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Cas:116539-55-0
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inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need CMO
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inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystalline powder Storage:cool dry place Package:25kg/drum Application:pharmaceutical intermediate Transpor
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryDayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:116539-55-0
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inquiry(S)-(-)-N-Methyl-3-hydroxy-3-(2-thienytl)propanamine Chemical name:(S)-(-)-N-Methyl-3-hydroxy-3-(2-thienytl)propanamine Molecular formula:C8H13NOS Molecular weight:171.26 CAS:116539-55-0
Cas:116539-55-0
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:116539-55-0
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:116539-55-0
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inquiryProduct Name: 3-Methylamino-1-(2-thienyl)-1-propanol CAS: 116539-55-0 MF: C8H13NOS MW: 171.26 EINECS: 601-437-5 Mol File: 116539-55-0.mol 3-Methylamino-1-(2-thienyl)-1-propanol Structure 3-Methylamino-1-(2-thienyl)-1-propanol Chem
Cas:116539-55-0
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inquiry(S)-3-(MethylaMino)-1-(2-thienyl)-1-propanol CAS:116539-55-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:116539-55-0
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:116539-55-0
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:116539-55-0
Min.Order:1 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:116539-55-0
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inquiryProName: High quality S)-(-)-N -Methyl-3-Hydrox... CasNo: 116539-55-0 Molecular Formula: C8H13NOS Appearance: white-off powder or granule ( referto ... Application: Duloxetine.HCL DeliveryTime: IN STOCK . PackAge: 25kgs/fiber drum or 200kgs/U
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
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inquiryOur Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci
Cas:116539-55-0
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:116539-55-0
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inquiry3-Methylamino-1-(2-thienyl)-1-propanolAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Inter
Cas:116539-55-0
Min.Order:1 Gram
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Type:Other
inquirySuperior quality, moderate price & quick delivery. Appearance:White Solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:A Duloxetine intermediate. Transportation:as per yo
Cas:116539-55-0
Min.Order:1 Kilogram
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inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
Cas:116539-55-0
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inquiryProduct name: (S)-3-(Methylamino)-1-(2-thienyl)-1-propanol CAS No.: 116539-55-0 Molecule Formula:C8H13NOS Molecule Weight:171.26 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard
Cas:116539-55-0
Min.Order:1 Kilogram
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Type:Trading Company
inquiryC8H13NO2S
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
Stage #1: C8H13NO2S With acetic acid; zinc In water at 50℃; for 1.5h; Stage #2: With sodium hydroxide In water | 100% |
(S)-3-hydroxy-N-methyl-3-(thiophen-2-yl)propanamide
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 20℃; for 4h; Reagent/catalyst; | 98% |
Stage #1: (S)-3-hydroxy-N-methyl-3-(thiophen-2-yl)propanamide With sodium tetrahydroborate; iodine In tetrahydrofuran at 20℃; for 4.33333h; Heating / reflux; Stage #2: With sodium hydroxide; water In tetrahydrofuran; water; butanone at 64℃; for 0.333333h; | 91% |
With lithium aluminium tetrahydride In tetrahydrofuran Heating / reflux; | 80% |
methylamine
(S)-3-hydroxy-3-(2-thienyl)propyl methanesulfonate
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 65℃; for 3h; | 94% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With Rh[((S,S)-BenzP*)(cod)]SbF6; hydrogen; caesium carbonate; zinc(II) chloride In methanol at 20℃; under 19001.3 Torr; for 20h; Reagent/catalyst; Solvent; Autoclave; enantioselective reaction; | 94% |
With hydrogen; potassium carbonate; [Rh{(SC,RP)-duanphos}(norbornadiene)]SbF6 In methanol at 20℃; under 7500.6 Torr; for 12h; | 93% |
With [Rh((S,S)-QuinoxP*)(cod)]SbF6; potassium tert-butylate; hydrogen; zinc(II) iodide In tetrahydrofuran at 25℃; under 15001.5 Torr; for 12h; Reagent/catalyst; enantioselective reaction; | 83% |
(S)-3-(N-trifluoroacetyl-N-methyl)amino-1-(2-thienyl)propan-1-ol
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With water; sodium carbonate In methanol at 20℃; for 4h; | 94% |
(S)-[3-methoxy(methyl)amino]-1-(2-thienyl)propan-1-ol
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With hydrogen; Raney-nickel In methanol at 50℃; for 12h; Autoclave; | 90.8% |
Raney-nickel In methanol at 50℃; for 12h; Autoclave; |
((S)-3-Hydroxy-3-thiophen-2-yl-propyl)-carbamic acid ethyl ester
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 1.5h; Heating; | 88% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water for 0.25h; Product distribution / selectivity; | 87% |
(S)-3-chloro-1-(thiophen-2-yl)propan-1-ol
methylamine
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In methanol; water at 80℃; for 8h; Reagent/catalyst; | 85% |
(S)-3-methyl-6-(2-thienyl)-1,3-oxazinan-2-one
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With water; lithium hydroxide In methanol for 8h; Reflux; | 84% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With methanol; potassium hydroxide at 75℃; for 4h; | 83% |
phenyl (S)-N-[3-acetoxy-3-(thien-2-yl)propyl]-N-methylcarbamate
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With methanol; potassium hydroxide at 75℃; for 4h; | 83% |
S-(-)-3-iodo-1-(2-thienyl)-1-propanol
methylamine
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 25℃; for 12h; Inert atmosphere; | 80% |
In tetrahydrofuran; water for 6h; Ambient temperature; | 71.5% |
In tetrahydrofuran; water at 20℃; for 18h; | 71% |
In tetrahydrofuran | |
In tetrahydrofuran; water at 20℃; for 18h; |
3-(N-methyl-N-benzylamino)-1-(2-thienyl)-2-propen-1-one
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With potassium tert-butylate; hydrogen; [(R)-Binap RuCl2 (R)-DAIPEN] In isopropyl alcohol at 80℃; under 7500.75 Torr; for 16h; Inert atmosphere; | 80% |
(S)-3-dimethylamino-1-(2-thienyl)propan-1-ol
isobutyl chloroformate
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
Stage #1: (S)-3-dimethylamino-1-(2-thienyl)propan-1-ol; isobutyl chloroformate With triethylamine In toluene at 20 - 30℃; for 6h; Stage #2: With potassium hydroxide In methanol at 75℃; for 3.5h; Heating / reflux; | 79.6% |
3-methylamino-1-thiophen-2-yl-propenone
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With hydrogen; potassium carbonate; ruthenium(II) chloride In isopropyl alcohol at 30℃; under 18751.9 Torr; for 18h; | 79.2% |
methylamine
(S)-1-hydroxy-3-(thiophen-2-yl)propanenitrile
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With hydrogen; nickel In methanol; water at 65℃; under 37503.8 Torr; for 24h; Product distribution / selectivity; | 79% |
With hydrogen; 5%-palladium/activated carbon In methanol; water at 60℃; under 75007.5 Torr; for 24h; Product distribution / selectivity; | 74% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 82℃; for 3h; | 74.6% |
A
(S)-3-methylamino-1-(2-thienyl)-1-propanol
B
(R)-3-(methylamino)-1-(thiophen-2-yl)propan-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride Product distribution / selectivity; | A 74% B n/a |
With hydrogen; sodium methylate; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; (S)-(-)-(6,6’-dimethoxybiphenyl-2,2’-diyl)bis(diphenylphosphine) In methanol at 30 - 50℃; under 22502.3 Torr; for 24h; Product distribution / selectivity; | A 12.7 - 20.4 %Chromat. B n/a |
With hydrogen; sodium methylate; ethyl acetoacetate; [(12aS)-6,7-dihudrodibenzo[e,g][1,4]dioxocin-1,12-diyl]bis[diphenylphosphine]; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate In methanol at 50℃; under 22502.3 Torr; for 24h; Product distribution / selectivity; | A 6.2 %Chromat. B n/a |
With hydrogen; [(12aS)-6,7-dihudrodibenzo[e,g][1,4]dioxocin-1,12-diyl]bis[diphenylphosphine]; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In methanol at 50℃; under 22502.3 Torr; for 24h; Product distribution / selectivity; | A 11.6 %Chromat. B n/a |
With hydrogen; [(12aS)-6,7-dihudrodibenzo[e,g][1,4]dioxocin-1,12-diyl]bis[diphenylphosphine]; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate In methanol at 50℃; under 22502.3 Torr; for 24h; Product distribution / selectivity; | A 4 %Chromat. B n/a |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With potassium hydroxide In water | 70% |
With sodium carbonate In water for 0.25h; | 61% |
With sodium hydroxide In water |
(S)-N-(3-hydroxy-3-(thiophen-2-yl)propyl)-N-methylacetamide
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With potassium hydroxide In methanol at 70℃; for 2h; | 68% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With sodium hydroxide In water; iso-butanol | 66% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With bis-[(trifluoroacetoxy)iodo]benzene In water; acetonitrile for 4h; Reflux; | 54% |
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With formic acid; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; triethylamine; N-[(1S,2S)-2-amino-1,2-diphenylethyl]-4-methylbenzenesulfonamide In methanol at 40 - 45℃; for 2h; Time; Reagent/catalyst; | 48% |
(1S,2R)-1-amino-2-indanol
A
(S)-3-methylamino-1-(2-thienyl)-1-propanol
B
(R)-3-(methylamino)-1-(thiophen-2-yl)propan-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide; (p-cymene)-ruthenium(II) chloride dimer In isopropyl alcohol at 20 - 85℃; for 5h; | A 39% B n/a |
3-(methylamino)-1-(thiophen-2-yl)propan-1-ol
A
(S)-3-methylamino-1-(2-thienyl)-1-propanol
B
(R)-3-(methylamino)-1-(thiophen-2-yl)propan-1-ol
Conditions | Yield |
---|---|
With (S)-Mandelic acid In water at 29 - 50℃; | A 27% B n/a |
With diethylamine In ethanol; n-heptane Resolution of racemate; |
(2S,6S)-2-[(S)-1-triisopropylsilyloxyethyl]-3-methyl-6-(thiophen-2-yl)-1,3-oxazinane
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; water at 20℃; for 4h; |
(2S,6S)-2-[(S)-1-triisopropylsilyloxyethyl]-6-(thiophen-2-yl)-[1,3]oxazinan-4-one
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: LiHMDS / tetrahydrofuran / 0 - 20 °C 2: Ph2SiH2 / RhH(CO)(PPh3)3 / tetrahydrofuran / 15 h / 20 °C 3: HCl / H2O; tetrahydrofuran / 4 h / 20 °C View Scheme |
(2S,6S)-N-methyl-2-[(S)-1-triisopropylsilyloxyethyl]-6-(thiophen-2-yl)-[1,3]oxazinan-4-one
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Ph2SiH2 / RhH(CO)(PPh3)3 / tetrahydrofuran / 15 h / 20 °C 2: HCl / H2O; tetrahydrofuran / 4 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 36 percent / BF3*Et2O / CH2Cl2 / -78 - 20 °C 2: aluminum amalgam / propan-2-ol 3: LiHMDS / tetrahydrofuran / 0 - 20 °C 4: Ph2SiH2 / RhH(CO)(PPh3)3 / tetrahydrofuran / 15 h / 20 °C 5: HCl / H2O; tetrahydrofuran / 4 h / 20 °C View Scheme |
1-Fluoronaphthalene
(S)-3-methylamino-1-(2-thienyl)-1-propanol
duloxetine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-Fluoronaphthalene; (S)-3-methylamino-1-(2-thienyl)-1-propanol With sodium hydride In paraffin oil (nujol); dimethyl sulfoxide at 20 - 50℃; Stage #2: With hydrogenchloride; acetic acid In Isopropyl acetate at 0 - 15℃; for 5h; | 93% |
Stage #1: (S)-3-methylamino-1-(2-thienyl)-1-propanol With sodium hydride In dimethyl sulfoxide at 20 - 35℃; Stage #2: 1-Fluoronaphthalene In dimethyl sulfoxide at 45 - 50℃; for 30h; Stage #3: With hydrogenchloride In water; dimethyl sulfoxide; toluene pH=4 - 5; Solvent; |
1-Fluoronaphthalene
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With potassium tert-butylate In dimethyl sulfoxide at 60℃; for 8h; | 90% |
With potassium tert-butylate In dimethyl sulfoxide at 60℃; for 8h; | 90% |
With sodium hydride In dimethyl sulfoxide for 8h; | 81% |
benzenesulfonyl chloride
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 14h; | 90% |
3-fluorobromobenzene
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
Stage #1: (S)-3-methylamino-1-(2-thienyl)-1-propanol With sodium hydride In N,N-dimethyl acetamide; mineral oil at 20℃; for 0.5h; Stage #2: 3-fluorobromobenzene In N,N-dimethyl acetamide; mineral oil at 90℃; for 3h; | 90% |
Stage #1: (S)-3-methylamino-1-(2-thienyl)-1-propanol With sodium hydride In N,N-dimethyl acetamide; mineral oil at 20℃; for 0.5h; Stage #2: 3-fluorobromobenzene In N,N-dimethyl acetamide; mineral oil at 90℃; for 3h; |
(1S)-10-camphorsulfonic acid
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
In ethanol; ethyl acetate at 30 - 50℃; for 0.916667h; Product distribution / selectivity; | 89% |
toluene-4-sulfonic acid
(S)-3-methylamino-1-(2-thienyl)-1-propanol
Conditions | Yield |
---|---|
In methanol; dichloromethane at 25℃; for 1h; Product distribution / selectivity; | 60% |
4-[2-(tert-butyldimethylsilyloxy)ethyl]phenol
(S)-3-methylamino-1-(2-thienyl)-1-propanol
(R)-3-[4-[2-(tert-butyldimethylsilyloxy)ethyl]phenoxy]-N-methyl-3-(thiophen-2-yl)propan-1-amine
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In ethyl acetate; toluene | 52% |
With triphenylphosphine; diethylazodicarboxylate In toluene at 20℃; for 18h; | 52% |
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