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Cas:134-84-9
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inquiryProduct Description Product Name 4-Methylbenzophenone CAS No. 134-84-9 Appearance White powder Assay ≥99% Capacity 500mt/year Min.packing 100gram Applicat
Cas:134-84-9
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inquiryUnique advantages for 4-Methylbenzophenone Cas 134-84-9 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystals or crystalline powder Storage:N/A Package:25kg/drum
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Cas:134-84-9
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Cas:134-84-9
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inquiryProduct Name: 4-Methylbenzophenone Synonyms: P-TOLYL PHENYL KETONE;P-METHYLBENZOPHENONE;PHENYL P-TOLYL KETONE;PHENYL 4-TOLYL KETONE;P-BENZOYL TOLUENE;(4-methylphenyl)phenyl-methanon;4-METHYLBENZOPHENONE;(4-METHYLPHENYL)PHENYLM
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inquiryProduct Name 4-Methylbenzophenone CAS No. 134-84-9 Molecular Formula C14H12O Chemical
Appearance:white to slightly yellow powder Storage:Sealed in dry,Room Temperature Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Any port in China
Cas:134-84-9
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Cas:134-84-9
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Cas:134-84-9
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Cas:134-84-9
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Cas:134-84-9
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Conditions | Yield |
---|---|
With diisopropyl-carbodiimide In toluene at 120℃; for 24h; Inert atmosphere; Sealed tube; | 100% |
With iodic acid In N,N-dimethyl-formamide at 60℃; for 2h; Reagent/catalyst; Temperature; Inert atmosphere; | 99% |
With nickel(II) triflate; cyclohexanone; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 110℃; for 12h; Schlenk technique; | 97% |
2-phenyl-2-p-tolyl-[1,3]dithiolane
4-Methylbenzophenone
Conditions | Yield |
---|---|
With trichloroisocyanuric acid; silver nitrate In water; acetonitrile Ambient temperature; | 100% |
With trimethylsilyl iodide; dimethyl sulfoxide In tetrachloromethane at 75 - 80℃; for 6h; | 96% |
With 2,4,6-triphenylpyrilium perchlorate; oxygen In acetonitrile for 1h; Irradiation; | 92% |
2-(4-methylphenyl)-2-phenyl-1,3-dithiane
4-Methylbenzophenone
Conditions | Yield |
---|---|
With antimonypentachloride In dichloromethane at 0℃; for 0.166667h; | 100% |
With 2,4,6-triphenylpyrilium perchlorate; oxygen In acetonitrile for 2.5h; Irradiation; | 95% |
With 2,4,6-triphenylpyrilium perchlorate; oxygen In acetonitrile for 2.5h; Product distribution; Irradiation; diff. reagent; diff. time; further 1,3-dithianes and 1,3-dithiolanes; | 95% |
Stage #1: 2-(4-methylphenyl)-2-phenyl-1,3-dithiane With chloro-trimethyl-silane; sodium iodide In acetonitrile at 60℃; for 48h; Stage #2: With water In acetonitrile for 0.0833333h; | 54% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine)palladium dichloride In benzene at 85℃; for 3h; | 100% |
Conditions | Yield |
---|---|
With zinc at 71 - 73℃; for 0.00555556h; Friedel-Crafts acylation; microwave irradiation; | 99% |
With copper(II) ferrite In neat (no solvent) at 80℃; for 18h; Friedel-Crafts Acylation; | 98% |
With polystyrene supported aluminium triflate at 20℃; for 1.2h; Friedel-Crafts acylation; Neat (no solvent); regioselective reaction; | 96% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline In N,N-dimethyl-formamide at 60℃; for 15h; Inert atmosphere; | 99% |
With P(p-CH3OC6H4)3; water; dimethyl dicarbonate; palladium diacetate In tetrahydrofuran at 50℃; for 16h; | 87% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); 3-(dicyclohexylphosphino)-2-(2,6-dimethoxyphenyl)-1-methyl-1H-indole In 1,4-dioxane at 100℃; for 6h; Suzuki-Miyaura Coupling; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With oxygen at 110℃; for 8h; Schlenk technique; Green chemistry; | 98% |
With oxygen at 110℃; for 8h; Sealed tube; | 97.8% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at -78 - 20℃; for 1.83333h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With [Pd(η(5)-C5H5)Fe(η(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; potassium carbonate In 1,4-dioxane at 110℃; for 12h; Inert atmosphere; | 98% |
With PEG200; sodium carbonate; palladium diacetate at 60℃; for 2h; Suzuki reaction; | 97% |
With sodium dodecyl-sulfate; potassium carbonate; palladium dichloride In water at 60℃; for 6h; | 88% |
iodobenzene
carbon monoxide
4-methylphenylboronic acid
4-Methylbenzophenone
Conditions | Yield |
---|---|
With (3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; palladium diacetate In tetrahydrofuran at 50℃; for 10h; Suzuki reaction; | 98% |
With tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In methoxybenzene at 100℃; under 760.051 Torr; for 20h; Suzuki carbonylative coupling; chemoselective reaction; | 98% |
With palladium diacetate; sodium carbonate In water at 100℃; under 760.051 Torr; for 7h; Suzuki Coupling; Sealed tube; Autoclave; Green chemistry; | 90% |
Conditions | Yield |
---|---|
With [1-(2,4,6-trimethylbenzyl)-3-(isopropyl)]-benzimidazolin-2-ylidene-[(1,2,5,6-η4)-1,5-cyclooctadiene]chlororhodium(I); water In o-xylene at 120℃; for 1h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 98% |
With 1,3-bis-(diphenylphosphino)propane; water; 1,1'-(1,2-ethanediyl)bisbenzene; chloro(1,5-cyclooctadiene)rhodium(I) dimer In o-xylene at 120℃; |
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Reagent/catalyst; Temperature; Solvent; Suzuki-Miyaura Coupling; | 98% |
With [Pd(1,3-bis (2,6-di-iso-propylphenyl)imiazol-2-ylidene)(cinnamyl)Cl]; water; potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Reagent/catalyst; Temperature; Suzuki-Miyaura Coupling; Inert atmosphere; | 98% |
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
4-methylphenylboronic acid
N-(methylsulfonyl)-N-phenylbenzamide
4-Methylbenzophenone
Conditions | Yield |
---|---|
With (bis(tricyclohexyl)phosphine)palladium(II) dichloride; boric acid; potassium carbonate In tetrahydrofuran at 20 - 120℃; for 15h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
With tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; tricyclohexylphosphine tetrafluoroborate In 1,4-dioxane at 120℃; for 15h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; chemoselective reaction; | 97% |
4-methylphenylboronic acid
N,N-di(tert-butyloxycarbonyl) benzamide
4-Methylbenzophenone
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); water; potassium carbonate In 2-methyltetrahydrofuran at 23℃; for 15h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; Green chemistry; chemoselective reaction; | 98% |
With potassium fluoride; (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II) In water; toluene at 23℃; for 15h; Catalytic behavior; Temperature; Reagent/catalyst; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 94% |
With boric acid; palladium diacetate; potassium carbonate; triethylamine; tricyclohexylphosphine tetrafluoroborate In tetrahydrofuran at 110℃; for 15h; Suzuki-Miyaura Coupling; | 94% |
N-acetyl-N-phenylbenzamide
4-methylphenylboronic acid
4-Methylbenzophenone
Conditions | Yield |
---|---|
With C18H33P*BF3*FH; boric acid; palladium diacetate; potassium carbonate In toluene at 60℃; for 15h; Catalytic behavior; Reagent/catalyst; Solvent; Suzuki-Miyaura Coupling; chemoselective reaction; | 98% |
Conditions | Yield |
---|---|
With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate In 1,4-dioxane at 80℃; for 15h; Reagent/catalyst; Temperature; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
With allylchloro[1,3-bis(2,6-di-isopropylphenyl)imidazol-2-ylidine]palladium(II); potassium carbonate In 1,4-dioxane at 110℃; for 15h; Suzuki-Miyaura Coupling; Sealed tube; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With boric acid; palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In 1,4-dioxane at 120℃; for 15h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With boric acid; palladium diacetate; potassium carbonate; tricyclohexylphosphine tetrafluoroborate In 1,4-dioxane at 120℃; for 15h; Inert atmosphere; | 98% |
N-methoxy-N-methylbenzamide
para-methylphenylmagnesium bromide
4-Methylbenzophenone
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 0.5h; Temperature; Solvent; Inert atmosphere; Schlenk technique; chemoselective reaction; | 98% |
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran at 60℃; for 15h; Catalytic behavior; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
N,N-di(tert-butyloxycarbonyl) benzamide
p-tolylboronic pinacol ester
4-Methylbenzophenone
Conditions | Yield |
---|---|
With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate In tetrahydrofuran; water at 23℃; for 16h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With tert.-butylnitrite; oxygen; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In 1,1,2,2-tetrachloroethane at 130℃; for 8h; Autoclave; | 97% |
With 18-crown-6 ether; potassium tert-butylate; oxygen In N,N-dimethyl-formamide at 0 - 20℃; for 3h; Inert atmosphere; | 95% |
With tert.-butylhydroperoxide; C40H48AuN4(1+)*BF4(1-) In pyridine at 90℃; for 18h; | 95% |
(4-methylphenyl)phenylmethanone oxime
4-Methylbenzophenone
Conditions | Yield |
---|---|
With sodium nitrite In water; acetonitrile at 40℃; for 0.416667h; | 97% |
With periodic acid at 20℃; for 0.3h; | 94% |
With Iron(III) nitrate nonahydrate; oxygen In toluene at 37℃; under 760.051 Torr; for 1.5h; Schlenk technique; Green chemistry; | 92% |
With perchloric acid; N-chloro-3-methyl-2,6-diphenylpiperidin-4-one In ethanol; water for 3h; | 72% |
With manganese triacetate In acetic acid at 28℃; Rate constant; |
Conditions | Yield |
---|---|
With triethylamine; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane at 80℃; for 3h; | 97% |
With tributyl-amine In 1-methyl-pyrrolidin-2-one at 80℃; for 3h; Schlenk technique; Inert atmosphere; | 92% |
With triethylamine; triphenylphosphine; palladium dichloride In 1,4-dioxane at 80℃; for 4h; | 90% |
With palladium 10% on activated carbon; triethylamine; triphenylphosphine In tetrahydrofuran at 80℃; for 3h; Inert atmosphere; | 90% |
para-bromotoluene
phenylglyoxylic acid potassium salt
4-Methylbenzophenone
Conditions | Yield |
---|---|
Stage #1: para-bromotoluene; phenylglyoxylic acid potassium salt With 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-Phenanthroline; palladium(II) hexafluoroacetylacetonate; cyclohexylamine; copper(I) bromide In quinoline at 100℃; for 10h; Inert atmosphere; Molecular sieve; Stage #2: With hydrogenchloride In tetrahydrofuran; quinoline; water at 80℃; for 1h; Inert atmosphere; | 97% |
With quinoline; 1,10-Phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide In 1-methyl-pyrrolidin-2-one at 170℃; for 16h; | 83% |
With 1,10-Phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide; palladium(II) hexafluoroacetylacetonate In 1-methyl-pyrrolidin-2-one; quinoline at 170℃; for 16h; Reflux; | 83% |
With copper(I) oxide; palladium(II) acetylacetonate; copper(l) iodide; 1,10-Phenanthroline In 1-methyl-pyrrolidin-2-one; quinoline at 50 - 190℃; for 0.25h; Inert atmosphere; Microwave irradiation; | 83% |
4-Methylbenzophenone
(4-(azidomethyl)phenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 20℃; for 4.5h; | 100% |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide / tetrachloromethane / 3 h / Inert atmosphere; Reflux; IR irradiation 2: sodium azide / water; acetone / 1 h / Cooling with ice View Scheme | |
Multi-step reaction with 2 steps 1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 24 h / 85 °C 2: sodium azide / acetone; water / 3 h / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 24 h / 85 °C 2: sodium azide / acetone; water / 3 h / 60 °C View Scheme |
4-Methylbenzophenone
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
2-(1-(4-methylphenyl)-1-phenylmethoxy)pinacolborane
Conditions | Yield |
---|---|
With C37H76N6Si6Th In benzene-d6 at 25℃; for 0.166667h; Catalytic behavior; Glovebox; Sealed tube; Schlenk technique; chemoselective reaction; | 100% |
With titanocene bis(catecholborane) In toluene; pentane at 20℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox; | 69% |
With tris[N,N-bis(trimethylsilyl)amide]lanthanum(III) In benzene-d6 at 25℃; for 0.25h; | > 99 %Spectr. |
With C48H57HfN3 In benzene-d6 at 25℃; for 0.25h; Reagent/catalyst; Glovebox; | 99 %Spectr. |
Conditions | Yield |
---|---|
Stage #1: 4-Methylbenzophenone With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; polymethylhydrosiloxane; copper(l) chloride; sodium t-butanolate In toluene at 0℃; for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide; water In ethyl acetate; toluene for 1h; Inert atmosphere; | 99% |
With C33H39Cl2IrOP2; isopropyl alcohol; sodium t-butanolate at 82℃; for 0.5h; air; | 98% |
With ethanol; (ethylenebis(bicyclohexylphosphane))Ni(cis,cis-1,5-cyclooctadiene) In neat (no solvent) at 130℃; for 36h; Catalytic behavior; | 98% |
Conditions | Yield |
---|---|
With KNdF4 for 0.0666667h; Irradiation; | 99% |
With zinc(II) iodide In dichloromethane at 50℃; for 12h; | 76% |
With lithium perchlorate In diethyl ether at 20℃; for 8h; | 61% |
1.3-propanedithiol
4-Methylbenzophenone
2-(4-methylphenyl)-2-phenyl-1,3-dithiane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere; | 99% |
With P-benzyltriphenylphosphonium tribromide at 20℃; for 1.3h; | 93% |
With boron trifluoride diethyl etherate; sodium sulfate In chloroform at 0 - 20℃; Inert atmosphere; | |
With boron trifluoride diethyl etherate In dichloromethane at 20℃; |
4-Methylbenzophenone
trimethylsulphonium iodide
2-(4-methylphenyl)-2-phenyloxirane
Conditions | Yield |
---|---|
With potassium hydroxide In tert-butyl alcohol at 40 - 50℃; for 12h; Corey-Chaykovsky epoxidation; | 99% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 48h; | 98% |
With palladium 10% on activated carbon; water; hydrazine hydrate In ethanol at 100℃; for 24h; Reagent/catalyst; | 97% |
With palladium on carbon; hydrogen In methanol at 20℃; for 16h; | 95% |
4-Methylbenzophenone
ethane-1,2-dithiol
2-phenyl-2-p-tolyl-[1,3]dithiolane
Conditions | Yield |
---|---|
With silica gel; toluene-4-sulfonic acid In dichloromethane for 72h; Heating; | 98% |
With P-benzyltriphenylphosphonium tribromide at 20℃; for 1.3h; | 93% |
With P-benzyltriphenylphosphonium tribromide In dichloromethane at 20℃; for 15h; | 90% |
Nafion-H In benzene Heating; | 85% |
4-Methylbenzophenone
ethyl acetoacetate
malononitrile
6-amino-2,4-dihydro-3-methyl-4-phenyl-4-p-tolylpyrano[2,3-c]pyrazole-5-carbonitrile
Conditions | Yield |
---|---|
With hydrazine hydrate; heptakis(6-amino-6-deoxy)-β-cyclodextrin at 20℃; for 0.0166667h; Neat (no solvent); | 98% |
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