As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryAbout Product Technical Details Rhodium(III) Chloride Chemical Properties Melting point 450 °C Boiling point 717 °C (730
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryWe provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor uv formulations non-yellowing uv formulations benzene-free uv formulations polymeric uv formul
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiryProduct Name: Rhodium trichloride CAS: 10049-07-7 MF: Cl3Rh MW: 209.26 EINECS: 233-165-4 Mol File: 10049-07-7.mol Rhodium trichloride Structure Rhodium trichloride Chemical Properties Melting point 450 °C Boiling point
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermediat
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Good quantity Storage:R.T. Package:as per buyers Application:Reagent Transportation:by air/sea
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Ocean inorganic department is a professional supplier and exporter engaging in inorganic chemical materials and metal organic compounds. Over the past years, our company is committed to improving the product quality and developing new products, in or
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inquiryConditions | Yield |
---|---|
In neat (no solvent) finely divided metallic Rh is heated in dry Cl2 at to 540 °C ;; | 100% |
In neat (no solvent) Kinetics; exposing Rh to flowing Cl2 (0.05-0.80 atm) at 300-1150°C; | |
In neat (no solvent) rhodium black is heated at 800 °C in dry Cl2 and cooled slowly inflowing Cl2;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
In solid in air or in Ar atmosphere; TG and DTA monitoring, X-ray diffraction anal.; |
rhodium
phosphorus trichloride
rhodium(III)chloride
Conditions | Yield |
---|---|
In neat (no solvent) heating;; | |
In not given heating; | |
In neat (no solvent) heating;; |
phosphorus pentachloride
rhodium
rhodium(III)chloride
Conditions | Yield |
---|---|
In neat (no solvent) heating with Rh;; | |
In not given heating; |
rhodium(III)chloride
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide In propan-1-ol Kinetics; byproducts: CO, CO2, H2O; oxidation of {Rh(CO)2Cl}2 with H2O2 in propanol contg. HCl is investigated, intermediate discussed; reaction monitored by UV/VIS spectroscopy; | |
With hydrogenchloride; dihydrogen peroxide In methanol Kinetics; byproducts: CO, CO2, H2O; oxidation of {Rh(CO)2Cl}2 with H2O2 in methanol contg. HCl is investigated, intermediate discussed; reaction monitored by UV/VIS spectroscopy; | |
With hydrogenchloride; dihydrogen peroxide In ethanol Kinetics; byproducts: CO, CO2, H2O; oxidation of {Rh(CO)2Cl}2 with H2O2 in ethanol contg. HCl is investigated, intermediate discussed; reaction monitored by UV/VIS spectroscopy; |
chlorine
rhodium
sodium chloride
rhodium(III)chloride
Conditions | Yield |
---|---|
In neat (no solvent) mixt. of Rh and NaCl in Cl2 stream (red heat);; |
Conditions | Yield |
---|---|
In neat (no solvent) heating finely divided Rh in a Cl2-stream;; |
B
rhodium(III)chloride
Conditions | Yield |
---|---|
With hydrogenchloride In neat (no solvent) Kinetics; heating in dry HCl-stream; loss of water proceeds slowly at 360 °C, rapidly at 440 °C to form insol. RhCl3;; KCl is leached by water;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
With chlorine In neat (no solvent) Kinetics; dried K3(RhCl6)*H2O (105-110 °C); heating to 440 °C in a dry Cl2-stream;; washing with water;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
In hydrogenchloride byproducts: Cl2; | |
In hydrogenchloride byproducts: Cl2; |
Conditions | Yield |
---|---|
In neat (no solvent) heating RhSn3 to 440 °C in a rapid stream of dry Cl2; air and moisture must be excluded;; Sn contents corresponding to RhSn(<3) causes formation of mixtures of RhCl3 and Rh;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
With air In neat (no solvent) heating RhCl3.aq in air;; | |
heating nerly until the glowing heat;; | |
heating nerly until the glowing heat;; |
A
hydrogenchloride
C
rhodium(III)chloride
Conditions | Yield |
---|---|
With air In neat (no solvent) heating; decomposition;; | A n/a B n/a C 0% |
Conditions | Yield |
---|---|
In neat (no solvent) heating to 175-180 °C in a stream of dry HCl-gas, then to 440 °C in a Cl2-stream, cooling in CO2-stream;; |
Conditions | Yield |
---|---|
In hydrogenchloride prepn. by dissolving Rh2O3 in the least amt. of hot concd. HCl; |
rhodium(III)chloride
Conditions | Yield |
---|---|
With alkali In hydrogenchloride addn. of alkali to Na3(RhCl6)-soln. and dissolving ppt. in HCl;; |
A
rhodium(III)chloride
B
sodium chloride
Conditions | Yield |
---|---|
With hydrogenchloride In neat (no solvent) Kinetics; heating slowly in a stream of dry HCl; dehydration proceeds slowly at 350 °C, rapidly at 440 °C to form insol. RhCl3; by-product NaCl is leached by water;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
With hydrogenchloride; sulfuric acid In not given reacting with concd. H2SO4 leads to rhodium(III) oxide chlorides that were treated with gaseous HCl to yield RhCl3*2/3H2O; heating to 360 °C with HCl gas;; | |
With chlorine In neat (no solvent) Kinetics; Na3(RhCl6)*12H2O is dried at 105-110 °C and then heated to 440 °C in a stream of dry Cl2;; washing with water;; | |
With HCl; H2SO4 In not given reacting with concd. H2SO4 leads to rhodium(III) oxide chlorides that were treated with gaseous HCl to yield RhCl3*2/3H2O; heating to 360 °C with HCl gas;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
With chlorine calcination in dry Cl2;; | |
With chlorine In neat (no solvent) calcination in a dry Cl2-stream;; | |
With Cl2 |
rhodium(III)chloride
Conditions | Yield |
---|---|
With chlorine In neat (no solvent) heating to 440 °C in a stream of dry Cl2;; product does not contain impurities;; | |
With nitrogen In neat (no solvent) calcination in a dry N2-stream;; product does not contain impurities;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
In neat (no solvent) static air atmosphere, 260°C; thermogravimetry; |
B
rhodium(III)chloride
Conditions | Yield |
---|---|
In neat (no solvent) 440°C;; | |
In neat (no solvent) 440°C;; |
rhodium(III)chloride
Conditions | Yield |
---|---|
In hydrogenchloride byproducts: Cl2; |
rhodium(III)chloride
sodium nitrite
Conditions | Yield |
---|---|
With sodium carbonate In hydrogenchloride aq. HCl soln. of RhCl3 partly neutralized by sodium carbonate; to soln. added soln. of NaNO2 and mixt. heated on water bath for 1 h; NH4Cl addedto soln.; ppt. sepd., washed with NH4Cl and min. amt. cold water; dried in air; detn. by XRD; | 99% |
rhodium(III)chloride
tricyclohexylphosphine
HRhCl2(tricyclohexylphosphine)2
Conditions | Yield |
---|---|
In water; isopropyl alcohol bubbled N2 through a stirred soln. of RhCl3; added tricyclohexylphosphine; refluxed for 18 h under stirring; filtered; washed with ethanol; dried in vacuo; | 99% |
3-(2-thiazolylazo)-2,6-diaminopyridine
rhodium(III)chloride
Conditions | Yield |
---|---|
With sodium sulfate In water Kinetics; placing of soln. of 3-(2-thiazolylazo)-2,6-diaminopyridine) and RhCl3 ationic strength I = 1.50 (0.497 M Na2SO4) into tube; addn. of water, pla cing of tube on boiling water bath, heating for 50-60 min, cooling in a wessel with water (10°C); monitoring by UV; | 99% |
rhodium(III)chloride
(C2H5OOC(CH2)3OC6H4)4C20H8N4RhCl
Conditions | Yield |
---|---|
In benzonitrile (N2), porphyrin refluxed in benzonitrile for 5 min, treated with 2 equiv. of RhCl3, refluxed for 3 h; cooled, dried (vac.) with heating,treated with CH2Cl2, washed (aq.NaCl),org. layer dried (Na2SO4), filtered, concd., chromy.(silica gel - CH2Cl 2/EtOH 100:1), elem. anal.; | 98% |
rhodium(III)chloride
potassium iodide
Conditions | Yield |
---|---|
With ethylenediamine In methanol; water RhCl3 and KI are warmed in mixt. of ethylendiamine and water, after cooling methanol is added; washing (methanol), drying (vac.); elem. anal.; | 96% |
Conditions | Yield |
---|---|
With ammonium hydroxide In 1,4-dioxane; water byproducts: HCl; the complex was prepd. by mixing a hot aq. soln. of the metal chloride (4 mmol) with hot dioxane soln. of the ligand (4 mmol); the react. mixt. was then refluxed; aq. ammonia soln. (1:10) was slowly added with stirring (pH 5.0-5.5); the ppt. was filtered, washed with hot dioxane and diethyl ether and dried over anhyd. CaCl2; elem. anal.; | 92% |
glyoxalbis(N-phenyl)osazone
rhodium(III)chloride
triphenylphosphine
trans-Rh(glyoxalbis(N-phenyl)osazone)(PPh3)Cl2
Conditions | Yield |
---|---|
In ethanol (Ar); to soln. of osazone in EtOH, RhCl3 and PPh3 were added, refluxed for 40 min; solid was separated, soln. was cooled at 20°C, filtered, residue was dried in air and collected, elem. anal.; | 92% |
Conditions | Yield |
---|---|
In water pyridine was added to aq. soln. of RhCl3 and heated (water bath) for two hours;; cooling; pptn.; addn. of concd. HCl soln. yields further pptn.; washing (first: concd. HCl soln./H2O / second: H2O); recrystn. (little boiling water); drying (100 °C);; | 90% |
In water byproducts: {Rh py3 Cl3}; pyridine was added to aq. soln. of RhCl3 and heated (water bath) for two hours; pptn. of (Rhpy3Cl3) when heating;; cooling; pptn.; addn. of concd. HCl soln. yields further pptn.; washing (first: concd. HCl soln./H2O / second: H2O); recrystn. (little boiling water); drying (100 °C);; | 90% |
In water byproducts: {Rh py3 Cl3}; pyridine was added to aq. soln. of RhCl3 and heated (water bath) for two hours; pptn. of (Rhpy3Cl3) when heating;; cooling; pptn.; addn. of concd. HCl soln. yields further pptn.; washing (first: concd. HCl soln./H2O / second: H2O); recrystn. (little boiling water); drying (100 °C);; | 90% |
2,3,5,6-tetrakis(2-pyridyl)pyrazine
rhodium(III)chloride
Conditions | Yield |
---|---|
With methanol In methanol mixing of RhCl3 and tppz (2:1 mole ratio) in methanol, refluxing in an open-top condenser, pptn. (after 1 h), further refluxing (24 h), cooling to room temp.; filtration, washing (boiling anhyd. methanol or ethanol), drying (vac.); elem. anal.; | 89% |
Conditions | Yield |
---|---|
In not given bubbling of ethylene through RhCl3 soln. for 22 h; | 86% |
pyridine-4-carboxylic acid
rhodium(III)chloride
trans-[Rh(isonicotinic acid)3(isonicotonic acid(-H))Cl2]
Conditions | Yield |
---|---|
With NaOH In hydrogenchloride; ethanol EtOH soln. of ligand added to aq. HCl soln. of RhCl3, mixt. refluxed with vigorous stirirng; cooled, pH 4.5 (NaOH), ppt. filtered off, washed (hot water, acetone), dried in air, elem. anal.; | 85% |
hydrogenchloride
3-Methylpyridine
hydrazine hydrochloride
water
rhodium(III)chloride
Conditions | Yield |
---|---|
In hydrogenchloride small amt. of hydrazine hydrochloride added to soln. of Rh salt in 0.5 MHCl, heated on water bath, β-picoline added to hot soln. under sti rring, cooled, mixed with equal vol. of concd. HCl; ppt. filtered off, washed with ice water, dried in air; elem. anal.; | 85% |
rhodium(III)chloride
tris(1-methylethyl)phosphine
(((CH3)2CH)3P)2Rh(H)Cl2
Conditions | Yield |
---|---|
In water; isopropyl alcohol bubbled N2 through a stirred soln. of RhCl3 for 1 h; added triisopropylphosphine; refluxed for 33 h under stirring; filtered; washed with acetone; dried in vacuo; | 82% |
ethyleneimine
rhodium(III)chloride
Conditions | Yield |
---|---|
With hydrogenchloride In hydrogenchloride aziridine dissolved in conc. HCl (cooling), addn. of saturated RhCl3 soln. in conc. HCl (molar ratio aziridine:RhCl3 3:1); solvent evapd. on a water bath, crystn., cooled, filtered, residue washed with acetone and ether, dried in vac. (P2O5); elem. anal.; | 80% |
2,3,5,6-tetrakis(2-pyridyl)pyrazine
rhodium(III)chloride
(RhCl3)(2,3,5,6-tetrakis(2-pyridyl)pyrazine)
Conditions | Yield |
---|---|
In ethanol mixing of RhCl3 and tppz (1:2 mole ratio) in ethanol, refluxing in an open-top condenser, pptn. (after 1 h), further refluxing (24 h), cooling to room temp.; filtration, washing (boiling anhyd. methanol or ethanol), drying (vac.); elem. anal.; | 80% |
ammonium tetrafluroborate
rhodium(III)chloride
5-oxa-2,8-dithia[9](2,9)-1,10-phenanthrolinophane
[Rh(5-oxa-2,8-dithia[9](2,9)-1,10-phenanthrolinophane)Cl2]BF4
Conditions | Yield |
---|---|
In water; acetonitrile mixt. of ligand and RhCl3 in MeCN/H2O refluxed under N2 for 5 h, a largeexcess of NH4BF4 added; pptd. by concn. (vac.), recrystd. by slow diffusion of Et2O vapor into an MeCN soln.; | 80% |
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