Conditions | Yield |
---|---|
With hydrogenchloride; water under 2250.23 Torr; for 7h; Reflux; | 95.6% |
Conditions | Yield |
---|---|
Stage #1: 2-chloroethanamine hydrochloride With sodium thiocarbonate In water at 40 - 60℃; Stage #2: With hydrogenchloride In water at 70 - 85℃; | 95% |
Conditions | Yield |
---|---|
Stage #1: sodium 2‐aminoethyl sulfate With sodium thiocarbonate In water at 40 - 60℃; Stage #2: With hydrogenchloride In water at 70 - 85℃; | 93.5% |
Conditions | Yield |
---|---|
Stage #1: sodium thiocarbonate; 2-chloroethanamine hydrochloride at 40 - 60℃; for 2.5h; Large scale; Stage #2: With hydrogenchloride In water at 70 - 80℃; for 2h; Large scale; | 93.27% |
Conditions | Yield |
---|---|
Stage #1: sodium thiocarbonate; sodium 2‐aminoethyl sulfate at 40 - 60℃; for 2.5h; Large scale; Stage #2: With hydrogenchloride In water at 70 - 85℃; for 2h; Large scale; | 93.03% |
Conditions | Yield |
---|---|
With potassium bromide; sodium nitrite In sulfuric acid; water | 61.4% |
Conditions | Yield |
---|---|
With hydrogenchloride |
thiazolidine-2-thione
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride for 168h; Heating; |
hydrochloride salt of (1-chloro-2-acetylamino-2-methyl-1-phenylpropyl) 2-aminoethyl sulfide
A
N-(2-methyl-1-oxo-1-phenylpropan-2-yl)acetamide
B
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With water |
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride at 155℃; |
ethyleneimine
nitrogen
butanone
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
In acetone |
Conditions | Yield |
---|---|
In water |
Conditions | Yield |
---|---|
Stage #1: 2-mercaptothiazole With sodium hydroxide In water for 3h; Stage #2: With hydrogenchloride In water pH=3; |
N-(tert-butoxycarbonyl)-2-(acetylthio)ethylamine
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water; butan-1-ol at 75℃; for 6h; | 17.8 g |
Conditions | Yield |
---|---|
With acetic acid In methanol |
4-methyl-2,3-pentadienenitrile
2-mercaptoethylamine hydrochloride
(Z)-3-(2-Amino-ethylsulfanyl)-4-methyl-pent-2-enenitrile
Conditions | Yield |
---|---|
With calcium carbonate In ethanol; water for 0.5h; Heating; | 100% |
1,1-Diphenylmethanol
2-mercaptoethylamine hydrochloride
N-<2-(diphenylmethylthio)ethyl>amine hydrochloride
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; acetic acid at 90 - 95℃; for 0.333333h; | 100% |
With boron trifluoride diethyl etherate; acetic acid at 90 - 95℃; for 0.333333h; | 100% |
With boron trifluoride In diethyl ether; acetic acid at 90℃; for 0.25h; | 80% |
With trifluoroacetic acid | |
With boron trifluoride In sodium hydroxide; diethyl ether; ethanol; acetic acid |
3-chloro-2-phenyl-but-2-enal
2-mercaptoethylamine hydrochloride
7-methyl-6-phenyl-2,3-dihydro-1,4-thiazepine
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 0.5h; Ambient temperature; | 100% |
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
Irradiation; | 100% |
In water for 2h; Ambient temperature; Irradiation; | 96% |
triphenylmethyl alcohol
2-mercaptoethylamine hydrochloride
2-amino tritylthio ethane
Conditions | Yield |
---|---|
With trifluoroacetic acid at 20℃; for 3h; | 100% |
With boron trifluoride diethyl etherate; triethylamine In chloroform at 75℃; | 99% |
With boron trifluoride diethyl etherate; triethylamine In chloroform at 75℃; | 99% |
2-mercaptoethylamine hydrochloride
1,3-dibromo-propane
3,7-dithianonane-1,9-diamine
Conditions | Yield |
---|---|
With sodium methylate In methanol at 40℃; for 10h; Inert atmosphere; | 100% |
With sodium methylate In methanol at 40℃; for 10h; | 100% |
With sodium methylate In methanol at 40℃; for 10h; | 100% |
With sodium hydrogencarbonate In ethanol for 3h; Substitution; Heating; | |
Stage #1: 2-mercaptoethylamine hydrochloride; 1,3-dibromo-propane With sodium methylate In methanol at 40℃; for 10h; Stage #2: With sodium hydroxide In water at 20℃; for 10h; |
2-mercaptoethylamine hydrochloride
trityl chloride
<2-<(triphenylmethyl)thio>ethyl>amine hydrochloride
Conditions | Yield |
---|---|
With trifluoroacetic acid at 20℃; for 7h; | 100% |
In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 99% |
In dichloromethane; N,N-dimethyl-formamide at 20℃; for 2h; | 90% |
2-mercaptoethylamine hydrochloride
Nα-carbobenzyloxy-L-2-amino-3-(oxiranecarbonylamino)propionic acid
Conditions | Yield |
---|---|
In water; acetone at 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 2,2'-dipyridyldisulphide In methanol for 0.5h; Sonication; Inert atmosphere; Stage #2: 2-mercaptoethylamine hydrochloride In methanol at 20℃; Inert atmosphere; | 100% |
In methanol at 20℃; Sonication; Inert atmosphere; | 100% |
In methanol at 20℃; Inert atmosphere; Sealed tube; Sonication; | 93% |
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; for 3h; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 3h; | 100% |
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
In methanol at 20℃; for 4h; UV-irradiation; | 100% |
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
In water for 0.25h; UV-irradiation; | 100% |
Conditions | Yield |
---|---|
Stage #1: 2-mercaptoethylamine hydrochloride With N,N,N',N'-tetramethylguanidine In N,N-dimethyl-formamide at 0℃; for 1h; Stage #2: M40409 In N,N-dimethyl-formamide at 20℃; for 20h; | 100% |
pent-4-en-1-yl 6(VI)-O-((2-naphthyl)methyl)-1-thio-β-maltohexaoside
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
In methanol; water at 20℃; for 4h; UV-irradiation; | 100% |
With water In methanol at 20℃; UV-irradiation; |
methanethiosulfonic acid S-methyl ester
2-mercaptoethylamine hydrochloride
2-methyldithio-ethylamine
Conditions | Yield |
---|---|
Stage #1: methanethiosulfonic acid S-methyl ester; 2-mercaptoethylamine hydrochloride In methanol at 20℃; Stage #2: With triethylamine In methanol | 100% |
2-mercaptoethylamine hydrochloride
acetic anhydride
2-(acetylamino)ethanethiol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; potassium hydroxide In water at 22℃; | 100% |
With sodium hydrogencarbonate; potassium hydroxide In water at 20℃; for 2.5h; | 92% |
With sodium hydrogencarbonate; potassium hydroxide In water at 20℃; for 2.5h; | 92% |
triphenylmethyl alcohol
2-mercaptoethylamine hydrochloride
<2-<(triphenylmethyl)thio>ethyl>amine hydrochloride
Conditions | Yield |
---|---|
With trifluoroacetic acid at 20℃; | 100% |
2-mercaptoethylamine hydrochloride
methyl iodide
(2-aminoethyl)methylsulfide
Conditions | Yield |
---|---|
Stage #1: 2-mercaptoethylamine hydrochloride With sodium hydroxide In ethanol at 0℃; for 0.166667h; Stage #2: methyl iodide In ethanol at 0 - 20℃; for 3.5h; | 100% |
With sodium hydroxide In ethanol at -10 - 0℃; for 3h; | 89% |
With sodium hydroxide In ethanol at 20℃; for 2.25h; Inert atmosphere; Cooling with ice; | 80% |
With potassium hydroxide In ethanol at 20℃; | 39.3% |
pent-4-en-1-yl 4-O-(6-O-((2-naphthyl)methyl)-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside
2-mercaptoethylamine hydrochloride
5-((2-aminoethyl)thio)pent-1-yl 4-O-(6-O-((2-naphthyl)methyl)-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol; water at 20℃; for 4h; UV-irradiation; | 100% |
pent-4-en-1-yl 6(III)-O-((2-naphthyl)methyl)-1-thio-β-maltotrioside
2-mercaptoethylamine hydrochloride
5-((2-aminoethyl)thio)pent-1-yl 6(III)-O-((2-naphthyl)methyl)-1-thio-β-maltotrioside
Conditions | Yield |
---|---|
In methanol; water at 20℃; for 4h; UV-irradiation; | 100% |
7-octen-1-yl β-D-galactopyranosyl-(1→4)-[α-L-fucopyranosyl-(1→3)]-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1→3)-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside
2-mercaptoethylamine hydrochloride
8-[(2-aminoethyl)thiol]-1-octyl β-D-galactopyranosyl-(1→4)-[α-L-fucopyranosyl-(1→3)]-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1→3)-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside
Conditions | Yield |
---|---|
In methanol for 2.5h; Inert atmosphere; UV-irradiation; | 100% |
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With 2,2-dimethoxy-2-phenylacetophenone In tetrahydrofuran; methanol for 0.5h; Inert atmosphere; UV-irradiation; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; Inert atmosphere; Sealed tube; | 100% |
With acetic acid In methanol at 40℃; for 48h; |
ethyl (4-biphenyl)-α-bromoacetate
2-mercaptoethylamine hydrochloride
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 70℃; for 24h; | 100% |
2-mercaptoethylamine hydrochloride
allyl L-glycero-α-D-manno-heptopyranoside
3-(2-Aminoethylthio)propyl-L-glycero-α-D-manno-heptopyranosid hydrochloride
Conditions | Yield |
---|---|
In water at 25℃; for 2h; Irradiation; | 99% |
2-mercaptoethylamine hydrochloride
Allyl-O-(L-glycero-α-D-manno-heptopyranosyl)-(1->7)-O-(L-glycero-α-D-manno-heptopyranosyl)-(1->3)-L-glycero-α-D-manno-heptopyranosid
3-(2-Aminoethylthio)propyl-O-(L-glycero-α-D-manno-heptopyranosyl)-(1->7)-O-(L-glycero-α-D-manno-heptopyranosyl)-(1->3)-L-glycero-α-D-manno-heptopyranosid
Conditions | Yield |
---|---|
In water for 2h; Ambient temperature; Irradiation; | 99% |
2-mercaptoethylamine hydrochloride
acetic acid
allyl (7-O-carbamoyl-L-glycero-α-D-manno-heptopyranosyl)-(1->3)-L-glycero-α-D-manno-heptopyranoside
Conditions | Yield |
---|---|
In water at 20℃; for 1.5h; Addition; Irradiation; | 99% |
Conditions | Yield |
---|---|
With sodium hydroxide In neat (no solvent) at 80℃; for 0.5h; | 99% |
With tetrakis(μ2-α-methacrylate-O,O')-bis(H2O)-dicopper(II); sodium acetate at 80℃; for 5h; Neat (no solvent); | 84% |
2-mercaptoethylamine hydrochloride
anthranilic acid nitrile
2-(4,5-dihydrothiazol-2-yl)aniline
Conditions | Yield |
---|---|
With sodium hydroxide In neat (no solvent) at 80℃; for 2h; | 99% |
With sodium hydroxide at 80℃; | 96% |
With tetrakis(μ2-α-methacrylate-O,O')-bis(H2O)-dicopper(II); sodium acetate at 80℃; for 3.5h; Neat (no solvent); | 92% |
IUPAC Name :2-AMINOETHANETHIOL hydrochloride
Chemical Formula :C2H8ClNS
Cysteamine HCl is the manufacturing cimetidine as such drug intermediates.
Risk terms : R22 : Harmful if swallowed
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