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inquiryName: 2-Iodobenzaldehyde Synonyms: Benzaldehyde, 2-iodo- CAS: 26260-02-6 MF: C7H5IO Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum Application:Intermediate of synthetic
2-IODOBENZALDEHYDE CAS:26260-02-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryBenzaldehyde, 2-iodo- 2-Iodobenzaldehyde CAS No.: 26260-02-6 Synonyms: iodobenzaldehyde; Benzaldehyde, 2-iodo-; O-IODOBENZALDEHYDE; 2-iodobenzenealdehyde; Benzaldehyde,2-iodo; ortho-iodobenzaldehyde; Formula: C7H5IO Exact Mass: 231.939
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inquiryProduct Name: 2-IODOBENZALDEHYDE Synonyms: 2-IODOBENZALDEHYDE;2-Iodobenzaldehyde o-Iodobenzaldehyde;2-Iodobenzaldehyde,98%;o-Iodobenzaldehyde;Benzaldehyde, 2-iodo-;2-Iodobenzaldehyde 97% CAS: 26260-02-6 MF: C7H5IO MW: 232.02 EINECS:
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Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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2-iodobenzyl alcohol
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With manganese(IV) oxide In chloroform at 20℃; for 70h; | 99% |
With 1-methyl-1H-imidazole; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; 4,4'-Dimethoxy-2,2'-bipyridin; 9-azabicyclo[3.3.1]nonane N-oxyl; oxygen In acetonitrile at 20℃; for 1h; | 98% |
With silica gel; pyridinium chlorochromate In dichloromethane at 20℃; Inert atmosphere; | 98% |
ortho-bromobenzaldehyde
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With copper(l) iodide; Trimethylenediamine; sodium iodide In 1,4-dioxane for 24h; Finkelstein Reaction; Reflux; Inert atmosphere; | 99% |
Multi-step reaction with 3 steps 1: 83 percent / TsOH / 5 h / Heating 2: 1.) Grignard reagent, 2.) I2 / 1.), 2.) THF 3: 83 percent / aq. HCl / tetrahydrofuran / 20 h / Ambient temperature View Scheme | |
With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine In 1,4-dioxane at 120℃; under 1500.15 Torr; for 24h; Reagent/catalyst; Finkelstein Reaction; Autoclave; Inert atmosphere; Schlenk technique; |
(2-iodophenyl)methyl acetate
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With methanol; potassium permanganate In ethyl acetate at 25℃; for 14h; | 98% |
Multi-step reaction with 2 steps 1: aqueous KOH 2: AgNO3; Na2S2O8; water View Scheme |
2-bromobenzaldehyde diethyl acetal
2-iodobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-bromobenzaldehyde diethyl acetal With n-butyllithium In tetrahydrofuran; hexane at -78 - -10℃; for 1.41667h; Stage #2: With iodine In tetrahydrofuran; hexane at -78 - 20℃; for 12.6667h; | 98% |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 94% |
2-Iodobenzoic acid
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With manganese(IV) oxide; borane-THF Inert atmosphere; | 90% |
Multi-step reaction with 2 steps 1: 40 percent / HCl / 30 h / Heating 2: 34 percent / diisobutylaluminum hydride / toluene / 2 h / -60 °C View Scheme | |
Multi-step reaction with 2 steps 1: 67 percent / SOCl2, DMF / 2 h / Heating 2: tert-butyl alcohol, LiAlH4 / bis-(2-methoxy-ethyl) ether / -78 - 20 °C View Scheme |
2-Iodo-N-methyl-N-phenylbenzamide
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With zirconocene dichloride; lithium tri-t-butoxyaluminum hydride In tetrahydrofuran at 20℃; for 0.116667h; Inert atmosphere; | 90% |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 90% |
Multi-step reaction with 2 steps 1: acetonitrile / 10 h / 20 °C / pH 5 2: Iodine monochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 89% |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With Iodine monochloride In dichloromethane at 20℃; for 2h; Inert atmosphere; | 85% |
Multi-step reaction with 2 steps 1: acetonitrile / 10 h / 20 °C / pH 5 2: Iodine monochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme |
2-iodobenzaldehyde ethylene glycol ketal
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 20h; Ambient temperature; | 83% |
2-formylbenzene boronic acid
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With perfluoroisopropyl iodide; copper; hydroquinone In N,N-dimethyl-formamide at 20℃; for 24h; | 83% |
2-iodo-N-methoxy-N-methyl-benzamide
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In tetrahydrofuran; hexane at -78℃; for 2h; Inert atmosphere; | 77% |
C13H20IN
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; sodium hydrogencarbonate In chloroform at 60℃; for 2h; Polonovski type reaction; | 75% |
2-(2'-formylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With copper(I) oxide; 1,10-Phenanthroline; potassium iodide In methanol; water at 80℃; for 1h; High pressure; | 70% |
With copper(I) oxide; 1,10-Phenanthroline; potassium iodide In methanol; water at 80℃; for 1h; Sealed tube; | 65% |
o-iodo-methyl-benzoic acid
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In toluene at -60℃; for 2h; | 34% |
ortho-methylphenyl iodide
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With sulfuric acid bei der elektrolytischen Oxydation; | |
Multi-step reaction with 4 steps 1: tetrachloromethane; dibenzoyl peroxide; N-bromo-succinimide 2: acetic acid 3: aqueous KOH 4: AgNO3; Na2S2O8; water View Scheme |
2-iodobenzonitrile
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether; tin(ll) chloride anschl. mit H2O; |
2-Iodobenzyl bromide
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With chloroform; hexamethylenetetramine Erhitzen des Reaktionsprodukts mit wss. Essigsaeure; | |
Multi-step reaction with 3 steps 1: acetic acid 2: aqueous KOH 3: AgNO3; Na2S2O8; water View Scheme |
benodanil
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With phosphorus pentachloride; toluene at 100℃; Erwaermen des Reaktionsprodukts mit SnCl2 und aether. HCl und anschliessendes Behandeln mit Wasser; |
2-Iodobenzoyl chloride
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With tetrahydrogenoboratebis(triphenylphosphine)copper(I); triphenylphosphine In acetone for 1h; | 17.2 g |
Multi-step reaction with 2 steps 1: 98 percent / sodium borohydride / dioxane / 1 h / steam-bath 2: 76.4 percent / pyridinium dichromate / CH2Cl2 / 3 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 2: toluene; PCl5 / 100 °C / Erwaermen des Reaktionsprodukts mit SnCl2 und aether. HCl und anschliessendes Behandeln mit Wasser View Scheme |
2-iodobenzylamine
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With N-bromoacetamide In water at 14.9 - 34.9℃; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
In acetic acid at 19.9℃; Rate constant; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.), ΔG(excit.), var. temp.; |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; tert-butyl alcohol In diethylene glycol dimethyl ether at -78 - 20℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
ortho-methylphenyl iodide
sulfuric acid
A
2-Iodobenzoic acid
B
2-iodobenzaldehyde
Conditions | Yield |
---|---|
bei der elektrolytischen Oxydation; |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With potassium iodide | |
With potassium iodide |
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With potassium permanganate |
(2-iodo-benzylidene)-malonic acid
water
A
malonic acid
B
carbon dioxide
C
2-iodobenzaldehyde
D
(E)-3-(2-Iodophenyl)propenoic acid
2-(2-bromophenyl)-1,3-dioxolan
2-iodobenzaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) Grignard reagent, 2.) I2 / 1.), 2.) THF 2: 83 percent / aq. HCl / tetrahydrofuran / 20 h / Ambient temperature View Scheme |
2-iodobenzaldehyde
2-(3,4-dimethoxyphenyl)-ethylamine
2-iodobenzaldehyde
phenylhydrazine
2-iodo-benzaldehyde phenylhydrazone
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 160℃; for 0.166667h; microwave irradiation; | 100% |
2-iodobenzaldehyde
N-methylhydroxyamine hydrochloride
(Z)-N-(2-iodobenzylidene)methylamine N-oxide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate at 20℃; for 2h; | 100% |
2-iodobenzaldehyde
glycine ethyl ester hydrochloride
methyl 2-[N-(2-iodobenzyl)amino]acetate
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid; triethylamine In dichloromethane at 20℃; for 19h; Inert atmosphere; | 100% |
2-iodobenzaldehyde
glycine ethyl ester hydrochloride
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid; triethylamine In dichloromethane at 20℃; for 19h; Inert atmosphere; | 100% |
2-iodobenzaldehyde
methoxymethyltriphenylphosphonium bromide
Conditions | Yield |
---|---|
Stage #1: methoxymethyltriphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere; Stage #2: 2-iodobenzaldehyde In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; | 100% |
2-Methoxypropene
2-iodobenzaldehyde
Conditions | Yield |
---|---|
With silica gel; acetic acid; tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium In dichloromethane at 25℃; Addition; | 99% |
With tris(6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato)ytterbium; silica gel; acetic acid at 25℃; | 97% |
2-iodobenzaldehyde
2-Iodobenzoic acid
Conditions | Yield |
---|---|
With potassium permanganate; tetrabutylammomium bromide; water In dichloromethane; acetone at 20℃; for 24h; | 99% |
With perchloric acid; N-Chlorourethan; acetic acid In water at 29.9℃; for 10h; Rate constant; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.), ΔG(excit.); | |
With perchloric acid; mercury(II) diacetate; N-bromoacetamide In acetic acid at 24.9℃; Kinetics; Mechanism; Thermodynamic data; other temperatures, ΔG(excit.), ΔH(excit.), ΔS(excit.); |
Conditions | Yield |
---|---|
With potassium carbonate In water at 20℃; for 0.5h; Suzuki-Miyaura Coupling; | 99% |
With potassium carbonate In ethanol; water at 20℃; for 1h; Suzuki-Miyaura Coupling; Green chemistry; | 94% |
With potassium phosphate In 1,4-dioxane at 70℃; for 1.5h; Suzuki-Miyaura Coupling; | 93% |
Cyclohexyl isocyanide
2-iodobenzaldehyde
acetic acid
N-butylamine
Conditions | Yield |
---|---|
In methanol at 20℃; Ugi reaction; | 99% |
2-iodobenzaldehyde
isocyanoacetic acid methyl ester
acetic acid
GlyOEt*HCl
Conditions | Yield |
---|---|
In methanol at 20℃; Ugi reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: (2-iodobenzyl)triphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran at 0℃; Stage #2: 2-iodobenzaldehyde In tetrahydrofuran at 20℃; Wittig reaction; Further stages.; | 99% |
With potassium hydroxide In chloroform; water at 20℃; for 2.5h; Reflux; | 92% |
4-Octyne
2-iodobenzaldehyde
1-amino-naphthalene
N-(2,3-dipropyl-1H-inden-1-yl)naphthalen-1-amine
Conditions | Yield |
---|---|
With Co(dppe)Cl2; zinc In tetrahydrofuran; acetonitrile at 120℃; for 12h; Inert atmosphere; regioselective reaction; | 99% |
4-Octyne
2-iodobenzaldehyde
p-toluidine
2,3-dipropyl-N-p-tolyl-1H-inden-1-amine
Conditions | Yield |
---|---|
With Co(dppe)Cl2; zinc In tetrahydrofuran; acetonitrile at 120℃; for 12h; Inert atmosphere; regioselective reaction; | 99% |
2,2-dimethyl-3-butyne
2-iodobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 3,3-Dimethylbut-1-yne With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; Stage #2: 2-iodobenzaldehyde In tetrahydrofuran at 20℃; for 3h; | 99% |
Stage #1: 3,3-Dimethylbut-1-yne With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: 2-iodobenzaldehyde In tetrahydrofuran; hexane at 20℃; for 4h; Stage #3: With ammonium chloride In tetrahydrofuran; hexane; water |
2-iodobenzaldehyde
phenylmagnesium bromide
(2-iodophenyl)(phenyl)methanol
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; for 1h; Inert atmosphere; | 99% |
diethoxyphosphoryl-acetic acid ethyl ester
2-iodobenzaldehyde
ethyl 3-(2-iodophenyl)acrylate
Conditions | Yield |
---|---|
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Stage #2: 2-iodobenzaldehyde In tetrahydrofuran at 0 - 20℃; for 2h; | 99% |
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; Stage #2: 2-iodobenzaldehyde In tetrahydrofuran; mineral oil at 0 - 20℃; Horner-Wadsworth-Emmons Olefination; Inert atmosphere; | 85% |
diethoxyphosphoryl-acetic acid ethyl ester
2-iodobenzaldehyde
ethyl (E)-3-(2-iodophenyl)-2-propenoate
Conditions | Yield |
---|---|
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In dichloromethane at 0℃; for 0.0833333h; Wittig-Horner reaction; Stage #2: 2-iodobenzaldehyde In dichloromethane at 0℃; for 0.5h; Wittig-Horner reaction; Further stages.; | 98.7% |
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran Stage #2: 2-iodobenzaldehyde In tetrahydrofuran at 20℃; | 92% |
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In dichloromethane; mineral oil at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-iodobenzaldehyde In dichloromethane; mineral oil at 0℃; for 2h; Inert atmosphere; | 89% |
2-iodobenzaldehyde
Biphenyl-2,2'-dicarbaldehyde
Conditions | Yield |
---|---|
With copper(I) thiophene-2-carboxylate; copper In dimethyl sulfoxide at 65℃; Ullmann Condensation; | 98% |
With indium; palladium 10% on activated carbon; tetrabutylammomium bromide; lithium chloride In water at 90℃; for 24h; Green chemistry; | 75% |
With palladium diacetate; potassium carbonate In N,N-dimethyl-formamide at 100℃; for 24h; | 64% |
2-iodobenzaldehyde
acetylenemagnesium bromide
1-(2-iodophenyl)prop-2-yn-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; Sealed tube; | 98% |
In tetrahydrofuran for 2h; Ambient temperature; | 95% |
In tetrahydrofuran at -60℃; for 14h; | 86% |
In tetrahydrofuran at 0℃; Inert atmosphere; |
2-iodobenzaldehyde
N-tosyl-N-allylpropargylamine
N-allyl-N-(3-(2-formylphenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
Stage #1: 2-iodobenzaldehyde With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine for 0.166667h; Inert atmosphere; Stage #2: N-tosyl-N-allylpropargylamine Inert atmosphere; | 98% |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate In tetrahydrofuran at 50℃; for 6h; Sonogashira coupling; | |
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine Inert atmosphere; |
4-Octyne
2-iodobenzaldehyde
3,5-difluoroaniline
N-(3,5-difluorophenyl)-2,3-dipropyl-1H-inden-1-amine
Conditions | Yield |
---|---|
With Co(dppe)Cl2; zinc In tetrahydrofuran; acetonitrile at 120℃; for 12h; Inert atmosphere; regioselective reaction; | 98% |
2-iodobenzaldehyde
3-(p-tolylamino)-5,5-dimethylcyclohex-2-enone
9-(4,4-dimethyl-6-oxo-2-(p-tolylamino)cyclohex-1-enyl)-3,3-dimethyl-10-(p-tolyl)-3,4,9,10-tetrahydroacridin-1(2H)-one
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; caesium carbonate In toluene at 110℃; for 12h; | 98% |
With caesium carbonate In toluene at 110℃; for 24h; Inert atmosphere; | 86% |
2-iodobenzaldehyde
tri(naphthalen-1-yl)bismuth
2-(naphthalene-1-yl)benzaldehyde
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; palladium diacetate; triphenylphosphine In N,N-dimethyl-formamide at 90℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With silver(I) acetate; copper diacetate; ethoxy(potassiosulfanyl)methanethione In N,N-dimethyl-formamide at 100℃; for 5h; | 98% |
1-ethynyl-4-fluorobenzene
2-iodobenzaldehyde
3-(4-fluorophenyl)isoquinoline
Conditions | Yield |
---|---|
With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; triethylamine In acetonitrile at 20℃; for 12h; Inert atmosphere; Schlenk technique; regioselective reaction; | 98% |
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