloxymethyl)-2,2-dimethyl-4,6a-dihydro-3aH-cyclopenta[1,3]dioxol-4-yl ester

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: SO2Cl2 / CH2Cl2 / 0.5 h / -78 °C 2: 1.) nBu3SnH, LDA, 2.) nBuLi 3: 96 percent / Et3N, DMAP / CH2Cl2 / 48 h / Ambient temperature 4: 64 percent / benzoquinone, Pd(CH3CN)2Cl2 / tetrahydrofuran / 3.5 h / Heating View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-85-9
1-(1,1-Dimethyl-prop-2-ynyloxymethoxymethyl)-4-methoxy-benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 89 percent / diisopropylethylamine / CH2Cl2 / 5 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-84-8
4-(4-Methoxy-benzyloxymethoxy)-4-methyl-tetrahydro-pyran-2-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 84 percent / diisopropylethylamine / CH2Cl2 / 30 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-87-1
1-((E)-3,7-Dimethyl-octa-2,6-dienyloxymethoxymethyl)-4-methoxy-benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 95 percent / diisopropylethylamine / CH2Cl2 / 5 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 96 percent / diisopropylethylamine / CH2Cl2 / 4 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-82-6
(3S,4aS,8aS)-3-(4-Methoxy-benzyloxymethoxy)-hexahydro-thiochromen-8-one

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 78 percent / diisopropylethylamine / CH2Cl2 / 4 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-88-2
4-(4-Methoxy-benzyloxymethoxymethyl)-1-(toluene-4-sulfonyl)-1H-indole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 96 percent / diisopropylethylamine / CH2Cl2 / 5 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-83-7
(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 78 percent / diisopropylethylamine / CH2Cl2 / 4 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-86-0
4-[1-(4-Methoxy-benzyloxymethoxy)-3-methyl-but-2-enyl]-1-(toluene-4-sulfonyl)-1H-indole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sulfuryl chloride / CH2Cl2 / -78 °C 2: 100 percent / diisopropylethylamine / CH2Cl2 / 10 h / Ambient temperature View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 1362209-48-0
(1S,4S)-4-((p-methoxybenzyloxy)methoxy)-3-iodocyclopent-2-enol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: sulfuryl dichloride / dichloromethane / 0.5 h / 20 °C / Cooling with ice 2: N-ethyl-N,N-diisopropylamine / dichloromethane; toluene / 3.5 h / 90 °C 3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C View Scheme

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 1362209-54-8
(1S,4S)-4-((p-methoxybenzyloxy)methoxy)-3-((S)-3-(tert-butyldimethylsilyloxy)-5-phenylpentyl)cyclopent-2-enol

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: sulfuryl dichloride / dichloromethane / 0.5 h / 20 °C / Cooling with ice 2: N-ethyl-N,N-diisopropylamine / dichloromethane; toluene / 3.5 h / 90 °C 3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C 4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium hydroxide / tetrahydrofuran / 2 h / 20 °C View Scheme

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