We have the best quality of China,our product exports to all over the world. It is widely used in many different kinds of chemical area. We our quality means the best in China,even all over the world. We can export according to customers’ re
Cas:134-85-0
Min.Order:1 Metric Ton
FOB Price: $1236.0
Type:Trading Company
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:134-85-0
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:134-85-0
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryProduct Description Product Name 4-Chlorobenzophenone CAS No. 134-85-0 Appearance White crystalline powder Assay ≥99% Capacity 1000mt/year Min.packing 100gram
Cas:134-85-0
Min.Order:1 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:134-85-0
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:134-85-0
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:134-85-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAbout Product Details Mol File: 134-85-0.mol
Cas:134-85-0
Min.Order:1 Kilogram
FOB Price: $3.0 / 10.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:134-85-0
Min.Order:1 Gram
FOB Price: $12.0 / 15.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:134-85-0
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:134-85-0
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryProduct name 4-Chlorobenzophenone Appearance white crystals Powder MF C13H9ClO MW 216.
1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla
Cas:134-85-0
Min.Order:100 Gram
Negotiable
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:134-85-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry4-Chlorobenzophenone CAS:134-85-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:134-85-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:134-85-0
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several
Cas:134-85-0
Min.Order:25 Gram
FOB Price: $90.0 / 100.0
Type:Trading Company
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:134-85-0
Min.Order:1 Kilogram
FOB Price: $16.0 / 20.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:134-85-0
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:134-85-0
Min.Order:100 Gram
Negotiable
Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:134-85-0
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:134-85-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediate
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:134-85-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: 4-Chlorobenzophenone Synonyms: para-chlorobenzophenone;p-CBP;p-Chlorodiphenylketone;p-Chlorophenyl phenyl ketone;2-BROMO-1-(4-CHLOROPHENYL)ETHAN-1-ONE;4-CHLORO-2'-BROMINE ACETOPHENONE;4-CHLOROPHENACYL BROMIDE;AKOS 90589 CAS:
Cas:134-85-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With butyltriphenylphosphonium chlorochromate In acetonitrile for 0.75h; Heating; | 100% |
With diisopropyl-carbodiimide In toluene at 120℃; for 24h; Inert atmosphere; Sealed tube; | 100% |
With Montmorillonite K10; ferric nitrate In hexane at 60℃; for 4h; | 99% |
Conditions | Yield |
---|---|
With t-butyl bromide; dimethyl sulfoxide at 70 - 75℃; for 24h; | 100% |
With trimethylsilyl iodide; dimethyl sulfoxide In tetrachloromethane at 75 - 80℃; for 6h; | 99% |
With trichloroisocyanuric acid; silver nitrate In water; acetonitrile Ambient temperature; | 94% |
4-cholorobenzophenone oxime
4-chlorobenzophenone
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In tetrachloromethane for 2h; Product distribution; Heating; other oxidants, various solvents, various times, other temperature; | 100% |
With tert.-butylhydroperoxide In tetrachloromethane for 4h; Heating; | 98% |
With aluminum(III) nitrate nonahydrate; sodium bromide In dichloromethane at 20℃; for 1.75h; | 97% |
Conditions | Yield |
---|---|
With potassium phosphate; 3,3-dimethyl-butan-2-one; C14H10Cl2N2O2Ru; tri tert-butylphosphoniumtetrafluoroborate In water; toluene at 100℃; for 24h; | 100% |
With C35H26NO2PPd; caesium carbonate In toluene for 18h; Reagent/catalyst; Reflux; | 97% |
With [Pd(2-((1-naphthalenyl)methylene)-N-phenylhydrazinecarbothioamide)Cl(PPh3)]; caesium carbonate In toluene at 110℃; for 12h; | 94% |
Conditions | Yield |
---|---|
With pyridine; tert.-butylhydroperoxide; iodine In water at 80℃; chemoselective reaction; | 99% |
With N-Bromosuccinimide; water In chloroform for 3h; Reflux; | 98% |
With pyridine; tert.-butylhydroperoxide; air; K(1+)*AuCl4(1-)*0.5H2O=K[AuCl4]*0.5H2O In decane at 90℃; for 24h; | 96% |
Conditions | Yield |
---|---|
With water; sodium carbonate; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; palladium diacetate at 60℃; for 2h; Suzuki reaction; | 99% |
With C35H35ClFeN3O2PPd; sodium hydrogencarbonate In water; toluene at 50℃; Inert atmosphere; | 99% |
With C42H36ClFeN2O4PPdS*C6H15N; sodium carbonate In water; toluene at 50℃; for 1h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; Sealed tube; | 99% |
Conditions | Yield |
---|---|
With palladium diacetate; N-picolinoylcyclohexylamine; potassium hydrogencarbonate In tert-Amyl alcohol at 150℃; for 24h; | 99% |
4-Chlorophenylboronic acid
N,N-bis(methanesulfonyl)benzamide
4-chlorobenzophenone
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In toluene at 65℃; for 4h; Inert atmosphere; | 99% |
4-chloro-N,N-bis(methanesulfonyl)benzamide
phenylboronic acid
4-chlorobenzophenone
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate In toluene at 65℃; for 0.333333h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Time; Inert atmosphere; | 99% |
1-Chloro-4-iodobenzene
carbon monoxide
trimethyl(phenyl)stannane
4-chlorobenzophenone
Conditions | Yield |
---|---|
bis(η3-allyl-μ-chloropalladium(II)) In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 12h; | 98% |
Conditions | Yield |
---|---|
With potassium fluoride; bis-triphenylphosphine-palladium(II) chloride In acetone for 0.15h; microwave irradiation (525 W); | 98% |
With aluminum oxide; bis-triphenylphosphine-palladium(II) chloride; potassium fluoride In acetone for 0.0833333h; MW-irradiation; | 95% |
With silica-supported diphenylphosphine palladium(0) In tetrahydrofuran at 40℃; for 48h; | 80% |
Conditions | Yield |
---|---|
Stage #1: 4-Chlorophenylboronic acid; benzoic acid anhydride With sodium hydrogencarbonate In water at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: With C19H25Br2N5Pd In water at 20℃; for 36h; Inert atmosphere; | 98% |
With [Pd(η(5)-C5H5)Fe(η(5)-C5H3-C(CH3)=N-C6H4-4-CH3)Cl(P(C6H5)3)]; potassium carbonate In 1,4-dioxane at 110℃; for 12h; Inert atmosphere; | 81% |
With NHC-Pd(II)-Im; sodium hydrogencarbonate In water at 20℃; for 12h; Inert atmosphere; | 52% |
4-chlorobenzophenone
Conditions | Yield |
---|---|
With 2,4,6-triphenylpyrylium tetrafluoroborate at 35℃; for 10h; Irradiation; | 98% |
1-(4-chlorophenyl)-1-phenylethene
4-chlorobenzophenone
Conditions | Yield |
---|---|
With oxygen at 110℃; for 8h; Sealed tube; | 97.2% |
With oxygen at 110℃; for 8h; Schlenk technique; Green chemistry; | 97% |
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at -78 - 20℃; for 1.33333h; Inert atmosphere; | 83% |
1-Chloro-4-iodobenzene
carbon monoxide
phenyl(diisobutyl)aluminium
A
benzophenone
B
4-chlorobenzophenone
Conditions | Yield |
---|---|
dichloro bis(acetonitrile) palladium(II) In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide at 40℃; for 2h; Product distribution; | A 16% B 97% |
1-Chloro-4-iodobenzene
carbon monoxide
phenyllithium
A
benzophenone
B
4-chlorobenzophenone
Conditions | Yield |
---|---|
With diisobutylaluminum chloride; dichloro bis(acetonitrile) palladium(II) In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide at 40℃; under 760 Torr; for 2h; | A 16% B 97% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline In N,N-dimethyl-formamide at 60℃; for 15h; Inert atmosphere; | 97% |
With P(p-CH3OC6H4)3; water; dimethyl dicarbonate; palladium diacetate In tetrahydrofuran at 50℃; for 16h; | 71% |
4-chlorobenzophenone
Conditions | Yield |
---|---|
With benzyltriphenylphosphonium peroxodisulfate In acetonitrile for 0.133333h; Heating; | 97% |
With quinolinium monofluorochromate(VI) In dichloromethane at 20℃; for 1h; | 95% |
With cetyltrimethylammonium peroxodisulphate In acetonitrile for 0.416667h; Reflux; | 95% |
1-Chloro-4-iodobenzene
carbon monoxide
phenylboronic acid
4-chlorobenzophenone
Conditions | Yield |
---|---|
With potassium carbonate under 7500.75 Torr; for 1h; Autoclave; Reflux; | 97% |
With potassium carbonate under 11251.1 Torr; for 0.5h; Suzuki-Miyaura Coupling; Autoclave; Reflux; | 96% |
With potassium phosphate; palladium diacetate at 20℃; under 760.051 Torr; for 20h; | 95% |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Stage #2: 4-chlorobenzaldehyde In tetrahydrofuran; hexane at -78 - 20℃; for 1h; Stage #3: With iodine; potassium carbonate In tert-butyl alcohol for 3h; Reflux; | 97% |
With palladium diacetate; N-picolinoylcyclohexylamine; potassium hydrogencarbonate In tert-Amyl alcohol at 150℃; for 24h; | 82% |
Conditions | Yield |
---|---|
With [Ph2P(ferrocene-1,1′-diyl)ONHCH2CH2NHC(NH2)NH2]Cl*0.4chloroform; palladium diacetate; sodium carbonate In water; toluene at 50℃; for 1h; Schlenk technique; Inert atmosphere; | 97% |
With trans-(Et3NH)2[PdCl2(Ph2Pferrocene-1,1′-diylSO3-κP)2]; sodium phosphate In water; toluene at 50℃; for 3h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; Sealed tube; | 95% |
With palladium 10% on activated carbon; sodium carbonate In water; acetone at 60℃; Suzuki Coupling; Green chemistry; | 93% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; water In chloroform for 3h; Time; Reflux; | 97% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; palladium diacetate; 2-(3,5-dimethyl-1H-pyrazol-1-yl)pyridine In water at 60℃; for 7h; | 97% |
1-Chloro-4-iodobenzene
chromium(0) hexacarbonyl
phenylboronic acid
4-chlorobenzophenone
Conditions | Yield |
---|---|
With sodium t-butanolate In N,N-dimethyl acetamide at 80℃; for 0.25h; Suzuki Coupling; | 97% |
Conditions | Yield |
---|---|
With 3-carboxypyridinium chlorochromate In acetonitrile for 0.0333333h; Product distribution; Further Variations:; Reagents; Temperatures; without microwave irradiation; solvent-free; microwave irradiation; | 96% |
With clay supported ferric nitrate In dichloromethane for 1h; Ambient temperature; | 95% |
With 4-nitrobenzaldehdye; trimethylsilyl trifluoromethanesulfonate In dichloromethane for 3h; Ambient temperature; | 74% |
With bismuth(III) nitrate In acetonitrile for 1h; Heating; | 18% |
Conditions | Yield |
---|---|
With C35H26NO2PPd; caesium carbonate In toluene for 18h; Reagent/catalyst; Reflux; | 96% |
With [Pd(2-((1-naphthalenyl)methylene)-N-phenylhydrazinecarbothioamide)Cl(PPh3)]; caesium carbonate In toluene at 110℃; for 12h; | 94% |
With potassium phosphate; 3,3-dimethyl-butan-2-one; C14H10Cl2N2O2Ru; tri tert-butylphosphoniumtetrafluoroborate In water; toluene at 100℃; for 24h; | 82% |
Conditions | Yield |
---|---|
With lithium acetate; palladium diacetate; triethylamine tris(hydrogen fluoride); tricyclohexylphosphine In 1,4-dioxane; water at 90℃; for 6h; Hiyama Coupling; | 96% |
4-chlorobenzophenone
Conditions | Yield |
---|---|
With benzyltriphenylphosphonium peroxodisulfate In acetonitrile for 0.133333h; Heating; | 95% |
With manganese triacetate In acetic acid at 28℃; Mechanism; Rate constant; |
2-(4-chlorophenyl)-2-phenyl-1,3-dioxolane
4-chlorobenzophenone
Conditions | Yield |
---|---|
With 2,6-dicarboxypyridinium chlorochromate In acetonitrile at 20℃; for 0.25h; | 95% |
With caro's acid; silica gel In acetonitrile at 20℃; for 1h; | 93% |
potassium ferrate(VI); montmorillonite K-10 In dichloromethane for 0.25h; Heating; | 88% |
With K5 In acetone for 1.25h; Heating; | 80% |
Conditions | Yield |
---|---|
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran for 0.666667h; Heating; | 100% |
With [(OC-6-13)-RuCl2[P(p-CH3C6H5)3]2(en)]; potassium tert-butylate; hydrogen In isopropyl alcohol at 35℃; under 6080.41 Torr; for 8h; Catalytic hydrogenation; | 99.8% |
Stage #1: 4-chlorobenzophenone With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; polymethylhydrosiloxane; copper(l) chloride; sodium t-butanolate In toluene at 0℃; for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide; water In ethyl acetate; toluene for 1h; Inert atmosphere; | 99% |
ethane-1,2-dithiol
4-chlorobenzophenone
2-(4-chlorophenyl)-2-phenyl-1,3-dithiolane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere; | 99% |
With silica gel-supported phosphorus pentoxide at 20℃; Neat (no solvent); | 98% |
Nafion-H In benzene Heating; | 80% |
Conditions | Yield |
---|---|
With potassium phosphate monohydrate; 1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; palladium diacetate In 1,4-dioxane at 135℃; for 24h; Suzuki-Miyaura coupling; Inert atmosphere; | 99% |
With 2-chloro-1,3-[di-(2,6-diisopropyl)phenyl]-1,3,2-diazaphospholidine; tris-(dibenzylideneacetone)dipalladium(0); cesium fluoride In 1,4-dioxane at 80℃; for 19h; Suzuki-Miyaura cross-coupling; Inert atmosphere; | 98% |
With {N,N-bis((3,5-dimethylpyrazol-1-yl)methyl)benzylamine}PdCl2; tetrabutylammomium bromide; caesium carbonate In water; N,N-dimethyl-formamide at 120℃; for 5h; Suzuki-Miyaura cross-coupling; | 93% |
Conditions | Yield |
---|---|
With sodium hydride; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; tert-butyl alcohol; bis(acetylacetonate)nickel(II) In tetrahydrofuran at 65℃; | 99% |
With (IPr)Ni(π-allyl)Cl; sodium t-butanolate In tetrahydrofuran at 25℃; for 24h; Buchwald-Hartwig reaction; Inert atmosphere; | 98% |
With [Ni(N,N'-bis[2,6-bis(diphenylmethyl)-4-methoxyphenyl]imidazol-2-ylidene)(allyl)Cl]; sodium t-butanolate In tetrahydrofuran at 60℃; for 2h; Buchwald-Hartwig Coupling; Glovebox; | 97% |
4-chlorobenzophenone
N-methylaniline
(4‐(methyl(phenyl)amino)phenyl)(phenyl)methanone
Conditions | Yield |
---|---|
With sodium hydride; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride; tert-butyl alcohol; bis(acetylacetonate)nickel(II) In 1,4-dioxane at 100℃; | 99% |
With polymethylhydrosiloxane; sodium t-butanolate; bis(acetylacetonate)nickel(II) In 1,2-dimethoxyethane; toluene at 130℃; for 18h; | 94% |
With 2‐(di‐tert‐butylphosphino)‐N,N‐diisopropyl‐5,6‐dimethyl‐1H‐benzo[d]imidazole‐1‐carboxamide; palladium diacetate; potassium carbonate In toluene at 110℃; for 24h; Buchwald-Hartwig Coupling; Schlenk technique; Inert atmosphere; Sealed tube; | 92% |
ethylene glycol
4-chlorobenzophenone
2-(4-chlorophenyl)-2-phenyl-1,3-dioxolane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 40h; Heating; | 99% |
phenyl trimethylsiloxane
4-chlorobenzophenone
biphenyl-4-yl-phenyl-methanone
Conditions | Yield |
---|---|
With 3-(dicyclohexylphosphino)-2-(2-methoxyphenyl)-1-methyl-1-H-indole; tetrabutyl ammonium fluoride; palladium diacetate In toluene at 110℃; for 3h; Hiyama Coupling; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
With tetrabutyl ammonium fluoride; [Pd(dibenzylideneacetone)2] In 1,4-dioxane at 80℃; for 17h; Hiyama cross-coupling; | 65% |
4-bromo-N,N-dimethylaniline
4-chlorobenzophenone
(4'-(dimethylamino)-[1,1'-biphenyl]-4-yl)(phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: 4-bromo-N,N-dimethylaniline With lithium Stage #2: With zinc(II) chloride Stage #3: 4-chlorobenzophenone; nickel phosphine amido pincer complex In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 70℃; for 8h; Negishi cross-coupling; Further stages.; | 99% |
Conditions | Yield |
---|---|
Stage #1: furan With n-butyllithium In diethyl ether Stage #2: With zinc(II) chloride Stage #3: 4-chlorobenzophenone; nickel amido phosphine pincer complex In tetrahydrofuran; diethyl ether at 70℃; for 10h; Negishi cross-coupling; Further stages.; | 99% |
With potassium phosphate; palladium diacetate; CyJohnPhos In 1-methyl-pyrrolidin-2-one at 15 - 100℃; for 24.25h; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With lithium Stage #2: With zinc(II) chloride Stage #3: 4-chlorobenzophenone; nickel phosphine amido pincer complex In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 70℃; for 6h; Negishi cross-coupling; Further stages.; | 99% |
p-tolylzinc(II) chloride
4-chlorobenzophenone
4-benzoyl-4'-methylbiphenyl
Conditions | Yield |
---|---|
With C26H24ClN2NiP*0.1C7H8 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 80℃; for 24h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 99% |
With C38H34Br2N4Ni2P2 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 40℃; for 12h; Reagent/catalyst; Negishi Coupling; Inert atmosphere; Schlenk technique; | 99% |
With C27H22Cl2N3NiP In tetrahydrofuran; 1-methyl-pyrrolidin-2-one for 2h; Schlenk technique; Inert atmosphere; Heating; | 99% |
With Ni(Cl){2-(Ph2P)C6H4NCH(Ph)P(O)Ph2} In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 25℃; for 24h; Negishi coupling reaction; Inert atmosphere; | 98% |
With C21H18N8Ni2O(2+)*2F6P(1-) In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 20 - 80℃; Negishi coupling reaction; | 95% |
1.3-propanedithiol
4-chlorobenzophenone
2-(4-chlorophenyl)-2-phenyl-1,3-dithiane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; Inert atmosphere; | 99% |
With silica gel-supported phosphorus pentoxide at 20℃; Neat (no solvent); | 96% |
With ferric hydrogen sulphate In acetonitrile at 20℃; for 0.133333h; | 91% |
With boron trifluoride diethyl etherate; sodium sulfate In chloroform at 0 - 20℃; Inert atmosphere; |
ethyl acetoacetate
4-chlorobenzophenone
malononitrile
6-amino-4-(4-chorophenyl)-2,4-dihydro-3-methyl-4-phenylpyrano[2,3-c]pyrazole-5-carbonitrile
Conditions | Yield |
---|---|
With hydrazine hydrate; heptakis(6-amino-6-deoxy)-β-cyclodextrin at 20℃; for 0.0166667h; Neat (no solvent); | 99% |
2,6-dimethylbenzene boronic acid
4-chlorobenzophenone
(2',6'-dimethylbiphenyl-4-yl)phenyl-methanone
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate monohydrate; 2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole In 1,4-dioxane at 90℃; for 24h; Suzuki-Miyaura coupling; Inert atmosphere; | 99% |
4-chlorobenzophenone
Conditions | Yield |
---|---|
With potassium phosphate monohydrate; 1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; bis(dibenzylideneacetone)-palladium(0) In toluene; tert-butyl alcohol at 135℃; for 24h; Suzuki coupling; Inert atmosphere; | 99% |
2-furylzinc chloride
4-chlorobenzophenone
Conditions | Yield |
---|---|
With C27H22Cl2N3NiP In tetrahydrofuran; 1-methyl-pyrrolidin-2-one for 1.5h; Inert atmosphere; Schlenk technique; Heating; | 99% |
With C26H24ClN2NiP*0.1C7H8 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 90℃; for 24h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 84% |
p-toluidine
4-chlorobenzophenone
{4-[(4-methylphenyl)amino]phenyl}(phenyl)methanone
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; [1,1′-bis(diphenylphosphino)ferrocene]bis(triphenylphosphite)nickel(0); sodium t-butanolate In toluene at 100℃; for 18h; Schlenk technique; Inert atmosphere; | 99% |
9H-carbazole
4-chlorobenzophenone
[4-(9H-carbazol-9-yl)phenyl](phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: 9H-carbazole With methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 5 - 20℃; for 0.166667h; Inert atmosphere; Stage #2: 4-chlorobenzophenone With PdCl(π-allyl)(cyclohexyl-(1-methyl-2,2-diphenylcyclopropylphophine)) In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 108 - 112℃; for 0.25h; Inert atmosphere; | 99% |
4-chlorobenzophenone
Conditions | Yield |
---|---|
With C60H48BP3Pd; potassium deuteroformate; [2.2.2]cryptande In tetrahydrofuran at 60℃; for 72h; Schlenk technique; Inert atmosphere; | 99% |
With potassium phosphate; d(4)-methanol; palladium diacetate; catacxium A In toluene at 80℃; for 10.5h; | 96% |
With 5%-palladium/activated carbon; triethylamine; deuterium In tetrahydrofuran at 20℃; for 6h; Time; Sealed tube; regiospecific reaction; |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); 3-(dicyclohexylphosphino)-2-(2,6-dimethoxyphenyl)-1-methyl-1H-indole In 1,4-dioxane at 100℃; for 6h; Suzuki-Miyaura Coupling; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With (S,E)-3-methyl-N-phenyl-2-((pyridin-2-ylmethylene)amino)butanamide-UiO-Fe metal-organic framework In tetrahydrofuran at 25℃; for 2h; Inert atmosphere; Glovebox; enantioselective reaction; | 99% |
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