Conditions | Yield |
---|---|
With alkali hydroxide at 170 - 220℃; |
Conditions | Yield |
---|---|
With potassium hydroxide at 260 - 280℃; | |
With sodium hydroxide at 260 - 280℃; | |
With sulfuric acid at 145℃; |
Conditions | Yield |
---|---|
With diluted alkali at 260 - 280℃; | |
With diluted acid at 150 - 160℃; |
chromatotropic acid
Conditions | Yield |
---|---|
at 170 - 220℃; beim Verschmelzen; |
chromatotropic acid
Conditions | Yield |
---|---|
With alkali beim Schmelzen; |
chromatotropic acid
Conditions | Yield |
---|---|
With alkali hydroxide at 170 - 220℃; |
chromatotropic acid
Conditions | Yield |
---|---|
With sodium hydroxide; water at 200℃; |
Conditions | Yield |
---|---|
at 260 - 280℃; |
Conditions | Yield |
---|---|
at 170 - 220℃; |
Conditions | Yield |
---|---|
at 260 - 280℃; |
Conditions | Yield |
---|---|
beim Verschmelzen; |
Conditions | Yield |
---|---|
at 150 - 160℃; |
3-[(2,6-dibromo-4-methylphenyl)azo]-6[(2-sulfophenyl)azo]-4,5-dihydoxynaphthalene-2,7-disulfonic acid
A
chromatotropic acid
B
3,5-dibromotoluene
C
benzenesulfonic acid
Conditions | Yield |
---|---|
With potassium metaperiodate In water |
Conditions | Yield |
---|---|
With potassium metaperiodate; bovine serum albumin In ethanol; water at 75℃; for 0.0833333h; pH=2; aq. buffer; Enzymatic reaction; |
Conditions | Yield |
---|---|
Stage #1: 1-aminonaphthalene-3,6,8-trisulphonic acid trisodium salt With sodium hydroxide In methanol at 180 - 200℃; under 21002.1 Torr; Stage #2: With sulfuric acid In methanol |
naphthalene
A
chromatotropic acid
B
4-amino-5-hydroxy-2,7-naphthalenedisulfonic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sulfur trioxide; sulfuric acid / 65 - 150 °C 1.2: 40 °C 2.1: hydrogen / 170 °C / 150015 Torr 3.1: sodium hydroxide / methanol / 180 - 200 °C / 21002.1 Torr View Scheme |
4-(4-acetylamino-2-sulphophenylazo)-2,5-di(2-acetoxyethoxy)aniline
chromatotropic acid
C26H25N5O15S3
Conditions | Yield |
---|---|
Stage #1: 4-(4-acetylamino-2-sulphophenylazo)-2,5-di(2-acetoxyethoxy)aniline With hydrogenchloride; aminosulfonic acid; sodium nitrite In water; acetone at 20℃; for 1h; pH=10; Stage #2: chromatotropic acid With lithium hydroxide In water; acetone at 0 - 10℃; pH=7 - 8; Stage #3: With hydrogenchloride; lithium hydroxide more than 3 stages; | 67% |
chromatotropic acid
4-bromo-5-nitrophthalonitrile
Conditions | Yield |
---|---|
With potassium carbonate In water; N,N-dimethyl-formamide at 90℃; for 2h; | 63.8% |
chromatotropic acid
Conditions | Yield |
---|---|
pH 5; | 37% |
p-nitrobenzenediazonium
chromatotropic acid
3-(4-amino-phenylazo)-4,5-dihydroxy-naphthalene-2,7-disulfonic acid ; sodium salt
Conditions | Yield |
---|---|
With sodium sulfide |
chromatotropic acid
4-ethoxybenzenediazonium
Conditions | Yield |
---|---|
With sodium acetate |
chromatotropic acid
benzene diazonium chloride
3-benzeneazo-4,5-dihydroxynaphthalene-2,7-disulfonic acid
Conditions | Yield |
---|---|
With sodium carbonate at 0 - 5℃; | |
With sodium carbonate at 0 - 5℃; |
chromatotropic acid
sodium ethyl sulfate
4-ethoxy-5-hydroxy-naphthalene-2,7-disulfonic acid
Conditions | Yield |
---|---|
With alkali at 180 - 200℃; |
chromatotropic acid
Conditions | Yield |
---|---|
With alkali hydroxide |
chromatotropic acid
Conditions | Yield |
---|---|
With sodium hypochlorite |
chromatotropic acid
4,5-dihydroxy-3-(2-hydroxy-4-sulfo-[1]naphthylazo)-naphthalene-2,7-disulfonic acid
Conditions | Yield |
---|---|
With calcium hydroxide; sodium hydroxide anschliessend mit diazotierter 4-Amino-3-hydroxy-naphthalin-1-sulfonsaeure; |
chromatotropic acid
Conditions | Yield |
---|---|
With calcium hydroxide; sodium hydroxide anschliessend mit diazotiertem 5-Amino-2-anilino-benzolsulfonsaeure in wss.Na2CO3; |
chromatotropic acid
4,5-dihydroxy-6-nitroso-3-(4-sulfo-[1]naphthylazo)-naphthalene-2,7-disulfonic acid
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite anschliessend mit diazotierter 4-Amino-naphthalin-1-sulfonsaeure; |
chromatotropic acid
Conditions | Yield |
---|---|
With calcium hydroxide beim nachfolgenden Behandeln mit diazotiertem 3,3'-Dimethoxy-benzidin, CuSO4 und wss. NH3; |
2-thiazolylamine
chromatotropic acid
4,5-dihydroxy-3-thiazol-2-ylazo-naphthalene-2,7-disulfonic acid
Conditions | Yield |
---|---|
(i) NaNO2, aq. HCl, (ii) /BRN= 1827764/; Multistep reaction; |
chromatotropic acid
4,5,5'-trihydroxy-3,4'-azo-bis-naphthalene-2,7-disulfonic acid
Conditions | Yield |
---|---|
With sodium acetate |
chromatotropic acid
IUPAC Name: 4,5-Dihydroxynaphthalene-2,7-disulfonic acid
The molecular structure of 2,7-Naphthalenedisulfonicacid, 4,5-dihydroxy- (CAS NO.148-25-4) is
.
Empirical Formula: C10H8O8S2
Molecular Weight: 320.2957
Einecs: 205-712-7
Density: 1.929 g/cm3
Freely Rotating Bonds: 4
Polar Surface Area: 121.96 Å2
Index of Refraction: 1.756
Molar Refractivity: 68.06 cm3
Molar Volume: 165.9 cm3
Polarizability: 26.98 ×10-24 cm3
Surface Tension: 104.4 dyne/cm
Canonical SMILES: C1=C2C=C(C=C(C2=C(C=C1S(=O)(=O)O)O)O)S(=O)(=O)O
InChI: InChI=1S/C10H8O8S2/c11-8-3-6(19(13,14)15)1-5-2-7(20(16,17)18)4-9(12)10(5)8/h1-4,11-12H,(H,13,14,15)(H,16,17,18)
InChIKey: HLVXFWDLRHCZEI-UHFFFAOYSA-N
2,7-Naphthalenedisulfonicacid, 4,5-dihydroxy- (CAS NO.148-25-4) is used as organic intermediate.
The Cas Register Number of 2,7-Naphthalenedisulfonicacid, 4,5-dihydroxy- is 148-25-4.The chemical synonyms of 2,7-Naphthalenedisulfonicacid, 4,5-dihydroxy- (CAS NO.148-25-4) are 4,5-Dihydroxy-2,7-naphthalenedisulfonic acid ; and 4,5-Dihydroxynaphthalene-2,7-disulphonic acid .
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