Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Trifluoromethyl iodide 85% 99.5% Iodotrifluoromethane Trifluoroiodomethane cas: 2314-97-8, Please contact us by email freely. We are leadi
Cas:2314-97-8
Min.Order:1 Metric Ton
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:2314-97-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:2314-97-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
Cas:2314-97-8
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:2314-97-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:2314-97-8
Min.Order:1 Kilogram
FOB Price: $290.0 / 590.0
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:2314-97-8
Min.Order:1 Gram
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:2314-97-8
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:2314-97-8
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
Cas:2314-97-8
Min.Order:1 Kilogram
FOB Price: $500.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:2314-97-8
Min.Order:1 Kilogram
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:2314-97-8
Min.Order:4 Kilogram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:2314-97-8
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationships with ma
Cas:2314-97-8
Min.Order:1 Kilogram
FOB Price: $200.0
Type:Lab/Research institutions
inquiryProduct name: Trifluoromethyl Iodide CAS No.:2314-97-8 Molecule Formula:CF3I Molecule Weight:195.91 Purity: 99.0% Package: 25kg/drum Description:White or off-white powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:2314-97-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:2314-97-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryTrifluoromethyl iodide Basic information Product Name: Trifluoromethyl iodide Synonyms: PERFLUOROMETHYL IODIDE;CF3I;CIF3;FIC-1311;Freon13I1;freon13t1;iodotrifluoromethane(trifluoromethyliodide);Methane,trifluoroiodo- CAS: 2314-97-8 MF: C
Cas:2314-97-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:2314-97-8
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:2314-97-8
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Cas:2314-97-8
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:2314-97-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:2314-97-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
ADVANTAGE 1.Professional: More than 10 years chemical exporting experience. We have produced chemical more than fifteen years, 95% products are for export . More than 10 years chemical exporting experience. Good and stabilized factory price. 2.
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:2314-97-8
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryS-(trifluoromethyl)diphenylsulfonium tetrafluoroborate
iodotrifluoromethane
Conditions | Yield |
---|---|
With sodium iodide In acetonitrile for 0.25h; Heating; | 100% |
Conditions | Yield |
---|---|
With iodine byproducts: phophorus iodide; 280°C (48 h); | 95% |
Conditions | Yield |
---|---|
With sodium iodide In acetonitrile at 70℃; for 2h; Inert atmosphere; | 86% |
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 15% |
With iodine monofluoride; palladium on activated carbon; copper on carbon; platinum on activated charcoal at 250 - 550℃; Product distribution / selectivity; Vapor phase; |
tris(trifluoromethyl)arsine
iodine
A
iodotrifluoromethane
B
trifluoromethyl-arsonous acid diiodide
C
iodo-bis-trifluoromethyl-arsine
D
arsenic triiodide
Conditions | Yield |
---|---|
100°C, 48 h; at high temp. more AsI3 and CF3I; | A 80% B 5% C 8% D n/a |
100°C, 48 h; at high temp. more AsI3 and CF3I; | A 80% B 5% C 8% D n/a |
metyhyl chlorodifluoroacetate
A
iodotrifluoromethane
B
carbon dioxide
C
difluorodiiodomethane
D
methyl iodide
Conditions | Yield |
---|---|
With potassium fluoride; copper(l) iodide; iodine In N,N-dimethyl-formamide at 120℃; for 3h; Mechanism; other bromodifluoroacetate deriv.; var. temp. and times of reaction; | A 77% B n/a C 10% D n/a |
metyhyl chlorodifluoroacetate
A
iodotrifluoromethane
B
difluorodiiodomethane
C
methyl iodide
Conditions | Yield |
---|---|
With potassium fluoride; copper(l) iodide; iodine In N,N-dimethyl-formamide at 120℃; for 3h; | A 77% B 10% C n/a |
Conditions | Yield |
---|---|
With lithium iodide at 180℃; for 7h; | 73% |
trifluoroacetyl fluoride
A
iodotrifluoromethane
B
trifluoroacetyl iodide
Conditions | Yield |
---|---|
With lithium iodide at 180℃; for 7h; | A 73% B 26% |
Conditions | Yield |
---|---|
With potassium fluoride; copper(l) iodide; iodine In N,N-dimethyl-formamide at 80℃; for 5h; | A 70% B n/a |
Conditions | Yield |
---|---|
With hydrogen iodide; oxygen at 500℃; Product distribution / selectivity; | 67% |
With oxygen; iodine monofluoride at 550℃; Product distribution / selectivity; | 40% |
With iodine monofluoride at 550℃; Product distribution / selectivity; | 40% |
tris(trifluoromethyl)arsine
methyl iodide
A
trifluoromethan
B
iodotrifluoromethane
C
methylbistrifluoromethylarsine
D
iodo-bis-trifluoromethyl-arsine
E
Trifluormethyl-methyl-iodarsin
Conditions | Yield |
---|---|
235°C, 24 h; no formation of F3CCH3; | A n/a B 64% C n/a D n/a E n/a |
bis(trifluoromethyl)mercury
antimony triiodide
A
iodotrifluoromethane
B
tris(trifluoromethyl)stibane
C
Bis(trifluormethyl)-jodstiban
Conditions | Yield |
---|---|
SbI3 and Hg(CF3)2 heated to 165°C for 8h; at -131°C sepd. (CF3)2SbI and Sb(CF3)3; | A n/a B 63% C 2% |
dichloro-trifluoromethyl-λ3-iodane
silver trifluoroacetate
A
chlorotrifluoromethane
B
iodotrifluoromethane
C
Trifluoromethyliodine(III) bis-trifluoroacetate
Conditions | Yield |
---|---|
In acetonitrile at -40℃; | A n/a B n/a C 56% |
tris(trifluoromethyl)phosphine
methyl iodide
A
iodotrifluoromethane
B
methyl-bis-trifluoromethyl-phosphine
Conditions | Yield |
---|---|
240°C, 24 h; | A n/a B 54% |
tris(trifluoromethyl)stibane
A
iodotrifluoromethane
C
Bis(trifluormethyl)-jodstiban
Conditions | Yield |
---|---|
With iodine shaking in sealed tube for 30 min; | A n/a B 14% C 54% |
With I2 shaking in sealed tube for 30 min; | A n/a B 14% C 54% |
With iodine room temp.; | |
With iodine room temp.; |
iodo-bis-trifluoromethyl-phosphine
A
iodotrifluoromethane
B
Hexafluoroethane
C
trifluoromethyldiiodophosphine
D
tris(trifluoromethyl)phosphine
E
phosphorous triiodide
Conditions | Yield |
---|---|
205°C (48 h); | A 2% B 8% C 2% D 45% E n/a |
trifluoromethyldiiodophosphine
A
iodo-bis-trifluoromethyl-phosphine
B
iodotrifluoromethane
C
tris(trifluoromethyl)phosphine
D
phosphorous triiodide
Conditions | Yield |
---|---|
240°C (48 h); | A 41% B 13% C 23% D n/a |
In neat (no solvent) heating to 240°C;; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 40% |
With iodine heptafluoride; dihydrogen peroxide; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
With dihydrogen peroxide; iodine pentafluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 40% |
With iodine heptafluoride; dihydrogen peroxide; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
With dihydrogen peroxide; iodine pentafluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 40% |
With iodine heptafluoride; dihydrogen peroxide; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
With dihydrogen peroxide; iodine pentafluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 40% |
With iodine heptafluoride; dihydrogen peroxide; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
With dihydrogen peroxide; iodine pentafluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
trifluoromethyl disulphide
iodotrifluoromethane
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 40% |
With iodine heptafluoride; dihydrogen peroxide; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
With dihydrogen peroxide; iodine pentafluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 30% |
tris(trifluoromethyl)phosphine
iodine
A
iodo-bis-trifluoromethyl-phosphine
B
iodotrifluoromethane
C
trifluoromethyldiiodophosphine
D
phosphorous triiodide
Conditions | Yield |
---|---|
180°C, 24 h; | A 16% B 34% C 4% D n/a |
tris(trifluoromethyl)arsine
A
iodotrifluoromethane
B
trifluoromethyl-arsonous acid diiodide
C
iodo-bis-trifluoromethyl-arsine
Conditions | Yield |
---|---|
100-105°C, 72 h; | A 28% B n/a C 22% |
Conditions | Yield |
---|---|
With hydrogen; iodine monofluoride; 3 weight% Pd/C In dimethyl sulfoxide; N,N-dimethyl-formamide at 100℃; Product distribution / selectivity; | 20% |
With iodine monofluoride; zinc; 3 weight% Pd/C In dimethyl sulfoxide; N,N-dimethyl-formamide at 100℃; Product distribution / selectivity; | 20% |
With iodine Product distribution; Irradiation; thermal + multiple photon IR laser excitation; different laser energy fluence and temperatures; |
tris(trifluoromethyl)arsine
methyl iodide
A
iodotrifluoromethane
B
Hexafluoroethane
C
methylbistrifluoromethylarsine
Conditions | Yield |
---|---|
Irradiation (UV/VIS); with UV-light; | A 18% B 15% C n/a |
CF13IO2Te2
A
carbon tetrafluoride
B
iodotrifluoromethane
C
CF8OTe
Conditions | Yield |
---|---|
at 25℃; for 2h; | A n/a B n/a C 17% D n/a |
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 15% |
With potassium iodide at 200℃; | |
With iodine monofluoride; palladium on activated carbon; copper on carbon; platinum on activated charcoal at 250 - 550℃; Product distribution / selectivity; Vapor phase; | |
With hydrogen iodide at 350℃; for 0.00555556h; Catalytic behavior; Reagent/catalyst; | 65.19 %Chromat. |
With 0.5% Pd/Al2O3; hydrogen; iodine at 150 - 350℃; Flow reactor; |
(trifluoromethyl)trimethylsilane
iodotrifluoromethane
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 15% |
With iodine; oxygen; palladium on activated charcoal at 350℃; Product distribution / selectivity; | |
With sulfuric acid; iodine; oxygen; bis(acetylacetonate)oxovanadium In Hexafluorobenzene at 30 - 150℃; for 12h; Product distribution / selectivity; | |
With iodine monofluoride; palladium on activated carbon; copper on carbon; platinum on activated charcoal at 250 - 550℃; Product distribution / selectivity; Vapor phase; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; iodine monofluoride; bis(acetylacetonate)oxovanadium In water Product distribution / selectivity; Heating / reflux; | 15% |
With iodine monofluoride; palladium on activated carbon; copper on carbon; platinum on activated charcoal at 250 - 550℃; Product distribution / selectivity; Vapor phase; |
iodotrifluoromethane
perfluoro-NN'-dimethylethane-1,2-bis(amino-oxyl) diradical
Conditions | Yield |
---|---|
for 24h; Irradiation; | 100% |
iodotrifluoromethane
tetramethylammonium fluoride
(trifluoromethyl)trimethylsilane
Conditions | Yield |
---|---|
In tetrahydrofuran at -60℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With Tetrakis(dimethylamino)ethylen In N,N-dimethyl-formamide at 0 - 20℃; for 12h; | 100% |
With Tetrakis(dimethylamino)ethylen In N,N-dimethyl-formamide at 0 - 20℃; |
iodotrifluoromethane
1-Isopropyl-5-methoxy-2-(toluene-4-sulfonyl)-4-trifluoromethyl-benzene
Conditions | Yield |
---|---|
Stage #1: 1-iodo-4-isopropyl-2-methoxy-5-(toluene-4-sulfonyl)-benzene With potassium fluoride; copper(l) iodide In DMF (N,N-dimethyl-formamide) at 120℃; Stage #2: iodotrifluoromethane In DMF (N,N-dimethyl-formamide) for 4.5h; | 100% |
With potassium fluoride; copper(l) iodide In N,N-dimethyl-formamide at 20℃; for 4.5h; | 100% |
Conditions | Yield |
---|---|
In acetonitrile byproducts: EtI; Ar-atmosphere; stirring (-23°C); evapn. (vac.); | 100% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With potassium fluoride; copper(l) iodide In N,N-dimethyl-formamide at 120℃; for 4h; | 100% |
With potassium fluoride; copper(l) iodide In N,N-dimethyl-formamide at 120℃; for 4.5h; | 100% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With paraquat dichloride; triethylamine In N,N-dimethyl-formamide at -78 - 20℃; for 18h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
at -78℃; for 0.333333h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
at -78℃; for 0.333333h; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
at -78 - 23℃; Schlenk technique; Inert atmosphere; | 100% |
at -78 - 23℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
at -78 - 23℃; Schlenk technique; Inert atmosphere; | 100% |
at -78 - 23℃; Inert atmosphere; | 100% |
at -78℃; |
iodotrifluoromethane
Conditions | Yield |
---|---|
With paraquat dichloride; triethylamine In N,N-dimethyl-formamide at -78 - 20℃; for 24h; | 99.6% |
iodotrifluoromethane
diphenyl diselenide
phenyl trifluoromethylselenide
Conditions | Yield |
---|---|
With Tetrakis(dimethylamino)ethylen In N,N-dimethyl-formamide at 0 - 20℃; | 99% |
With rongalite In water; N,N-dimethyl-formamide at 20℃; | 28% |
With Tetrakis(dimethylamino)ethylen In N,N-dimethyl-formamide at 0 - 20℃; |
Conditions | Yield |
---|---|
In chloroform byproducts: EtI; 2.5 equiv. CF3I, -40°C, 10 min (pptn.); removal of volatiles (vac.); | 99% |
In not given absence of air and moisture; in presence of 1 equiv. HCF2I; |
iodotrifluoromethane
triluoromethyl(triphenylphosphine)gold(I)
Conditions | Yield |
---|---|
In dichloromethane byproducts: MeI; 4 equiv. of CF3I, standing in sealed tube at 35°C for 45 min; evapn.; elem. anal.; | 99% |
iodotrifluoromethane
1-(8-Bromo-7-methoxy-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepin-3-yl)-2,2,2-trifluoro-ethanone
2,2,2-Trifluoro-1-(7-methoxy-1-phenyl-8-trifluoromethyl-1,2,4,5-tetrahydro-benzo[d]azepin-3-yl)-ethanone
Conditions | Yield |
---|---|
With copper In N,N-dimethyl-formamide at 150℃; | 98% |
iodotrifluoromethane
1-(8-Bromo-6-chloro-7-methoxy-1-phenyl-1,2,4,5-tetrahydro-benzo[d]azepin-3-yl)-2,2,2-trifluoro-ethanone
1-(6-Chloro-7-methoxy-1-phenyl-8-trifluoromethyl-1,2,4,5-tetrahydro-benzo[d]azepin-3-yl)-2,2,2-trifluoro-ethanone
Conditions | Yield |
---|---|
With copper In N,N-dimethyl-formamide at 150℃; | 98% |
Conditions | Yield |
---|---|
With fac-tris(2-phenylpyridinato-N,C2')iridium(III); 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran; acetonitrile at 20℃; Sealed tube; Inert atmosphere; Irradiation; diastereoselective reaction; | 98% |
Conditions | Yield |
---|---|
With pyrrolidine; Diphenylacetaldehyde In dichloromethane at 20℃; for 16h; Inert atmosphere; Irradiation; | 98% |
With Eosin Y; sodium thiosulfate In acetonitrile at 20℃; for 1h; Inert atmosphere; Irradiation; | 53% |
Conditions | Yield |
---|---|
With 5,10-di(4-trifluoromethylphenyl)-5,10-dihydrophenazine; potassium formate In N,N-dimethyl acetamide at 40℃; for 6h; Irradiation; | 98% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine In dimethyl sulfoxide at 20℃; for 36h; Schlenk technique; Irradiation; | 98% |
Conditions | Yield |
---|---|
With platinum(II) (2-phenylpyridinato-N,C(2'))(2,4-pentanedionato-O,O); 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 6h; Quantum yield; Sealed tube; Irradiation; Inert atmosphere; | 97% |
With tris(1,10-phenanthroline)ruthenium(II) dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 2h; Solvent; Inert atmosphere; | 96% |
With tris(1,10-phenanthroline)ruthenium(II) dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; Inert atmosphere; Irradiation; regioselective reaction; | 95% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene; tri-(9-anthryl)borane In acetonitrile at 20℃; for 3h; Reagent/catalyst; Solvent; Wavelength; Inert atmosphere; Irradiation; | 93% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; eosin y In N,N-dimethyl-formamide at 20℃; for 0.5h; Reagent/catalyst; Concentration; Solvent; Time; Inert atmosphere; Irradiation; | 97% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine In dimethyl sulfoxide at 20℃; for 36h; Schlenk technique; Irradiation; | 97% |
Conditions | Yield |
---|---|
With (dppf)Ni(o-tol)Cl; sodium t-butanolate In Hexafluorobenzene at 50℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube; | 97% |
iodotrifluoromethane
(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-bromo-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate
(2R,3R,4R,5R)-2-(acetoxymethyl)-5-(6-(trifluoromethyl)-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate
Conditions | Yield |
---|---|
With copper(l) iodide; zinc In N,N-dimethyl-formamide at 70℃; for 10h; | 96% |
iodotrifluoromethane
2-iodo-5-bromopyridine
zinc
5-bromo-2(trifluoromethyl)pyridine
Conditions | Yield |
---|---|
Stage #1: iodotrifluoromethane; zinc With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone at 20℃; for 2h; Inert atmosphere; Stage #2: 2-iodo-5-bromopyridine With copper(l) iodide at 50℃; for 24h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With platinum(II) (2-phenylpyridinato-N,C(2'))(2,4-pentanedionato-O,O); 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; Sealed tube; Irradiation; Inert atmosphere; | 96% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; eosin y In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; Irradiation; | 96% |
iodotrifluoromethane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; eosin y In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; Irradiation; | 96% |
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