Our advantages: Higher cost performance and rich experience Goods in stock Superior service Convenient mode of transportation Shortest delivery time massive chemical's supply chain services is competitive, fast, better and secure, so pls c
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:100-19-6
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:100-19-6
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inquiryProduct description: Product name 4'-Nitroacetophenone CAS number 100-19-6 Assay ≥99% Appearance Yellowish crystal Capacity 200mt/year Application Pharmaceuticale interme
Cas:100-19-6
Min.Order:100 Gram
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inquiry1 Factory price 2 Good service 3 High quality 4 Prompt delivery chengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pha
Cas:100-19-6
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inquiryNow we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti
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Cas:100-19-6
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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Min.Order:10 Kilogram
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inquiryName 4-Nitroacetophenone CAS 100-19-6 Purity 99%min Appearance Yellow Ap
Appearance:Yellow crystalline powder Storage:R T Package:25kg/Barrel Application:Used as pharmaceutical chloramphenicol intermediate and dye intermediate Transportation:Express/Sea/Air Port:Any port in China
Cas:100-19-6
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inquiryProduct Name: 4-Nitroacetophenone CAS: 100-19-6 MF: C8H7NO3 MW: 165.15 EINECS: 202-827-4 Melting point 75-78 °C(lit.) Boiling point 202 °C(lit.) density 1.3450 (rough estimate) refractive index 1.5468 (estimat
4-Nitroacetophenone CAS: 100-19-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
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Min.Order:10 Gram
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Type:Trading Company
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Min.Order:1 Kilogram
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inquiry100-19-6 C8H7NO3 4-NitroacetophenoneAppearance:white powder Storage:Normal temperature Package:according to customers' requirements Application:Aromatic Acetophenones & Derivatives (substituted);C7 to C8;Carbonyl Compounds;Ketones
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Conditions | Yield |
---|---|
With silica-supported Jones reagent In dichloromethane for 0.00269444h; | 100% |
With Oxone; potassium bromide In water; acetonitrile at 20℃; for 3h; Reagent/catalyst; Solvent; | 99% |
With iodine pentoxide; potassium bromide In water at 20℃; for 12h; | 98% |
2-methyl-2-(4-nitrophenyl)-1,3-dithiane
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With water; silver (I) ion In 1,4-dioxane at 25℃; Kinetics; Product distribution; var. temp.; | 100% |
With dihydrogen peroxide; niobium pentachloride; sodium iodide In water; ethyl acetate at 20℃; for 5h; | 100% |
With iron(III)-acetylacetonate; dihydrogen peroxide; sodium iodide In water; ethyl acetate at 20℃; for 18.4h; | 92% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 0.166667h; Mechanism; | 100% |
With bis(η3-allyl-μ-chloropalladium(II)) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 0.166667h; | 100% |
With benzoylchlorobis(triphenylphosphine)palladium(II) In chloroform at 65℃; for 24h; | 95% |
With N,N,N,N,N,N-hexamethylphosphoric triamide; poly-γ-(diphenylphosphino)propylsiloxane palladium(0) at 65℃; for 20h; | 83% |
1,1-dimethoxy-1-(4-nitrophenyl)ethane
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With water at 80℃; for 2h; | 100% |
With carbon tetrabromide In water; acetonitrile at 80℃; for 2h; | 97% |
1-(4-nitrophenyl)-2-(phenylselanyl)ethan-1-one
A
diphenyl diselenide
B
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With GLUTATHIONE In methanol Product distribution; Mechanism; 0.1 M phosphate buffer, pH=6.9; differnt quantity of glutathione; relative reactivity to α-(phenylselenenyl)acetophenone; | A 99% B 87% |
Conditions | Yield |
---|---|
With water at 60℃; for 20h; Sealed tube; | 99% |
With C22H20AuN3O2P(1+)*CF3O3S(1-); water; silver trifluoromethanesulfonate; acetic acid at 100℃; for 10h; | 98% |
With chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I) In methanol; water at 120℃; for 6h; Schlenk technique; regioselective reaction; | 94% |
Conditions | Yield |
---|---|
With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Irradiation; Green chemistry; | 98% |
With tert.-butylhydroperoxide; phosphomolybdic acid; copper(II) acetate monohydrate In water; acetonitrile at 90℃; for 10h; Sealed tube; | 97% |
With Oxone; water; potassium bromide In dichloromethane at 20℃; for 16h; Time; Irradiation; Sealed tube; | 96% |
p-nitroacetophenone oxime
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With water; oxygen In acetonitrile at 60℃; under 760.051 Torr; for 2h; Autoclave; Green chemistry; | 98% |
With Dess-Martin periodane In dichloromethane; water for 0.25h; | 96% |
With sodium tungstate; dihydrogen peroxide In water; acetone at -5 - 20℃; for 5h; | 96% |
2-methyl-2-(4-nitrophenyl)-1,3-oxathiolane
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With t-butyl thionitrite In acetonitrile at 0℃; for 0.6h; | 98% |
With N-Bromosuccinimide; water In acetone at 20℃; for 6h; Hydrolysis; | 88% |
With eosin Y disodium salt In acetonitrile at 20℃; for 3h; Irradiation; | 68% |
With oxygen; Rose Bengal lactone In ethanol pH=7.4; Kinetics; | 50% |
1-(4-nitro-phenyl)-ethanone-diethylacetal
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With water at 80℃; for 2h; | 98% |
With carbon tetrabromide In water; acetonitrile at 80℃; for 2h; Product distribution; other reaction conditions; |
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With silica-OSO3H; silica gel In toluene at 60 - 70℃; for 1h; | 98% |
With tetrachlorosilane; silica gel In toluene at 60 - 70℃; for 1.33333h; | 93% |
With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; aluminium trichloride In acetonitrile Heating; |
4-methyl-N'-(1-(4-nitrophenyl)ethylidene)benzenesulfonohydrazide
A
(4-nitrophenyl)ethanone
B
4-nitro-benzoic acid
Conditions | Yield |
---|---|
With silica-supported selenamide; dihydrogen peroxide In tert-butyl alcohol at 55℃; for 20h; | A 98% B 2% |
α,α-dibromo-4-nitroethylbenzene
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With water In dichloromethane at 20℃; for 24h; visible light irradiation; | 98% |
2-methyl-2-(4-nitrophenyl)-1,3-dithiane
B
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With Methylthio(bismethylthio)sulfonium hexachloroantimonate In dichloromethane at -77℃; for 0.0166667h; Yields of byproduct given; | A n/a B 97% |
Conditions | Yield |
---|---|
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-d6-formamide at 20℃; for 4h; Irradiation; | 97% |
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate In 2,2,2-trifluoroethanol at 20℃; for 4h; UV-irradiation; Sealed tube; Green chemistry; | 96% |
With bismuth; ammonium fluoride-hydrogen fluoride In water at 20℃; for 3h; | 94% |
2-(4-nitrophenyl)-2-methyl-1,3-dioxolane
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With Montmorillonite K 10; water In acetone for 5.5h; Heating; | 97% |
With carbon tetrabromide In water; acetonitrile at 80℃; for 6h; | 96% |
With erbium(III) triflate In nitromethane at 20℃; for 96h; | 94% |
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; vanadia In water at 100℃; for 7h; | 97% |
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With 1-amino-3-methylbutane; ammonium chlorate; potassium bromide at 50 - 57℃; for 1h; Temperature; | 97% |
α-(2,4-dinitrophenyl)ethyl nitrate
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With sodium ethanolate; acetic acid In ethanol at 22 - 25℃; for 0.333333h; pH=7; | 96% |
With sodium methylate; potassium carbonate oder mit anderen Basen; | |
With sodium methylate; potassium carbonate oder mit anderen Basen; |
1-(4-nitrophenyl)ethanone hydrazone
A
(4-nitrophenyl)ethanone
B
1-(4-nitrophenyl)-1-diazoethane
Conditions | Yield |
---|---|
1-methylimidazole ligand In acetonitrile for 0.0833333h; | A 4% B 96% |
Conditions | Yield |
---|---|
With water; fluorine In chloroform; acetonitrile at -15℃; for 0.0333333h; Product distribution; other substituted anilines; | 95% |
With water; fluorine In chloroform; acetonitrile at -15℃; for 0.0333333h; | 95% |
With 1,9-diperoxynonanedioic acid In acetonitrile at 50℃; for 0.5h; | 94% |
p-nitrobenzene iodide
carbon monoxide
tetramethylstannane
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
bis(η3-allyl-μ-chloropalladium(II)) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 30h; | 95% |
With MCM-41-supported bidentate phosphine palladium(0) complex In N,N-dimethyl-formamide at 70℃; under 760.051 Torr; for 10h; Stille carbonylative cross-coupling; | 84% |
4-ethylnitrobenzene
A
1-[4-nitrophenyl]-1-ethanol
B
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With cerium(III) sulfate; barium bromate In water; acetonitrile for 24h; Heating; Title compound not separated from byproducts; | A n/a B 95% |
With N-hydroxyphthalimide; oxygen; acetaldehyde In acetonitrile Ambient temperature; | A 2 % Chromat. B 22 % Chromat. |
With oxygen under 760.051 Torr; Heating; | A 16.5 %Chromat. B 83.5 %Chromat. |
1-(4-nitro-phenyl)-ethylamine
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With 4-phenylnaphthalene-1,2-dione In acetonitrile at 80℃; for 36h; | 95% |
Multi-step reaction with 3 steps 1: N-chloro-succinimide / 0.17 h / 20 °C / Milling 2: triethylamine / 0.17 h / 20 °C / Milling 3: water; hydrogenchloride / tetrahydrofuran / 2 h / 20 °C View Scheme |
1-(4-nitrophenyl)-1-diazoethane
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With N,N'-bis(salicylidene)ethylenediaminatocobalt(III) hydroxide; oxygen In acetonitrile | 94% |
4-acetylphenylboronic acid
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With N-Bromosuccinimide; [bis(trifluoroacetoxy)iodo]benzene; sodium nitrite In acetonitrile at 20℃; for 3h; regioselective reaction; | 94% |
With bismuth (III) nitrate pentahydrate In toluene at 70 - 80℃; for 2h; Inert atmosphere; | 87% |
With 1,3-disulfonic acid imidazolium nitrate In neat (no solvent) at 20℃; for 0.0166667h; | 78% |
With dipotassium peroxodisulfate; bismuth (III) nitrate pentahydrate In benzene at 70℃; for 12h; Inert atmosphere; | 70% |
1,2-bis(1-(4-nitrophenyl)ethylidene)hydrazine
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water; acetonitrile at 50℃; for 16h; Oxidation; | 93% |
With 2-phenyl-1,2-benzoisoselenazol-3(2H)-one; dihydrogen peroxide In methanol; water at 65℃; for 72h; | 90% |
With HOF* CH3CN In dichloromethane at 0℃; for 0.0166667h; | 90% |
With sulfuric acid; silica gel In hexane for 1h; | 86% |
4-nitro-(1-bromoethyl)benzene
A
(4-nitrophenyl)ethanone
B
4-nitro-benzoic acid
Conditions | Yield |
---|---|
With Oxone In water; acetonitrile at 20℃; for 5.5h; | A 93% B 5% |
p-nitrobenzene iodide
carbon monoxide
methylmercury(II) iodide
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
dichloro bis(acetonitrile) palladium(II) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; under 760 Torr; for 1.5h; Product distribution; various solvents, Pd-catalysts and reaction conditions; | 92% |
With tetra-(n-butyl)ammonium iodide; dichloro bis(acetonitrile) palladium(II) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; under 760 Torr; for 1.5h; | 85% |
(4-nitrophenyl)ethanone
p-nitroacetophenone oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride | 100% |
With hydroxylamine hydrochloride; sodium acetate In ethanol for 0.0166667h; Condensation; Irradiation; | 98% |
With hydroxylamine hydrochloride; silica gel for 0.1h; | 95% |
(4-nitrophenyl)ethanone
N-(4-acetylphenyl)hydroxylamine
Conditions | Yield |
---|---|
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; for 3.5h; Inert atmosphere; | 100% |
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; Inert atmosphere; | 100% |
With rhodium contaminated with carbon; hydrazine hydrate In tetrahydrofuran at 0℃; for 3.5h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With methyltriphenylphosphonium tetrahydroborate In dichloromethane Reduction; | 100% |
Stage #1: (4-nitrophenyl)ethanone With sodium tetrahydroborate at 25℃; for 0.5h; Ball milling; neat (no solvent); Stage #2: With water regiospecific reaction; | 100% |
With C40H37ClN2PRuS(1+)*C24H20B(1-); isopropyl alcohol; potassium hydroxide at 82℃; for 2h; Catalytic behavior; | 100% |
Conditions | Yield |
---|---|
With bromine In 1,4-dioxane; diethyl ether for 0.5h; Ambient temperature; | 100% |
With copper(ll) bromide In ethyl acetate at 60 - 65℃; for 8h; | 99% |
With copper(ll) bromide In ethyl acetate at 60 - 65℃; for 8h; | 99% |
Conditions | Yield |
---|---|
With hydrogen In methanol at 20℃; under 760.051 Torr; for 9h; | 100% |
With hydrogenchloride; ammonium chloride In tetrahydrofuran; water at 45℃; for 2h; Sealed tube; Green chemistry; | 100% |
With hydrogen In water at 50℃; under 750.075 Torr; for 1.5h; | 100% |
(4-nitrophenyl)ethanone
trimethyl orthoformate
1,1-dimethoxy-1-(4-nitrophenyl)ethane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol for 72h; | 100% |
With toluene-4-sulfonic acid In methanol at 20℃; | 95% |
With toluene-4-sulfonic acid In methanol at 20℃; for 48h; | 58% |
4-chlorobenzaldehyde
(4-nitrophenyl)ethanone
3-(4-chlorophenyl)-1-(4-nitrophenyl)-2-propen-1-one
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water at 20℃; for 0.5h; | 100% |
Stage #1: 4-chlorobenzaldehyde; (4-nitrophenyl)ethanone With calcium hydroxyapatite In methanol at 20℃; for 0.0833333h; Stage #2: With water for 1h; Claisen Schmidt condensation; Microwave irradiation; | 93% |
With sodium hydroxide In ethanol at 20℃; | 85% |
ethylene glycol
(4-nitrophenyl)ethanone
2-(4-nitrophenyl)-2-methyl-1,3-dioxolane
Conditions | Yield |
---|---|
With zeolite HSZ-360 In toluene for 1h; Heating; | 100% |
With cyclohexane at 105℃; for 1h; Dean-Stark; | 100% |
With ammonium bisulphate for 6h; Concentration; Reagent/catalyst; Dean-Stark; Reflux; Green chemistry; | 99% |
(4-nitrophenyl)ethanone
4-nitroacetophenone oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In methanol; water Reflux; | 100% |
With hydroxylamine hydrochloride; sodium acetate In methanol Reflux; | 100% |
With N-hydroxyphthalimide In water at 90℃; for 10h; Sealed tube; | 98% |
(4-nitrophenyl)ethanone
(1R)-1-(4-nitrophenyl)ethanol
Conditions | Yield |
---|---|
With (S,S)-RuCl2(2,2'-bis(di-3,5-xylylphosphino)-1,1'-binaphthyl)(1,1-dianisyl-2-isopropyl-1,2-ethylenediamine); potassium tert-butylate; hydrogen In isopropyl alcohol at 26 - 30℃; under 6080 Torr; for 15h; | 100% |
With N(CH2)3CHCPh2OBO(n-Oct) | 100% |
With sodium tetrahydroborate; chloro-trimethyl-silane; polymer-supported chiral sulfonamide In tetrahydrofuran Heating; | 99% |
(4-nitrophenyl)ethanone
(S)-1-[4-nitrophenyl]ethanol
Conditions | Yield |
---|---|
With glucose dehydrogenase; D-glucose; ketoreductase from Pichia glucozyma; nicotinamide adenine dinucleotide phosphate In aq. buffer at 30℃; pH=8; Enzymatic reaction; enantioselective reaction; | 100% |
With D-glucose at 30℃; for 72h; pH=6.5; aq. phosphate buffer; Enzymatic reaction; optical yield given as %ee; enantioselective reaction; | 99% |
With D-glucose In aq. phosphate buffer at 25℃; for 24h; pH=7.0; stereoselective reaction; | 99% |
(4-nitrophenyl)ethanone
9-oxo-4,9-dihydro-pyrazolo[5,1-b]quinazoline-3-carbaldehyde
3-[(E)-3-(4-Nitro-phenyl)-3-oxo-propenyl]-4H-pyrazolo[5,1-b]quinazolin-9-one
Conditions | Yield |
---|---|
With piperidine In acetic acid; benzene for 24h; Heating; | 100% |
Conditions | Yield |
---|---|
With lithium tetrafluoroborate In acetonitrile at 20℃; for 7h; | 100% |
With potassium phtalimide at 20℃; for 1.5h; solvent-free; | 99% |
With rasta resin-PPh3BnCl In chloroform at 50℃; for 1.5h; Inert atmosphere; | 99% |
N-(2-bromobenzyl)-2-aminoethanol
(4-nitrophenyl)ethanone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene cyclocondensation; Heating; | 100% |
With p-toluenesulfonic acid monohydrate In benzene for 12h; Heating; | 100% |
Conditions | Yield |
---|---|
2,6-dimethylpyridine; zinc trifluoromethanesulfonate In dichloromethane at 20℃; for 24h; | 100% |
With C20H32N2O10 In water at 25℃; for 24h; | 97% |
With gadolinium(III) chloride In acetonitrile at 20℃; for 3h; | 85% |
(4-nitrophenyl)ethanone
(E)-N-[4-(1-{diaminomethylene}hydrazono)ethyl]-4-nitrobenzene hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water for 1h; Heating / reflux; | 100% |
formaldehyd
4-benzylpyperidine
(4-nitrophenyl)ethanone
C34H41N3O3
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol Mannich reaction; Heating; | 100% |
4-nitrobenzaldehdye
ethyl 2-cyanoacetate
(4-nitrophenyl)ethanone
2-cyano-3-(4-nitrophenyl)-2-propenoic acid ethyl ester
Conditions | Yield |
---|---|
With SBA-15-supported poly(4-methylvinylpyridinium hydroxide) composite In water Knoevenagel condensation; Reflux; | 100% |
((1E,3E)-4-nitrobuta-1,3-dien-1-yl)benzene
(4-nitrophenyl)ethanone
(S,E)-3-(nitromethyl)-1-(4-nitrophenyl)-5-phenylpent-4-en-1-one
Conditions | Yield |
---|---|
With (S)-di-tert-butyl 2-{3-[(1R,2R)-2-amino-1,2-diphenylethyl]thioureido}succinate In chloroform at 80℃; for 72h; Michael reaction; optical yield given as %ee; enantioselective reaction; | 100% |
With 1-((1R,2R)-2-aminocyclohexyl)-3-(((1R,4aS,10ar)-7-isopropyl-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthren-1-yl)methyl)thiourea; p-Toluic acid In dichloromethane at 25℃; for 168h; Michael Addition; enantioselective reaction; | 80% |
Conditions | Yield |
---|---|
In ethanol for 6h; Reflux; | 100% |
Conditions | Yield |
---|---|
In ethanol for 6h; Reflux; | 100% |
Conditions | Yield |
---|---|
With cyclohexane at 105℃; for 1h; Dean-Stark; | 100% |
Conditions | Yield |
---|---|
Stage #1: 1-bromo-1-propene With magnesium In tetrahydrofuran Stage #2: (4-nitrophenyl)ethanone at 20℃; Cooling with ice; | 100% |
ethane-1,2-dithiol
(4-nitrophenyl)ethanone
2-methyl-2-(4-nitrophenyl)-1,3-dithiolane
Conditions | Yield |
---|---|
With amberlyst-15 In acetonitrile for 1h; | 99.95% |
In hexane for 1h; Reflux; | 99% |
With 9,10-dihydro-10-methylacridine at 50℃; for 36h; Green chemistry; | 86% |
1.3-propanedithiol
(4-nitrophenyl)ethanone
2-methyl-2-(4-nitrophenyl)-1,3-dithiane
Conditions | Yield |
---|---|
With amberlyst-15 In acetonitrile for 1h; | 99.95% |
With sulfamic acid functionalized magnetic Fe3O4 nanoparticles In neat (no solvent) at 25℃; for 2h; | 94% |
With magnesium hydrogen sulfate In acetonitrile at 80℃; for 10h; chemoselective reaction; | 93% |
trimethylsilyl cyanide
(4-nitrophenyl)ethanone
2-(4-nitro-phenyl)-2-hydroxypropanenitrile
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at 20℃; for 18h; | 99.7% |
With titanium tetrachloride In dichloromethane at 20℃; for 18h; | 99.69% |
With titanium tetrachloride 1.) CH2Cl2, 0 deg C; 2.) CH2Cl2, RT, 24 h; | 45% |
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