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inquiryProName: 1-(4-Iodophenyl)-2-methylpropan-1-one CasNo: 99059-63-9 Molecular Formula: C10H11IO Appearance: white crystalline powder Application: pharmaceutical raw material DeliveryTime: 3-7days PackAge: 1kg/pack,10kg/pack,,25kg/drum Port: Sh
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inquiryIsobutyronitrile
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; palladium(II) trifluoroacetate; water; trifluoroacetic acid In tetrahydrofuran at 80℃; for 36h; Inert atmosphere; Schlenk technique; | 84% |
4-Iodoacetophenone
methyl iodide
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium hydroxide In toluene at 70℃; for 24h; | 79% |
Conditions | Yield |
---|---|
With bis[dichloro(pentamethylcyclopentadienyl)ruthenium(III)]; bis[2-(diphenylphosphino)phenyl] ether; lithium tert-butoxide at 110℃; for 24h; Inert atmosphere; regioselective reaction; | 72% |
1-(4-iodophenyl)propan-1-one
methyl iodide
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
With sodium amide |
isopropylmagnesium chloride
4-iodobenzoic acid chloride
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
iron(III)-acetylacetonate In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; | |
iron(III)-acetylacetonate In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; | |
iron(III)-acetylacetonate In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; | |
With iron(III)-acetylacetonate In tetrahydrofuran at 20℃; |
Conditions | Yield |
---|---|
With aluminum (III) chloride at 45℃; for 15h; Friedel-Crafts Acylation; |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II) In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; | 85% |
1-(4-iodophenyl)-2-methyl-1-propanone
p-methoxybenzyl chloride
1-[4-(4-methoxybenzyl)phenyl]-2-methylpropan-1-one
Conditions | Yield |
---|---|
Stage #1: p-methoxybenzyl chloride With indium; chloro-trimethyl-silane; ethylene dibromide; lithium chloride In tetrahydrofuran at 40℃; for 15h; Inert atmosphere; Stage #2: With TurboGrignard In tetrahydrofuran at -60 - -50℃; Inert atmosphere; Stage #3: 1-(4-iodophenyl)-2-methyl-1-propanone With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran; ethanol at 40℃; for 16h; Inert atmosphere; chemoselective reaction; | 82% |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II) In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Schlenk technique; | 80% |
3-iodobenzoic acid methyl ester
1-(4-iodophenyl)-2-methyl-1-propanone
ethyl 4'-isobutyrylbiphenyl-3-carboxylate
Conditions | Yield |
---|---|
Stage #1: 3-iodobenzoic acid methyl ester With chloro-trimethyl-silane; aluminium; lithium chloride; lead(II) chloride In tetrahydrofuran at 25 - 30℃; Inert atmosphere; Stage #2: With zinc diacetate In tetrahydrofuran at 25℃; for 0.333333h; Inert atmosphere; Stage #3: 1-(4-iodophenyl)-2-methyl-1-propanone With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride In tetrahydrofuran at 25 - 30℃; Inert atmosphere; chemoselective reaction; | 78% |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II); para-fluorostyrene In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Schlenk technique; | 73% |
5-iodofuran-2-carbaldehyde
1-(4-iodophenyl)-2-methyl-1-propanone
5-(4-(isobutyryl)phenyl)furan-2-carboxaldehyde
Conditions | Yield |
---|---|
Stage #1: 1-(4-iodophenyl)-2-methyl-1-propanone With indium; hepatdecane; lithium chloride In tetrahydrofuran at 50℃; for 24h; Stage #2: 5-iodofuran-2-carbaldehyde With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 60℃; for 12h; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 90℃; Inert atmosphere; | 64% |
1-(4-iodophenyl)-2-methyl-1-propanone
dimethyl sulfoxide
2-methyl-1-[4-(methylsulfonyl)phenyl]propan-1-one
Conditions | Yield |
---|---|
With copper(I) oxide; potassium tert-butylate; oxygen; palladium diacetate In acetylacetone at 100℃; for 20h; Reagent/catalyst; Temperature; | 58% |
1-(4-iodophenyl)-2-methyl-1-propanone
methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate
Conditions | Yield |
---|---|
With [Cp*Rh(MeCN)3](SbF6)2; silver(l) oxide In 1,2-dichloro-ethane at 120℃; for 6h; Schlenk technique; Inert atmosphere; | 50% |
1-(4-iodophenyl)-2-methyl-1-propanone
5-(4-iodo-phenyl)-4-methyl-[1,2]dithiol-3-thione
Conditions | Yield |
---|---|
With biphenyl; phosphorous (V) sulfide; sulfur at 210℃; |
1-(4-iodophenyl)-2-methyl-1-propanone
Methyltriphenylphosphonium bromide
1-iodo-4-(2-methyl-1-methylene-propyl)-benzene
Conditions | Yield |
---|---|
Stage #1: Methyltriphenylphosphonium bromide With tert.-butyl lithium In tetrahydrofuran; hexane at 0℃; for 1h; Stage #2: 1-(4-iodophenyl)-2-methyl-1-propanone In tetrahydrofuran at 20℃; for 14h; | |
Stage #1: Methyltriphenylphosphonium bromide With tert.-butyl lithium In tetrahydrofuran; hexane at 0℃; for 1h; Stage #2: 1-(4-iodophenyl)-2-methyl-1-propanone In tetrahydrofuran at 20℃; for 14h; | |
Stage #1: Methyltriphenylphosphonium bromide With tert.-butyl lithium In tetrahydrofuran; hexane at 0℃; for 1h; Stage #2: 1-(4-iodophenyl)-2-methyl-1-propanone In tetrahydrofuran at 20℃; for 14h; |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C 4.1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide / tetrahydrofuran / 2 h / 65 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C 4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 65 °C View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C 4.1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide / tetrahydrofuran / 2 h / 65 °C 5.1: sodium hydroxide; water / tetrahydrofuran / 16 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C 4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 65 °C 5.1: water; sodium hydroxide / tetrahydrofuran / 16 h / 20 °C View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C 4.1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide / tetrahydrofuran / 2 h / 65 °C 5.1: sodium hydroxide; water / tetrahydrofuran / 16 h / 20 °C 6.1: Chiralpak AD / isopropyl alcohol; n-heptane / Resolution of racemate View Scheme | |
Multi-step reaction with 6 steps 1.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1 h / 0 °C 1.2: 14 h / 20 °C 2.1: dirhodium tetraacetate / benzene / 0.17 h / 80 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: caesium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C 4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 65 °C 5.1: water; sodium hydroxide / tetrahydrofuran / 16 h / 20 °C 6.1: Chiralpak AD / n-heptane; isopropyl alcohol / Resolution of racemate View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
C17H14BrNO
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene-4-sulfonic acid / 85 °C 2.1: n-butyllithium / tetrahydrofuran / 1 h / 0 - 20 °C 2.2: 3 h / -78 - 20 °C View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
C29H24N2O
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: toluene-4-sulfonic acid / 85 °C 2.1: n-butyllithium / tetrahydrofuran / 1 h / 0 - 20 °C 2.2: 3 h / -78 - 20 °C 3.1: XPhos; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / toluene / 24 h / Reflux View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
(2E)-2-cyano-3-(4-(5-(diphenylamino)-3,3-dimethyl-3H-indol-2-yl)phenyl)acrylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: toluene-4-sulfonic acid / 85 °C 2.1: n-butyllithium / tetrahydrofuran / 1 h / 0 - 20 °C 2.2: 3 h / -78 - 20 °C 3.1: XPhos; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / toluene / 24 h / Reflux 4.1: sodium hydroxide / ethanol / 80 °C / Inert atmosphere View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
(4-bromophenyl)hydrazine
C16H13BrIN
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 85℃; Fischer Indole Synthesis; |
1-(4-iodophenyl)-2-methyl-1-propanone
4,5-diamino-6-hydroxypyrimidine
Conditions | Yield |
---|---|
Stage #1: 1-(4-iodophenyl)-2-methyl-1-propanone With bromine In tetrahydrofuran at 20℃; for 2h; Stage #2: 4,5-diamino-6-hydroxypyrimidine With hydrogenchloride In ethanol; water for 12h; Reflux; |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: bromine / tetrahydrofuran / 2 h / 20 °C 1.2: 12 h / Reflux 2.1: copper(l) iodide; Pd(PPh3)Cl2; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 18 h / 80 °C View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: bromine / tetrahydrofuran / 2 h / 20 °C 1.2: 12 h / Reflux 2.1: copper(l) iodide; Pd(PPh3)Cl2; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 18 h / 80 °C 3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 10 h / 20 °C View Scheme |
1-(4-iodophenyl)-2-methyl-1-propanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: bromine / tetrahydrofuran / 2 h / 20 °C 1.2: 12 h / Reflux 2.1: copper(l) iodide; Pd(PPh3)Cl2; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 18 h / 80 °C 3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 10 h / 20 °C 4.1: sodium tetrahydroborate / methanol View Scheme |
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