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Cas:2179-57-9
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryItems Standard Result Assay 98%min -----------------------------------------------------------------------------------------------
Cas:2179-57-9
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryProduct Name:Diallyldisulfide CAS No.:2179-57-9 EINECS: 218-548-6 Molecular Formula: C6H10S2 Molecular Weight: 146.27 Appearance:Light Yellow Liquid Appearance:Colorless Clear Liquid Storage:Preserve in well-closed, light-resistant and airtight cont
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inquiryDiallyldisulfide CAS:2179-57-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:2179-57-9
Min.Order:10 Gram
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Type:Trading Company
inquiryAllyl disulfide CAS: 2179-57-9 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The IR spectrum
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Conditions | Yield |
---|---|
With nanophase manganese (VII) oxide coated clay (NM7O coated clay) In toluene at 40℃; for 3h; | 99% |
With water; dihydrogen peroxide In various solvent(s) at 20℃; for 0.166667h; Oxidation; Dimerization; | 94% |
CoCl2 In acetonitrile Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With 1,2-bis(5-methylisoxazol-3-yl)hydrazine; sodium carbonate; thiourea In water; acetonitrile at 80℃; for 2h; | 95% |
With sodium sulfide trihydrate; hexachloroethane at 20℃; for 0.833333h; Reagent/catalyst; | 93% |
With Sodium thiosulfate pentahydrate; water; dimethyl sulfoxide at 50 - 60℃; for 3.5h; pH=< 3; | 91% |
Conditions | Yield |
---|---|
With lithium sulfide; sulfur; cetyl trimethyl ammonium bromide In chloroform; water for 1h; Ambient temperature; | 95% |
With 1,2-bis(5-methylisoxazol-3-yl)hydrazine; sodium carbonate; thiourea In water; acetonitrile at 80℃; for 3h; | 92% |
With sodium sulfide trihydrate; hexachloroethane at 20℃; for 1h; Reagent/catalyst; | 91% |
Conditions | Yield |
---|---|
With tetrachloromethane; water; triethylamine In glycerol at 50℃; for 12h; | 94% |
With sodium carbonate In water; acetonitrile at 80℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With sodium carbonate; sulfur; thiourea In water at 70℃; for 5h; Green chemistry; | 90% |
Conditions | Yield |
---|---|
With sodium carbonate In water; acetonitrile at 80℃; for 3h; | 87% |
Conditions | Yield |
---|---|
With samarium; titanium tetrachloride In tetrahydrofuran at 0℃; | 82% |
S-allyl ethanethioate
diallyl disulphide
Conditions | Yield |
---|---|
Stage #1: S-allyl ethanethioate With hydrogenchloride; water In methanol at 50℃; Stage #2: With iodine In methanol; water at 0℃; for 0.75h; | 82% |
Conditions | Yield |
---|---|
With hydrogen sulfide; dimethyl sulfoxide at 50℃; for 3h; | 76.3% |
Conditions | Yield |
---|---|
With hydrogen sulfide In dimethyl sulfoxide at 40℃; for 3h; | A 11% B 50.8% |
2-(allylthio)benzo[d]oxazole
chloroform
A
benzoxazole
B
diallyl disulphide
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide at 45 - 55℃; for 25h; Rearrangement; disproportionation; | A 37% B 21% C n/a |
2-(allylthio)-1H-benzimidazole
chloroform
A
2-(allylthio)benzo[d]oxazole
B
diallyl disulphide
C
1,2-diallyl sulfanyl-1H-benzoimidazole
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide at 45 - 55℃; for 18h; Rearrangement; substitution; disproportionation; allylation; Further byproducts given; | A 5% B 37% C n/a D n/a |
2-allylmercapto-1,3-benzothiazole
chloroform
A
1,3-Benzothiazole
B
diallyl disulphide
C
diallyl sulphide
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide at 45 - 55℃; for 25h; Rearrangement; disproportionation; Further byproducts given; | A 24% B 24% C 15% D n/a |
2-allylmercapto-1,3-benzothiazole
chloroform
A
1,3-Benzothiazole
B
diallyl disulphide
C
diallyl sulphide
D
2,2'-benzothiazolyl
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide at 45 - 55℃; for 25h; Rearrangement; disproportionation; Further byproducts given; | A 24% B 24% C 15% D 2% |
Conditions | Yield |
---|---|
With diethyl ether; sodium disulfide | |
With carbon disulfide; potassium hydroxide In dimethyl sulfoxide for 2h; | 0.5 g |
Conditions | Yield |
---|---|
With sodium tetrasulfide; diethyl ether |
Conditions | Yield |
---|---|
at 90 - 95℃; |
Conditions | Yield |
---|---|
In dimethyl sulfoxide for 2h; Yield given. Yields of byproduct given; |
S-allyl cysteine
A
diallyl disulphide
B
allicin
C
bis-2-propenyl thiosulfonate
D
sodium pyruvate
Conditions | Yield |
---|---|
With nitrogen(II) oxide In water for 24h; Ambient temperature; Yield given. Yields of byproduct given; |
S-allyl cysteine
A
diallyl disulphide
B
allicin
C
bis-2-propenyl thiosulfonate
D
2-oxo-propionic acid
Conditions | Yield |
---|---|
With nitrogen(II) oxide; trifluoroacetic acid In water for 5h; Mechanism; Ambient temperature; other time; also in absence of CF3COOH; |
allicin
A
3-vinyl-4H-<1,2>-dithiin
B
diallyl disulphide
C
diallyl trisulfide
D
2‐ethenyl‐4H‐1,3‐dithiine
Conditions | Yield |
---|---|
In chloroform-d1 at 25℃; for 144h; | A 0.008 g B 0.03 g C 0.01 g D 0.015 g |
allicin
A
3-vinyl-4H-<1,2>-dithiin
B
diallyl disulphide
C
diallyl trisulfide
D
2‐ethenyl‐4H‐1,3‐dithiine
E
(Z)-ajoene
F
(E)-ajoene
Conditions | Yield |
---|---|
at 37℃; for 48h; Product distribution; other temperatures, other times; |
2-propenyl ethaneimidothiolate hydrobromide
diallyl disulphide
Conditions | Yield |
---|---|
With sodium hydroxide |
benzyl chloride
N-methyl-N-<(2-propenylthio)methylene>methanaminium bromide
A
diallyl disulphide
B
allyl(benzyl)sulfide
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 10h; |
chloroacetic acid ethyl ester
N-methyl-N-<(2-propenylthio)methylene>methanaminium bromide
A
diallyl disulphide
B
ethyl 2-(allylthio)acetate
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 10h; |
N-methyl-N-<(2-propenylthio)methylene>methanaminium bromide
diallyl disulphide
Conditions | Yield |
---|---|
With sodium hydroxide |
N-methyl-N-<(2-propenylthio)methylene>methanaminium bromide
α-bromoacetophenone
A
diallyl disulphide
B
2-(allylthio)-1-phenylethan-1-one
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 10h; |
allyl bromide
A
diallyl disulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
With polysulfide; tetraethylammonium perchlorate In N,N-dimethyl-formamide in situ electrochemical generation of polysulfide from carbon-sulfur cathode; Title compound not separated from byproducts; |
N-allyl isothiocyanate
A
diallyl disulphide
B
diallyl sulphide
C
allyl thiocyanate
D
diallyl trisulfide
E
N,N'-diallylthiourea
Conditions | Yield |
---|---|
In water at 100℃; for 1h; thermal degradation; var. pH; |
diallyl disulphide
3,6-dihydro-[1,2]dithiine
Conditions | Yield |
---|---|
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride at 90℃; | 100% |
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum In benzene-d6 at 20℃; for 1h; Product distribution; further catalyst, variation of the reaction time; catalytic ring-closing metathesis of further acyclic dienes; | 77 % Spectr. |
With bis[1,1-di(trifluoromethyl)ethoxy][(2,6-diisopropylphenyl)imino](2-methyl-2-phenylpropylidene)molybdenum In benzene-d6 at 20℃; for 1h; | 77 % Spectr. |
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In dichloromethane-d2 for 4h; Heating; | 100 % Spectr. |
Conditions | Yield |
---|---|
With 3,3-dimethyldioxirane In acetone at -50 - -20℃; for 0.75h; Product distribution / selectivity; Inert atmosphere; | 96% |
With Peroxyformic acid In methanol at 0℃; for 0.25h; Reagent/catalyst; | 92% |
With peracetic acid; sodium carbonate In chloroform at 0℃; 1.) 30 min; 2.) 30 min; | 90% |
Conditions | Yield |
---|---|
With indium; ammonium chloride In ethanol for 1h; Reduction; Heating; | 95% |
With magnesium In methanol; benzene for 1.66667h; Ambient temperature; | 83% |
diallyl disulphide
3-mercaptopropionic acid
3-(prop-2-en-1-yldisulfanyl)propanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; diethyl ether at 20℃; for 24h; Inert atmosphere; | 92% |
With sodium hydroxide In methanol; diethyl ether at 25℃; for 24.5h; Inert atmosphere; | 84% |
With sodium hydroxide In methanol; diethyl ether at 20℃; for 24h; Inert atmosphere; | 63% |
With sodium hydroxide In methanol; diethyl ether; water at 20℃; for 24h; | 28% |
With sodium hydroxide at 20℃; for 24h; Reflux; Inert atmosphere; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 0.5h; | 89% |
trimethoxysilane
diallyl disulphide
bis-(3-trimethoxysilylpropyl)-disulphide
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; cyclo-octa-1,5-diene In dichloromethane-d2 at 20℃; for 6h; Reagent/catalyst; | 89% |
diallyl disulphide
1,1-dibromo-2,2-dimethylcyclopropane
1-bromo-2,2-dimethylcyclopropyl allyl sulfide
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; diethyl ether 2 h, < -95 deg C, 1.5 h; | 78% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 80℃; for 4h; Inert atmosphere; Sealed tube; | 78% |
1-vinyl-3,4,5-tribromo-1H-pyrazole
diallyl disulphide
Conditions | Yield |
---|---|
Stage #1: 1-vinyl-3,4,5-tribromo-1H-pyrazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.0333333h; Stage #2: diallyl disulphide In tetrahydrofuran; hexane at -78 - 20℃; for 2h; | 77% |
diallyl disulphide
4-t-butylbenzenethiol
B
bis(4-tert-butylphenyl)disulfide
Conditions | Yield |
---|---|
With triethylamine In methanol at 40℃; | A n/a B 20% C 75% |
diallyl disulphide
4-mercaptobenzoic acid
allyl (4-carboxyphenyl)disulfide
Conditions | Yield |
---|---|
With triethylamine at 60℃; for 8h; pH=4; | 74.3% |
diallyl disulphide
4-t-butylbenzenethiol
A
bis(4-tert-butylphenyl)disulfide
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 40℃; | A 71% B 29% |
diallyl disulphide
benzenediazonium tetrafluoroborate
allyl phenyl thioether
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 25℃; for 30h; Inert atmosphere; Green chemistry; | 71% |
diallyl disulphide
valeraldoxime
Conditions | Yield |
---|---|
With N-chloro-succinimide; triethylamine | 68% |
Conditions | Yield |
---|---|
With triethylamine In methanol at 40℃; for 24h; Time; | 68% |
diallyl disulphide
Isobutyl iodide
(E)-3-Allylsulfanyl-1-isobutylsulfanyl-propene
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 40℃; for 2h; | 65.6% |
Conditions | Yield |
---|---|
Stage #1: 4-bromo-1-phenyl-1H-pyrazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.75h; Stage #2: diallyl disulphide In tetrahydrofuran at 0 - 20℃; | 65% |
1-iodo-butane
diallyl disulphide
1-((E)-3-Allylsulfanyl-propenylsulfanyl)-butane
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 40℃; for 2h; | 61.2% |
Conditions | Yield |
---|---|
With bromine In tetrahydrofuran; dichloromethane; benzene | 61% |
Conditions | Yield |
---|---|
With triethylamine In methanol at 40℃; for 24h; Solvent; | 61% |
diallyl disulphide
Conditions | Yield |
---|---|
With pyridine; triphenylphosphine at 20℃; for 24h; | 58% |
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