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Cas:22071-15-4
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inquiryUnique advantages for Ketoprofen Cas 22071-15-4 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or almost white crystalline powder Storage:Store in 0-6°C Package:25kg/d
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Cas:22071-15-4
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inquiryKetoprofen English name ketoprofen Chinese alias: dexketoprofen; ketoprofen CAS: 22071-15-4; 22161-81-5 EINECS 244-759-8 Molecular formula C16H1403 Molecular weight 254.2806 Melting point: 93-96 C Content: 98.5-l0
Henan Tianfu Chemical Co., Ltd. is a modern pharmaceutical enterprise which manufactures APIs and intermediates, such as Ketoprofen, Felbinac, Loxoprofen Sodium, Fosfomycin Calcium, Fosfomycin Sodium, Fosfomycin Trometamol, 2-Thiophene ethylamine, et
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in t
CAS:Hot sale product Ketoprofen CAS 22071-15-4 EINECS:244-759-8 Molecular weight:254.28 Melting point:93-96°C Appearance:White powder Storage:RT. Package:drum Application:Animal Pharmaceuticals Transportation:By sea or by air
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Cas:22071-15-4
Min.Order:25 Kilogram
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Cas:22071-15-4
Min.Order:10 Gram
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Min.Order:10 Gram
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA
Cas:22071-15-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
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Cas:22071-15-4
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Min.Order:1 Kilogram
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Cas:22071-15-4
Min.Order:0 Metric Ton
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Cas:22071-15-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Ketoprofen(KP) CAS: 22071-15-4 Specification Items Specification Result Assay 98.5%-101.0% 99.52% Apperance White or almost white cry
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:22071-15-4
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inquiry1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France etc. 3) OEM/ODM Available;
2-(3-benzoyl-phenyl)-thiopropionic acid S-methyl ester
ketoprofen
Conditions | Yield |
---|---|
With potassium hydroxide In acetone for 2h; Heating; | 100% |
(S)-2-(3-Benzoyl-phenyl)-propionic acid (S)-1-carbamoylmethyl-4,4-dimethyl-2-oxo-pyrrolidin-3-yl ester
ketoprofen
Conditions | Yield |
---|---|
With potassium trimethylsilonate In tetrahydrofuran at 20℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With palladium diacetate; catacxium A In 1,4-dioxane at 100℃; for 20h; | 99% |
With palladium diacetate; catacxium A In 1,4-dioxane at 100℃; for 20h; | 99% |
With hydrogenchloride; water; palladium diacetate; catacxium A In 1,4-dioxane at 100℃; under 30003 Torr; for 20h; regioselective reaction; | 99 %Chromat. |
3-(3-benzoylphenyl)butan-2-one
ketoprofen
Conditions | Yield |
---|---|
With sodium hypochlorite at 70℃; for 0.25h; | 95% |
With sodium hypochlorite Yield given; |
dimethyl 2-methyl-2-(3'-benzoyl)phenylpropanedioate
ketoprofen
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran at 25℃; for 24h; | 95% |
alpha-(m-benzoylphenyl)propionitrile
ketoprofen
Conditions | Yield |
---|---|
With sulfuric acid for 7h; Reflux; | 92.8% |
With sulfuric acid In water; toluene | |
With sodium hydroxide; sulfuric acid In water; toluene | |
With sulfuric acid In water; toluene | |
With sulfuric acid for 7h; Reflux; |
C18H20O3
ketoprofen
Conditions | Yield |
---|---|
Stage #1: C18H20O3 With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide In acetonitrile at 5℃; for 2h; pH=9 - 10; Stage #2: With hydrogenchloride In ethanol; water at 70℃; for 1h; | 91% |
ketoprofen
Conditions | Yield |
---|---|
With nitric acid In 1,4-dioxane at 20℃; for 10h; | 90% |
With nitric acid In 1,4-dioxane at 20℃; for 10h; | 65.6% |
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite In water; acetonitrile at 35℃; for 24h; aq. phosphate buffer; | 40% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; laccase from Trametes versicolor; oxygen In water; acetone at 20℃; for 168h; Enzymatic reaction; | 13% |
S-butyl α-(3-benzoylphenyl)thiopropionate
ketoprofen
Conditions | Yield |
---|---|
With potassium hydroxide In acetone for 2h; Heating; | 89% |
neomenthyldiphenylphosphine
3-benzoylstyrene
sulfuric acid
pentan-3-one
ketoprofen
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide; CO; CuCl2; palladium dichloride In tetrahydrofuran; water; toluene | 88% |
α-(3-benzylphenyl)-propionic acid
ketoprofen
Conditions | Yield |
---|---|
With potassium permanganate; sulfuric acid; triethylamine In water; 1,2-dichloro-ethane at 20℃; for 3.5h; Oxidation; | 86.5% |
With potassium permanganate; sulfuric acid; water for 4h; Reflux; | 2.5 g |
With potassium permanganate; sulfuric acid In water for 6h; Reflux; | 2.5 g |
With potassium permanganate; sulfuric acid In water for 4h; Reflux; | 2.5 g |
With potassium permanganate; sulfuric acid In water for 6h; Reflux; | 2.5 g |
ethyl 2-<3-benzoylphenyl>propionate
ketoprofen
Conditions | Yield |
---|---|
With sodium hydroxide In methanol for 1h; Heating; | 86% |
With potassium hydroxide; water for 2h; Heating; |
3-(1-carboxy-ethyl)-phenyl boronic acid
carbon monoxide
Phenyl triflate
ketoprofen
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium(II) trifluoroacetate In tert-butyl methyl ether at 80℃; under 760.051 Torr; for 6h; Suzuki-Miyaura Coupling; | 86% |
3-(1-carboxy-ethyl)-phenyl boronic acid
carbon monoxide
toluene-4-sulfonic acid phenyl ester
ketoprofen
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; 1,2-bis-(diphenylphosphino)ethane In N,N-dimethyl acetamide at 80℃; under 760.051 Torr; for 6h; Suzuki-Miyaura Coupling; | 83% |
chloroacetic acid ethyl ester
(3-acetylphenyl)(phenyl)methanone
ketoprofen
Conditions | Yield |
---|---|
Stage #1: chloroacetic acid ethyl ester; (3-acetylphenyl)(phenyl)methanone With sodium ethanolate In ethanol Reflux; Stage #2: With sodium hydroxide In ethanol for 2h; Further stages; | 83% |
Stage #1: chloroacetic acid ethyl ester; (3-acetylphenyl)(phenyl)methanone With sodium ethanolate In ethanol for 3h; Reflux; Stage #2: With dihydrogen peroxide; acetic acid at 90℃; for 10h; | 60.1% |
Conditions | Yield |
---|---|
Stage #1: 3-bromobenzophenone With zinc(II) fluoride; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) In toluene for 0.666667h; Inert atmosphere; Stage #2: 1,1-bis(trimethylsilyloxy)prop-1-ene In tetrahydrofuran; N,N-dimethyl-formamide; toluene at 80℃; for 12h; Sealed tube; Inert atmosphere; | 81% |
2-(3-benzoylphenyl)acetonitrile
potassium carbonate
carbonic acid dimethyl ester
A
ketoprofen
B
alpha-(m-benzoylphenyl)propionitrile
Conditions | Yield |
---|---|
A 80% B n/a |
2-(3-benzoylphenyl)acetonitrile
carbonic acid dimethyl ester
A
ketoprofen
B
alpha-(m-benzoylphenyl)propionitrile
Conditions | Yield |
---|---|
With potassium carbonate | A 80% B n/a |
ketoprofen methyl ester
ketoprofen
Conditions | Yield |
---|---|
Stage #1: ketoprofen methyl ester With sodium hydroxide In methanol; water for 1h; Reflux; Stage #2: With hydrogenchloride In water pH=2; | 73.5% |
diphenyl N-<2-(3-benzoylphenyl)-1-pyrrolidinopropylidene>phosphoramidate
ketoprofen
Conditions | Yield |
---|---|
With potassium hydroxide In ethylene glycol for 6h; Heating; | 72% |
2-methyl-3-(5-oxo-5-phenylpentyl)maleic anhydride
ketoprofen
Conditions | Yield |
---|---|
With pyridine hydrochloride at 230℃; for 6h; | 72% |
ketoprofen
Conditions | Yield |
---|---|
With ruthenium trichloride; sodium periodate In tetrachloromethane; water; acetonitrile for 1.25h; Ambient temperature; | 72% |
5-benzoylbenzothiophene-3-carboxylic acid
A
ketoprofen
B
α-(3-benzylphenyl)-propionic acid
C
Dihydroketoprofen
Conditions | Yield |
---|---|
With sodium hydroxide; nickel In ethanol for 1h; Heating; | A 29% B n/a C 56.9% |
carbon monoxide
3-ethynylbenzophenone
A
ketoprofen
B
3-(m-benzoyl-phenyl)-propionic acid
Conditions | Yield |
---|---|
With potassium hydroxide; polyethylene glycol (PEG-400); potassium cyanide; nickel cyanide; cobalt(II) chloride In toluene at 90℃; under 760 Torr; for 24h; | A 55% B 2% |
3-benzoyl-α-chloro-propiophenone
A
1-(3-benzoylphenyl)propan-1-one
B
ketoprofen
Conditions | Yield |
---|---|
With methyloxirane In water; acetone Irradiation; | A 30% B 45% |
ketoprofen
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; laccase from Trametes versicolor; oxygen In water; acetone at 20℃; for 168h; Enzymatic reaction; | 24% |
3-Benzoyl-α-methylphenylessigsaeure-2-oxopropylester
ketoprofen
Conditions | Yield |
---|---|
With buffer pH 8.0 In acetonitrile at 37℃; half-life time of hydrolysis at different pH; |
2-(3-benzoylphenyl)acetonitrile
methyl iodide
A
ketoprofen
B
2-(3-benzoylphenyl)acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide; hydroalcoholic 2N NaOH; tetra(n-butyl)ammonium hydrogensulfate 1.) water-methylene chloride, 10 min, 2.) reflux, 6 h; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
(i) nBuLi, Et2NH, HMPT, THF, (ii) (acid hydrolysis); Multistep reaction; |
methanol
ketoprofen
ketoprofen methyl ester
Conditions | Yield |
---|---|
With sulfuric acid at 50℃; for 8h; Reflux; | 100% |
With sulfuric acid at 50℃; for 8h; | 100% |
With sulfuric acid In acetonitrile at 80 - 85℃; | 99% |
ketoprofen
α-(3-benzylphenyl)-propionic acid
Conditions | Yield |
---|---|
With potassium hydroxide; hydrazine hydrate; diethylene glycol 1.) reflux, 1.5 h, 2.) 195 deg C, 4 h; | 100% |
With 10% palladium on activated charcoal; hydrogen In methanol |
ketoprofen
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.166667h; | 100% |
In acetone at 20℃; for 0.166667h; | 100% |
ketoprofen
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.166667h; | 100% |
ketoprofen
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.166667h; | 100% |
In methanol at 20℃; for 0.166667h; | 100% |
ketoprofen
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.166667h; | 100% |
ketoprofen
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.166667h; | 100% |
In acetone at 20℃; for 0.166667h; | 100% |
ketoprofen
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.166667h; | 100% |
In acetone at 20℃; for 0.166667h; | 100% |
In acetone at 20℃; for 0.166667h; | 100% |
In methanol at 20℃; for 0.5h; |
ketoprofen
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.166667h; | 100% |
ketoprofen
Conditions | Yield |
---|---|
In acetone at 20℃; for 0.166667h; | 100% |
ketoprofen
N-(tert-butyloxycarbonyl)-2-amino-2-(hydroxymethyl)propane-1,3-diol
Conditions | Yield |
---|---|
Stage #1: ketoprofen With triethylamine; dimethylphosphinothioic chloride In dichloromethane for 0.166667h; Cooling with ice; Stage #2: N-(tert-butyloxycarbonyl)-2-amino-2-(hydroxymethyl)propane-1,3-diol With dmap; ammonia; triethylamine In 1,4-dioxane; dichloromethane; water at 20℃; for 0.666667h; | 100% |
ketoprofen
ketoprofen chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride In tetrachloromethane at 40℃; for 0.5h; | 99% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; for 6h; Inert atmosphere; | 98% |
With thionyl chloride In dichloromethane for 3h; | 95% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 5h; | 99% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.75h; Cooling with ice; | 99% |
ketoprofen
N-(tert-butyloxycarbonyl)-L-threonine tert-butyl ester
3-[2(R,S)-(3-benzoyl-phenyl)-propionyloxy]-2(S)-tert-butoxycarbonylamino-butyric acid tert-butyl ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 5h; | 98% |
Conditions | Yield |
---|---|
With (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; oxygen; palladium diacetate; potassium hydrogencarbonate In tert-Amyl alcohol at 90℃; under 760.051 Torr; for 2h; | 98% |
With oxygen; palladium diacetate; potassium hydrogencarbonate; p-benzoquinone In tert-Amyl alcohol at 85℃; under 760.051 Torr; for 48h; regioselective reaction; |
ketoprofen
ethyl acrylate
Conditions | Yield |
---|---|
With (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; oxygen; palladium diacetate; potassium hydrogencarbonate In tert-Amyl alcohol at 90℃; under 760.051 Torr; for 2h; | 98% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; | 98% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; Cooling with ice; | 98% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; | 87% |
Conditions | Yield |
---|---|
With sodium hydroxide In water for 0.5h; | 97% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 18h; Inert atmosphere; | 96.8% |
ketoprofen
S-ketoprofen
Conditions | Yield |
---|---|
96% | |
Multi-step reaction with 3 steps 1.1: oxalyl chloride / 12 h / 40 °C 2.1: rink amide linker modified polystyrene grafted crowns; piperidine; benzotriazolyloxy-tris(dimethylamino)phosphonium(1+) PF6(1-) / diisopropylethylamine / dimethylformamide / 12 h / 20 °C 2.2: triethylamine / tetrahydrofuran / 12 h / 0 °C 2.3: 104 mg / trifluoroacetic acid / CH2Cl2 / 0.67 h 3.1: LiOH / tetrahydrofuran; H2O / 1 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: oxalyl chloride / 12 h / 40 °C 2.1: triethylamine; (S)-(3-OH-4,4-di-Me-2-oxopyrrolidin-1-yl)CH2COOH on resin / tetrahydrofuran / 0 °C 2.2: LiOH*H2O / tetrahydrofuran; H2O / 4 h / 20 °C View Scheme |
ketoprofen
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; | 96% |
(S)-Leu-OMe
ketoprofen
2-[2-(3-benzoylphenyl)propionylamino]-4-methylpentanoic acid methyl ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide; dmap In dichloromethane at 20℃; | 94% |
ketoprofen
1,1'-carbonyldiimidazole
(S)-1-(2-(3-benzoylphenyl)propanoyl)imidazole
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; Inert atmosphere; | 94% |
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