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Cas:1134-94-7
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inquiry2-(Phenylthio)aniline CAS No.:1134-94-7 Name: 2-(Phenylthio)aniline Synonyms: 2-Aminophenyl phenyl sulfide Molecular Structu
Cas:1134-94-7
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Cas:1134-94-7
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inquiry2-(Phenylthio)aniline Basic information Product Name: 2-(Phenylthio)aniline Synonyms: O-(PHENYLTHIO)ANILINE;2-AMINOPHENYL PHENYL SULFIDE;2-AMINODIPHENYL SULFIDE;2-AMINODIPHENYL SULPHIDE;
Cas:1134-94-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:1134-94-7
Min.Order:1 Kilogram
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Cas:1134-94-7
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:1134-94-7
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inquiryAppearance:gray-brown Crystalline Storage:R T Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Any port in China
Cas:1134-94-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:1134-94-7
Min.Order:1 Kilogram
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inquiry2-(Phenylthio)aniline CAS:1134-94-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
Cas:1134-94-7
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:1134-94-7
Min.Order:1 Kilogram
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inquiryCompany information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big cust
Cas:1134-94-7
Min.Order:1 Kilogram
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Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:1134-94-7
Min.Order:0
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Type:Lab/Research institutions
inquiryProduct Name: 2-(Phenylthio)aniline Synonyms: 2-AMINOPHENYL PHENYL SULFIDE;2-AMINODIPHENYL SULFIDE;2-AMINODIPHENYL SULPHIDE;2-AMINODIPHENYL THIOETHER;2-(PHENYLTHIO)ANILINE;2-AMINODIPHENYL SULFIDE / 2-(PHENYLTHIO)ANILINE;O-(PHENYLTHIO)ANILINE;2-(
Cas:1134-94-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryAppearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application: For Organic Synthesis use Transportation:Common products:Sea/Air/Courier Dangerous Chem:S
Cas:1134-94-7
Min.Order:100 Metric Ton
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Type:Lab/Research institutions
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Cas:1134-94-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:1134-94-7
Min.Order:0 Metric Ton
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Cas:1134-94-7
Min.Order:1 Gram
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Type:Other
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:1134-94-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct name: 2-Amino Diphenyl Sulfide CAS No.:1134-94-7 Molecule Formula:C12H11NS Molecule Weight:201.29 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING
Cas:1134-94-7
Min.Order:1 Kilogram
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Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:1134-94-7
Min.Order:1 Kilogram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:1134-94-7
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
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Cas:1134-94-7
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:1134-94-7
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
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High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Superior quality, moderate price & quick delivery. Appearance:white powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediate
Conditions | Yield |
---|---|
With iron; copper; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; | 99% |
With copper(l) iodide; (S,S)-1,2-diaminocyclohexane In water at 120℃; | 98% |
With 2,2'-biimidazole; copper(II) acetate monohydrate; caesium carbonate In dimethyl sulfoxide at 80℃; for 3h; Ullmann Condensation; Schlenk technique; Inert atmosphere; chemoselective reaction; | 95% |
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydroxide; water; copper(l) chloride at 50℃; for 12h; Inert atmosphere; | 99% |
With copper; caesium carbonate at 140℃; for 6h; Reagent/catalyst; Time; Solvent; Inert atmosphere; | 96% |
With iron(III) chloride; trans-1,2-Diaminocyclohexane; sodium hydroxide In water at 110℃; for 24h; Reagent/catalyst; Solvent; Green chemistry; | 60% |
With iron(III) chloride; (S,S)-1,2-diaminocyclohexane; sodium hydroxide In water at 110℃; for 24h; Reagent/catalyst; Solvent; | 60% |
Conditions | Yield |
---|---|
With hydrogen In methanol under 4137.29 Torr; | 98% |
With ethanol; calcium chloride; zinc for 2h; Reflux; | 94% |
With iron; ammonium chloride In ethanol; water for 1h; Reflux; | 86% |
Conditions | Yield |
---|---|
With (1R,2R)-1,2-diaminocyclohexane; copper(l) chloride In water at 120℃; Schlenk technique; Sealed tube; Inert atmosphere; | 97% |
With copper(l) iodide; (S,S)-1,2-diaminocyclohexane In water at 120℃; | 95% |
With copper(l) iodide; potassium carbonate In 1-methyl-pyrrolidin-2-one at 100℃; for 16h; | 92% |
Conditions | Yield |
---|---|
With copper(l) iodide; N,N'-dihexyloxalamide; potassium tert-butylate In 1,4-dioxane at 110℃; for 24h; Sealed tube; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate In ethanol at 20℃; for 8h; | 82% |
Conditions | Yield |
---|---|
With copper; potassium hydroxide at 110℃; for 12h; Green chemistry; | 80% |
N-phenyl-benzenesulphenamide
A
4-aminophenyl phenyl sulfide
B
2-phenylsulfanyl-aniline
C
2'-(phenylthio)-benzenesulphenanilide
D
diphenyldisulfane
Conditions | Yield |
---|---|
In various solvent(s) at 85℃; for 720h; Further byproducts given; | A 5% B 3% C 4% D 78% |
Conditions | Yield |
---|---|
With potassium tert-butylate In dimethyl sulfoxide at 40 - 80℃; | 76% |
iodobenzene
tert-butylisonitrile
2-amino-benzenethiol
A
2-Phenylbenzothiazole
B
2-phenylsulfanyl-aniline
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; caesium carbonate In N,N-dimethyl-formamide at 120℃; for 24h; Inert atmosphere; | A 61% B 10% |
Conditions | Yield |
---|---|
With C24H22N6Ni; sodium t-butanolate In N,N-dimethyl-formamide; acetonitrile at 80℃; Temperature; Inert atmosphere; Schlenk technique; | 57% |
phenyl trimethylsiloxane
2-Aminophenyl disulfide
2-phenylsulfanyl-aniline
Conditions | Yield |
---|---|
With copper(l) iodide; tetrabutyl ammonium fluoride; johnphos at 100℃; for 24h; | 49% |
methyl-phenyl-thioether
Phenyl azide
A
4-aminophenyl phenyl sulfide
B
2-phenylsulfanyl-aniline
C
2-anilinothioanisole
D
4-(methylsulfanyl)diphenylamine
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trifluoroacetic acid Ambient temperature; | A 33% B 25% C 2% D 10% |
Conditions | Yield |
---|---|
With hydrogenchloride | |
hydrolysis; |
Conditions | Yield |
---|---|
(i) NaOH, EtOH, (ii) H2, Raney-Ni; Multistep reaction; | |
Stage #1: thiophenol; 2-Chloronitrobenzene With sodium hydroxide Stage #2: With hydrogenchloride; iron In methanol |
N-phenyl-benzenesulphenamide
A
4-aminophenyl phenyl sulfide
B
2-phenylsulfanyl-aniline
C
cyclohex-2-enyl phenyl sulfide
D
thiophenol
E
aniline
F
diphenyldisulfane
Conditions | Yield |
---|---|
In cyclohexene under 1 Torr; Product distribution; Mechanism; Irradiation; effect of solvent and lighting on the decomposition; |
α-(phenylthio)benzalphenylhydrazone
A
2-phenylsulfanyl-aniline
B
benzonitrile
Conditions | Yield |
---|---|
With PPA at 110℃; for 6h; |
2'-(phenylthio)-benzenesulphenanilide
A
2-phenylsulfanyl-aniline
B
diphenyldisulfane
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 79 percent / aq. NaOH / ethanol / Heating 2: 50 percent / H2 / 5percent Pd/C / ethanol / 3 h / 2585.7 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 79 percent / aq. NaOH / ethanol / Heating 2: 50 percent / H2 / 5percent Pd/C / ethanol / 3 h / 2585.7 Torr View Scheme |
N-phenyl-benzenesulphenamide
2-phenylsulfanyl-aniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 4 percent / various solvent(s) / 720 h / 85 °C 2: 6 M hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / ethanol / 6 h / Heating 2: polyphosphoric acid / 6 h / 110 °C View Scheme |
N-phenylbenzohydrazonoyl chloride
2-phenylsulfanyl-aniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / ethanol / 6 h / Heating 2: polyphosphoric acid / 6 h / 110 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper powder 2: alcohol; tin dichloride; hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper powder 2: alcohol; tin dichloride; hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper; concentrated KOH-solution / 20 °C / zuletzt bei 170-185grad 2: iron; water; iron chloride View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide / dimethyl sulfoxide / 80 °C 2: hydrogen / methanol / 4137.29 Torr View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium hydroxide / dimethyl sulfoxide / Inert atmosphere; Schlenk technique 1.2: 90 °C / Inert atmosphere; Schlenk technique 2.1: zinc / ethanol; acetic acid / Inert atmosphere; Schlenk technique View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper; concentrated KOH-solution / 20 °C / zuletzt bei 170-185grad 2: iron; water; iron chloride View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide / dimethyl sulfoxide / 80 °C 2: hydrogen / methanol / 4137.29 Torr View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium hydroxide / dimethyl sulfoxide / Inert atmosphere; Schlenk technique 1.2: 90 °C / Inert atmosphere; Schlenk technique 2.1: zinc / ethanol; acetic acid / Inert atmosphere; Schlenk technique View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydroxide / methanol 2: iron; ammonium chloride / water View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper / 300 °C 2: aq.-ethanolic hydrochloric acid View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper / 300 °C 2: aq.-ethanolic hydrochloric acid View Scheme |
2-phenylsulfanyl-aniline
phenyl chloroformate
phenyl [2-(phenylsulphanyl)phenyl]carbamate
Conditions | Yield |
---|---|
Stage #1: 2-phenylsulfanyl-aniline; phenyl chloroformate In toluene at 4℃; for 0.0833333h; Stage #2: phenyl chloroformate With sodium carbonate; sodium hydroxide In water; toluene at 4℃; for 1.5h; | 99.8% |
With sodium carbonate; sodium hydroxide In water; toluene at 5 - 20℃; for 3h; Product distribution / selectivity; | 92% |
With sodium carbonate | 90% |
2-phenylsulfanyl-aniline
Conditions | Yield |
---|---|
Stage #1: 2-phenylsulfanyl-aniline With isopentyl nitrite In tetrahydrofuran at 0℃; Stage #2: With trimethylsilylazide In tetrahydrofuran at 0 - 20℃; under air; | 99% |
With trimethylsilylazide; isopentyl nitrite In tetrahydrofuran at 0 - 20℃; | 90% |
With sulfuric acid; sodium nitrite anschliessendes Behandeln mit Natriumazid; |
2-phenylsulfanyl-aniline
Conditions | Yield |
---|---|
With n-butyllithium In hexane at 20℃; for 1h; Inert atmosphere; Schlenk technique; Reflux; | 99% |
Conditions | Yield |
---|---|
In methanol for 24h; Reflux; | 99% |
2-phenylsulfanyl-aniline
phenyl-2-amine-phenylsulfoxide
Conditions | Yield |
---|---|
With dihydrogen peroxide; Amberlyst 15 In methanol at 20℃; for 5h; | 98% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃; Inert atmosphere; Schlenk technique; | 95% |
With phosphoric acid; oxygen; uranyl(VI) acetate dihydrate In water; acetonitrile at 20℃; under 760.051 Torr; for 12h; Schlenk technique; Irradiation; | 68% |
With dihydrogen peroxide In methanol; water at 60℃; for 3h; | |
With C16H21MoNO9; urea hydrogen peroxide adduct In ethanol at 20℃; for 0.25h; Catalytic behavior; Reagent/catalyst; | 98 %Chromat. |
Conditions | Yield |
---|---|
With urea hydrogen peroxide adduct In ethanol at 20℃; for 0.25h; | 98% |
2-phenylsulfanyl-aniline
ammonium thiocyanate
benzoyl chloride
1-Benzoyl-3-(2-phenylsulfanyl-phenyl)-thiourea
Conditions | Yield |
---|---|
In acetone for 1h; Heating; | 97.1% |
2-phenylsulfanyl-aniline
acetyl chloride
N-(2-(phenylthio)phenyl)acetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at -10 - 20℃; for 5.5h; Inert atmosphere; | 95.6% |
With acetic acid | |
Stage #1: 2-phenylsulfanyl-aniline With triethylamine In dichloromethane for 0.166667h; Cooling with ice; Stage #2: acetyl chloride In dichloromethane for 2.25h; |
Conditions | Yield |
---|---|
With acetic acid for 48h; Reflux; | 95% |
Conditions | Yield |
---|---|
With formic acid In methanol for 24h; | 95% |
In ethanol at 65℃; for 72h; | 30% |
In methanol Reflux; |
2-phenylsulfanyl-aniline
3-nitro-benzaldehyde
phosphonic acid diethyl ester
diethyl α-(3-nitrophenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.1h; Reagent/catalyst; Kabachnik-Fields Reaction; Microwave irradiation; | 93% |
2-phenylsulfanyl-aniline
2,4-dichlorobenzaldeyhde
phosphonic acid diethyl ester
diethyl α-(2,4-dichlorophenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.116667h; Kabachnik-Fields Reaction; Microwave irradiation; | 93% |
2-phenylsulfanyl-aniline
phosphonic acid diethyl ester
4-chloro-3-nitro-benzaldehyde
diethyl α-(4-chloro-3-nitrophenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.1h; Kabachnik-Fields Reaction; Microwave irradiation; | 93% |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 1h; Inert atmosphere; Schlenk technique; | 92% |
Conditions | Yield |
---|---|
With acetic acid; zinc(II) chloride at 60 - 120℃; for 0.5h; | 92% |
2-phenylsulfanyl-aniline
chloroacetyl chloride
2-(N-(chloroacetyl)amine)-1-phenylthio-benzene
Conditions | Yield |
---|---|
In toluene for 0.166667h; Microwave irradiation; | 91% |
2-phenylsulfanyl-aniline
meta-hydroxybenzaldehyde
phosphonic acid diethyl ester
diethyl α-(3-hydroxyphenyl)-α-[2-(phenylthio)phenylamino]methyl phosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.133333h; Kabachnik-Fields Reaction; Microwave irradiation; | 91% |
Conditions | Yield |
---|---|
With acetic acid for 48h; Reflux; | 90% |
2-phenylsulfanyl-aniline
3,4-dimethoxy-benzaldehyde
phosphonic acid diethyl ester
diethyl α-(3,4-dimethoxyphenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.15h; Kabachnik-Fields Reaction; Microwave irradiation; | 90% |
thiophene-2-carbaldehyde
2-phenylsulfanyl-aniline
phosphonic acid diethyl ester
diethyl α-[2-(phenylthio)phenylamino]-α-(2-thienyl)methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.116667h; Kabachnik-Fields Reaction; Microwave irradiation; | 90% |
2-phenylsulfanyl-aniline
vanillin
phosphonic acid diethyl ester
diethyl α-(4-hydroxy-3-methoxyphenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.133333h; Kabachnik-Fields Reaction; Microwave irradiation; | 90% |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 8h; Reflux; | 90% |
Conditions | Yield |
---|---|
With magnesium sulfate In hexane at 20℃; for 12h; Inert atmosphere; | 89% |
2-phenylsulfanyl-aniline
phosphonic acid diethyl ester
syringic aldehyde
diethyl α-(3,5-dimethoxy-4-hydroxyphenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.15h; Kabachnik-Fields Reaction; Microwave irradiation; | 89% |
2-phenylsulfanyl-aniline
4-chlorobenzaldehyde
phosphonic acid diethyl ester
diethyl α-(4-chlorophenyl)-α-[2-(phenylthio)phenylamino]methylphosphonate
Conditions | Yield |
---|---|
With Nano-silica-supported boron trifluoride In neat (no solvent) for 0.15h; Kabachnik-Fields Reaction; Microwave irradiation; | 89% |
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