Boric-10B acid supplier | CasNO.13813-79-1

Name
BORIC-10B ACID
EINECS 237-478-7
CAS No. 13813-79-1
Article Data2
CAS DataBase
Density 1.438 g/cm³
Solubility
Melting Point 170.9oC
Formula H₃¹⁰BO₃
Boiling Point
Molecular Weight 61.022
Flash Point
Transport Information
Appearance
Safety 22-26-36/37/39-45
Risk Codes 36/37/38-62-63
Molecular Structure
Hazard Symbols Xn
Synonyms Boric-10Bacid (H310BO3) (6CI,7CI);[10B]Boric acid;
PSA 60.69000
LogP -2.05180

Synthetic route

: (10)B2O3

: 7732-18-5
water

: 13813-79-1
[10B]boric acid

Conditions

Conditions	Yield
(10)B2O3 was dissolved in H2O, evaporation to dryness at room temp.;;

: 4832-27-3
trimethyl borate-10

: 7732-18-5
water

: 13813-79-1
[10B]boric acid

Conditions

Conditions	Yield
at 25℃; Activation energy;

: 13813-79-1
[10B]boric acid

: 71-36-3
butan-1-ol

: 207742-80-1
tributyl (10B)borate

Conditions

Conditions	Yield
In neat (no solvent) Reflux; Inert atmosphere;	96%
Inert atmosphere; Reflux;	95%
In toluene byproducts: H2O; (Schlesinger, H. I., et al.; J. Am. Chem. Soc., 1953, v. 75, pp. 216-215); to anhyd. H3(10)BO3 b-BuOH and toluene added; mixt. heated to 130°C over 5 h; distilled at 226-228°C under 1 atm;	87%
With sulfuric acid In toluene at 130℃; for 3.5h;	73.58%

: 13813-79-1
[10B]boric acid

: 7288-07-5
2-methoxy-N,N-bis(2-methoxyphenyl)-aniline

: 113633-81-1
2,2',2''-nitrilotriphenyl borate

Conditions

Conditions	Yield
In toluene byproducts: H2O; heating a mixture of 0.61 g (10-B) boric acid and 3 g 2,2',2''-nitrilotriphenol in 50 ml toluene under reflux, evaporation and sublimation at 300°C, 0.05 Torr;; elem. anal.;;	90%

: 13813-79-1
[10B]boric acid

: 7789-21-1
fluorosulphonic acid

: 15875-25-9
boron trifluoride

Conditions

Conditions	Yield
room temperature; trap to trap condensation in vacuum, determination of purity by IR;	75%

: 13813-79-1
[10B]boric acid

: 7782-50-5
chlorine

: 28098-23-9
boron trichloride

Conditions

Conditions	Yield
chlorinated at 560°C;	75%

: 13813-79-1
[10B]boric acid

: 67-63-0
isopropyl alcohol

: [10B]-triisopropoxyborane

Conditions

Conditions	Yield
With calcium hydride at 90℃; Inert atmosphere; Schlenk technique;	54%
With calcium hydride In neat (no solvent) at 90℃; for 16h; Inert atmosphere;

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 13813-79-1
[10B]boric acid

: [10B]-pinacolborane

Conditions

Conditions	Yield
Stage #1: 2,3-dimethyl-2,3-butane diol; [10B]boric acid In benzene at 100℃; for 10h; Stage #2: With sodium tetrahydroborate In benzene	35%

: 78-10-4
tetraethoxy orthosilicate

: 13813-79-1
[10B]boric acid

: 86119-84-8, 7664-38-2
phosphoric acid

O2Si(88),(10)BO4P(12) (A%): O2Si(88),(10)BO4P(12) (A%)

Conditions

Conditions	Yield
In neat (no solvent) sol-gel method; accordingly to K. S. Chou, J. Non Cryst. Solids 110 (1989) 122, A. Adamczyk, PhD Thesis, University of Mining and Metallurgy, Krakow, 1999 and A. Adamczyk et al., XXII EUCMOS, Balatonfuered, Hungary, 1996;

...Expand

: 78-10-4
tetraethoxy orthosilicate

: 13813-79-1
[10B]boric acid

: 86119-84-8, 7664-38-2
phosphoric acid

O2Si(97),(10)BO4P(3) (A%): O2Si(97),(10)BO4P(3) (A%)

Conditions

Conditions	Yield
In neat (no solvent) sol-gel method; accordingly to K. S. Chou, J. Non Cryst. Solids 110 (1989) 122, A. Adamczyk, PhD Thesis, University of Mining and Metallurgy, Krakow, 1999 and A. Adamczyk et al., XXII EUCMOS, Balatonfuered, Hungary, 1996;

...Expand

: 78-10-4
tetraethoxy orthosilicate

: 13813-79-1
[10B]boric acid

: 86119-84-8, 7664-38-2
phosphoric acid

O2Si(94.06),(10)BO4P(5.94) (A%): O2Si(94.06),(10)BO4P(5.94) (A%)

Conditions

Conditions	Yield
In neat (no solvent) sol-gel method; accordingly to K. S. Chou, J. Non Cryst. Solids 110 (1989) 122, A. Adamczyk, PhD Thesis, University of Mining and Metallurgy, Krakow, 1999 and A. Adamczyk et al., XXII EUCMOS, Balatonfuered, Hungary, 1996;

...Expand

: gadolinium(III) oxide

: 13813-79-1
[10B]boric acid

: germanium dioxide

: Gd(10)BGeO5

Conditions

Conditions	Yield
In neat (no solvent, solid phase) well ground, mixed under petroleum ether, heated in a covered platinum crucible up to 850°C for 1 d, reground and heated by steps of 50°C up to a maximum of 1100°C; observed by IR spectroscopy and X-ray diffraction;

...Expand

: lanthanum(III) oxide

: 13813-79-1
[10B]boric acid

: germanium dioxide

: La(10)BGeO5

Conditions

Conditions	Yield
In neat (no solvent, solid phase) well ground, mixed under petroleum ether, heated in a covered platinum crucible up to 850°C for 1 d, reground and heated by steps of 50°C up to a maximum of 1100°C; observed by IR spectroscopy and X-ray diffraction;

...Expand

: (10)B2O3

: 13813-79-1
[10B]boric acid

: 7664-39-3
hydrogen fluoride

: 15875-25-9
boron trifluoride

Conditions

Conditions	Yield
In not given

...Expand

: 13813-79-1
[10B]boric acid

: 554-13-2
lithium carbonate

: Li(10)BO2

Conditions

Conditions	Yield
In neat (no solvent) powder ground, gradually heated in a Pt crucible, evolution of gases, sintered (24 h, 800°C); starting material: boric acid with 92.4% (10)B isotopic purity;

: 13813-79-1
[10B]boric acid

: calcium carbonate

: Ca(10)B2O4

Conditions

Conditions	Yield
In neat (no solvent) powder ground, gradually heated in a Pt crucible, evolution of gases, sintered (24 h, 800°C); starting material: boric acid with 92.4% (10)B isotopic purity;

: 13813-79-1
[10B]boric acid

: 802291-32-3
trihydroxy boroxine

Conditions

Conditions	Yield
In neat (no solvent) byproducts: H2O; 95-100°C, 24h;;
In toluene byproducts: H2O; dehydration in boiling toluene by azeotropic distn.;;
In toluene byproducts: H2O; dehydration in boiling toluene by azeotropic distn.;;
In neat (no solvent) byproducts: H2O; 95-100°C, 24h;;

: lithium-6 carbonate

: 13813-79-1
[10B]boric acid

: lithium carbonate

: ((7)Li0.924(6)Li0.076)2O*2.88B2O3

Conditions

Conditions	Yield
In melt melting, casting, annealing (500°C);

...Expand

: lithium-6 carbonate

: 13813-79-1
[10B]boric acid

: lithium carbonate

: ((7)Li0.047(6)Li0.953)2O*2.88B2O3

Conditions

Conditions	Yield
In melt melting, casting, annealing (500°C);

...Expand

: lanthanum(III) oxide

: 7722-76-1
ammonium dihydrogen phosphate

: 13813-79-1
[10B]boric acid

: La7O6(9+)*(10)BO3(3-)*2PO4(3-)=La7O6((10)BO3)(PO4)2

Conditions

Conditions	Yield
In neat (no solvent) mixing, pressing into pellets, heating (Pt crucible, 400°C, 4 h),grinding, pelletizing, calcination (1350+/-10°C, 72 h), cooling (room temp.);

...Expand

: 78-10-4
tetraethoxy orthosilicate

: 13813-79-1
[10B]boric acid

: 86119-84-8, 7664-38-2
phosphoric acid

O2Si(90.88),(10)BO4P(9.12) (A%): O2Si(90.88),(10)BO4P(9.12) (A%)

Conditions

Conditions	Yield
In neat (no solvent) sol-gel method; accordingly to K. S Chou, J. Non Cryst. Solids 110 (1989) 122, A. Adamczyk, PhD Thesis, University of Mining and Metallurgy, Krakow, 1999 and A. Adamczyk et al., XXIII EUCMOS, Balatonfuered, Hungary, 1996;

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.08(B2O3)092

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.13(B2O3)087

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.18(B2O3)082

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.23(B2O3)077

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.28(B2O3)072

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.33(B2O3)067

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 11113-50-1
boric acid

: 584-08-7
potassium carbonate

: (K2O)0.38(B2O3)062

Conditions

Conditions	Yield
In neat (no solvent) fusing, standing (1 h), quenching by removing the platinum crucible fromthe furnace, cooling (dry N2 atm.);

...Expand

: 13813-79-1
[10B]boric acid

: 584-08-7
potassium carbonate

: potassium pentaborate

Conditions

Conditions	Yield
In not given reacting, removing solvent, sintering slightly below m. p.;

: 13813-79-1
[10B]boric acid

: 584-08-7
potassium carbonate

: 3.8B2O3*K2O

Conditions

Conditions	Yield
In not given reacting, removing solvent, sintering slightly below m. p.;

: 13813-79-1
[10B]boric acid

: 7664-39-3
hydrogen fluoride

: 497-19-8
sodium carbonate

: Na(1+)*(10)BF4(1-)=Na(10)BF4

Conditions

Conditions	Yield
In not given HF, H3(10)BO3, Na2CO3 reacted according to H. S. Booth, K. S. Wilson, Inorg. Syn. 1 (1939) 21;

...Expand

Boric-10B acid Specification

The Boric-10B acid, with the CAS registry number 13813-79-1, is also known as (10B)Orthoboric acid. It belongs to the product categories of Alphabetical Listings; B; Stable Isotopes. Its EINECS registry number is 237-478-7. This chemical's molecular formula is H₃¹⁰BO₃ and molecular weight is 61.83. Its IUPAC name is called boric acid. This chemical's classification code is TSCA Flag P [A commenced PMN (Premanufacture Notice) substance].

Physical properties of Boric-10B acid: (1)ACD/BCF (pH 5.5): 1; (2)ACD/BCF (pH 7.4): 1; (3)ACD/KOC (pH 7.4): ; (4)#H bond acceptors: 3; (5)#H bond donors: 3; (6)#Freely Rotating Bonds: 3; (7)Index of Refraction: 1.385; (8)Molar Refractivity: 10.083 cm³; (9)Molar Volume: 43.003 cm³; (10)Surface Tension: 59.198 dyne/cm; (11)Density: 1.438 g/cm³.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause damage to health. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing, gloves and eye/face protection. In case of accident or if you feel unwell seek medical advice immediately (show the label where possible).

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: B(O)(O)O
(2)InChI: InChI=1S/BH3O3/c2-1(3)4/h2-4H
(3)InChIKey: KGBXLFKZBHKPEV-UHFFFAOYSA-N

Product Name

BORIC-10B ACID

Synthetic route

Boric-10B acid Specification

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