Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:3040-44-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiry2-Piperidinoethanol CAS:3040-44-6 Item Specification Results Apperance Colorless to light yellow liquid
The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dr
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:3040-44-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:3040-44-6
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:3040-44-6
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:3040-44-6
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam
Cas:3040-44-6
Min.Order:1 Kilogram
FOB Price: $7.0 / 10.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:3040-44-6
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:3040-44-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryMethanesulfonic acid is a raw material for medicine and pesticide. It can also be used as dehydrating agent, curing accelerator for coating, treating agent for fiber, solvent, catalysis, and esterification as well as polymerization reaction. It c
Cas:3040-44-6
Min.Order:1 Kilogram
FOB Price: $30.0 / 35.0
Type:Trading Company
inquiry2-Piperidinoethanol CAS:3040-44-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:3040-44-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:3040-44-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:3040-44-6
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Appearance/Colour:clear colourless liquid Vapor Pressure:0.0802mmHg at 25°C Melting Point:16 °C Refractive Index:n20/D 1.4804(lit.) Boiling Point:200.5 °C at 760 mmHg PKA:15.00±0.10(Predicted) Flash Point:91.2 °C
Cas:3040-44-6
Min.Order:1 Gram
FOB Price: $5.0
Type:Trading Company
inquiryHot sale High quality 3040-44-6 N-Piperidineethanol factory Molecular Formula C7H15NO Molar Mass 129.2 Density 0.973 g/mL at 25 °C (lit.) Melting Point 16°C Boling Point 199-202 &d
Cas:3040-44-6
Min.Order:1 Gram
Negotiable
Type:Other
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:3040-44-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:3040-44-6
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquirysuperior quality moderate price & quick delivery Appearance:Clear Colourless Liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to
Product name: 2-Piperidinoethanol CAS No.:3040-44-6 Molecule Formula:C7H15NO Molecule Weight:129.20 Purity: 99.0% Package: 200kg/drum Description:Colorless to light yellow liquid Manufacture Standards:Enterprise Standard TESTING
Cas:3040-44-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:3040-44-6
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:3040-44-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:3040-44-6
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 16h; | 99% |
at 80℃; for 72h; | 85% |
With sodium carbonate In acetonitrile at 20℃; for 48h; Reflux; | 36.8% |
piperidin-1-yl-acetic acid ethyl ester
1-piperidinoethanol
Conditions | Yield |
---|---|
With C30H34Cl2N2P2Ru; potassium methanolate; hydrogen In tetrahydrofuran at 100℃; under 38002.6 - 76005.1 Torr; for 5h; Glovebox; Autoclave; | 96% |
With ethanol; ruthenium(bis[2‐(ethylsulfanyl)ethyl]amine)(dichloro)(triphenylphosphine); potassium tert-butylate In toluene at 80℃; for 16h; | 95% |
With ethanol; nickel at 50℃; under 110326 - 147102 Torr; Hydrogenation; |
methyl 2-piperidylacetate
1-piperidinoethanol
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); hydrogen; sodium methylate In methanol at 100℃; under 37503.8 Torr; for 16h; Autoclave; Inert atmosphere; | 86% |
1-(2-(2-methoxy-4-nitrophenoxy)ethyl)piperidine
A
piperidine
B
1-ethyl-piperidine
C
1-piperidinoethanol
D
2-methoxy-4-nitrophenol
Conditions | Yield |
---|---|
In acetonitrile Rate constant; Product distribution; Mechanism; Ambient temperature; Irradiation; | A n/a B n/a C n/a D 83% E n/a F n/a |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; titanium(III) chloride at 20℃; for 0.5h; Acidic aq. solution; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
at 70℃; for 5h; | 75% |
With acetone | |
With benzene |
4-(2,6-dioxacyclohexyl)phenol
2-(dimethylamino)ethyl ethyl carbonate
1-piperidinoethanol
Conditions | Yield |
---|---|
Stage #1: 4-(2,6-dioxacyclohexyl)phenol; 2-(dimethylamino)ethyl ethyl carbonate In acetonitrile at 200℃; under 12001.2 Torr; for 8h; Autoclave; Stage #2: With trifluoroacetic acid In acetonitrile at 20℃; for 20h; | 69% |
Conditions | Yield |
---|---|
at 100℃; | |
at 100℃; | |
With water Im Rohr bei Raumtemperatur; |
Conditions | Yield |
---|---|
With potassium hydroxide |
piperidine
ethylene glycol
A
1-piperidinoethanol
B
1,2-dipiperidinoethane
Conditions | Yield |
---|---|
With triphenylphosphine; ruthenium trichloride at 120℃; for 15h; Product distribution; other catalyst, also with THF, other phosphine, also at 220 degC; | |
With triphenylphosphine; ruthenium trichloride at 220℃; for 15h; |
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(4-ethoxy-phenyl)-carbamic acid-(2-piperidino-ethyl ester); hydrochloride
A
1-piperidinoethanol
B
4-Ethoxyaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(3-Propoxy-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
3-propoxyaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
p-Tolyl-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
p-toluidine
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(4-Ethyl-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
4-aminoethylbenzene
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
2-piperidinoethyl N-(3-methoxyphenyl)carbamate hydrochloride
A
1-piperidinoethanol
B
m-Anisidine
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(4-Fluoro-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
4-fluoroaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(3-Fluoro-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
meta-fluoroaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
2-piperidinoethyl N-(4-chlorophenyl)carbamate hydrochloride
A
1-piperidinoethanol
B
4-chloro-aniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(3-Ethoxy-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
m-phenetidine
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(4-Isopropoxy-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
4-(isopropoxy)aniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(4-Propoxy-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
4-propoxyaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(3-Isopropoxy-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
3-isopropoxyaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
(3-Trifluoromethyl-phenyl)-carbamic acid 2-piperidin-1-yl-ethyl ester; hydrochloride
A
1-piperidinoethanol
B
3-trifluoromethylaniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
1-(2-(4-methoxyphenylcarbamoyloxy)ethyl)piperidinium chloride
A
1-piperidinoethanol
B
4-methoxy-aniline
Conditions | Yield |
---|---|
With water In ethanol at 40 - 70℃; Rate constant; Thermodynamic data; Kinetics; |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 40℃; Rate constant; Thermodynamic data; var. temp., EA; |
1-piperidinoethanol
Conditions | Yield |
---|---|
With potassium hydroxide Destillieren; |
1-piperidinoethanol
Conditions | Yield |
---|---|
With sulfuric acid at 160℃; |
1-piperidinoethanol
4-benzyloxy-2-fluoro-1-nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 1-piperidinoethanol With sodium hydride In tetrahydrofuran; mineral oil at 20 - 30℃; for 1h; Stage #2: 4-benzyloxy-2-fluoro-1-nitrobenzene In tetrahydrofuran; mineral oil at 20℃; for 1h; | 98.3% |
1-piperidinoethanol
4-(2-hydroxyethyl)morpholine 4-oxide
Conditions | Yield |
---|---|
With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; acetonitrile In tert-butyl alcohol at 20℃; for 18h; Green chemistry; chemoselective reaction; | 98% |
1-piperidinoethanol
(2-dimethylamino-6-methoxy-benzo[b]thiophen-3-yl)-(4-fluoro-phenyl)-methanone
[2-dimethylamino-6-methoxybenzothien-3-yl] [4-[2-(1-piperidinyl)ethoxy]phenyl]-methanone
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.25h; Alkylation; | 97% |
1-piperidinoethanol
phthalic anhydride
phtalate acide de (piperidinyl)-2 ethanol
Conditions | Yield |
---|---|
In benzene for 4.5h; Heating; | 96.5% |
With acetone |
1-piperidinoethanol
1,2-bis(2-aminophenoxy)ethane N,N,N',N'-tetraacetic acid
Conditions | Yield |
---|---|
With 3-nitrobenzoic acid In dimethyl sulfoxide at 60℃; for 6h; Temperature; Reagent/catalyst; Solvent; | 96.1% |
1-piperidinoethanol
(3,9-dibenzyloxybenzo[b]naphtho[1,2-d]furan-5-yl)(4-fluorofluorophenyl)methanone
(3,9-dihydroxybenzo[b]naphtho[1,2-d]furan-5-yl)(4-[2-(piperidin-1-yl)ethoxy]phenyl)methanone
Conditions | Yield |
---|---|
Stage #1: 1-piperidinoethanol With sodium hydride In N,N-dimethyl-formamide at 20℃; for 30h; Stage #2: (3,9-dibenzyloxybenzo[b]naphtho[1,2-d]furan-5-yl)(4-fluorofluorophenyl)methanone for 6h; | 96% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 2h; | 96% |
1-piperidinoethanol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 2h; | 96% |
1-piperidinoethanol
di-tert-butyl dicarbonate
tert-butyl 2-(2-hydroxyethyl)piperidine-1-carboxylate
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran-water | 95% |
Conditions | Yield |
---|---|
In diethyl ether addn. of slight excess of B-compd. to piperidine derivative; crystn., filtration, drying; | 95% |
1-piperidinoethanol
Conditions | Yield |
---|---|
With boric acid In methanol; water | 95% |
Conditions | Yield |
---|---|
In methanol; water to soln. H3BO3 in aq. MeOH (1:1) amine was added, stirred for 10 min, solvent was removed in vacuo, residue was heated in oven to dry 4 h at 100°C; elem. anal.; | 95% |
1-piperidinoethanol
Conditions | Yield |
---|---|
With sodium hydride; sodium hydrogencarbonate; sodium chloride In tetrahydrofuran at 0 - 20℃; | 93.1% |
1-piperidinoethanol
Conditions | Yield |
---|---|
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In tetrahydrofuran at 20℃; | 93% |
1-piperidinoethanol
{1-[3-(tert-butyldimethylsilyloxy)propyl]benzimidazolidin-2-ylidene}malononitrile
{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-piperidinoethyl)benzimidazolidin-2-ylidene}malononitrile
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran; toluene at 0 - 20℃; for 0.166667h; | 92.8% |
1-piperidinoethanol
phenyl isocyanate
1-phenylcarbamoyloxy-2-piperidin-1-yl-ethane
Conditions | Yield |
---|---|
In toluene for 7h; Heating; | 92% |
With diethyl ether | |
In dichloromethane for 1.5h; Heating; |
1-piperidinoethanol
methanol
2-(4-bromobenzoyl)benzoic acid
2-methoxycarbonyl-4'-(2-piperidinoethyloxy)benzophenone
Conditions | Yield |
---|---|
Stage #1: 1-piperidinoethanol With sodium hydride In tetrahydrofuran for 0.5h; Reflux; Stage #2: methanol; 2-(4-bromobenzoyl)benzoic acid With sodium hydride In tetrahydrofuran at 20℃; Stage #3: With thionyl chloride at 0 - 20℃; | 91% |
1-piperidinoethanol
6-methoxy-2-(4-methoxyphenyl)-3-(4-fluorobenzoyl)benzo[b]thiophene
[6-Methoxy-2-(4-Methoxyphenyl)benzo[b]thien-3-yl]-[4-[2-(1-Piperidinyl)ethoxy]phenyl] Methanone
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide for 0.25h; Ambient temperature; | 90% |
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h; Addition; | 90% |
1-piperidinoethanol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 0 - 20℃; Mitsunobu Displacement; | 90% |
1-piperidinoethanol
methyl isocyanate
Methyl-carbamic acid 2-piperidin-1-yl-ethyl ester
Conditions | Yield |
---|---|
With pyridine at 70 - 80℃; for 7.5h; | 89% |
1-piperidinoethanol
3-(4-hydroxyphenyl)-5-methoxy-2-(4-methoxyphenyl)benzo[b]thiophene
5-methoxy-2-(4-methoxyphenyl)-3-{4-[ 2-(1-piperidinyl)ethoxy]phenyl}benzo[b]thiophene
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu reaction; | 89% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu reaction; | 87% |
1-piperidinoethanol
6-bromo-3-methyl-4-oxo-2-phenyl-4H-1-benzopyran-8-carboxylic acid
β-piperidinoethyl 6-bromo-3-methylflavone-8-carboxylate
Conditions | Yield |
---|---|
Stage #1: 6-bromo-3-methyl-4-oxo-2-phenyl-4H-1-benzopyran-8-carboxylic acid With thionyl chloride In toluene at 0.9℃; for 3h; Stage #2: 1-piperidinoethanol In toluene at 0.9 - 40℃; for 3h; | 89% |
1-piperidinoethanol
sodium saccharinate dihydrate
Ag(saccharinate)(N-(2-hydroxyethylethyl)piperidine)
Conditions | Yield |
---|---|
In water; acetonitrile 1 equiv. of Na-salt in H2O to aq. AgNO3 soln., MeCN was added until dissoln., 1 equiv. of piperidine-compd. was added; mixt. was allowed to stand at room temp. in the darkness for 2 d, elem. anal.; | 87% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu reaction; | 87% |
1-piperidinoethanol
methyl 4-hydroxylbenzoate
4-[2-(N-piperidine)-ethoxy]benzoic acid methyl ester
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 16h; Inert atmosphere; | 86.7% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 30℃; for 4h; Inert atmosphere; | 76% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran for 0.5h; Cooling with ice; | |
Stage #1: 1-piperidinoethanol; methyl 4-hydroxylbenzoate With triphenylphosphine In tetrahydrofuran at 0℃; for 0.166667h; Mitsunobu Displacement; Stage #2: With di-isopropyl azodicarboxylate In tetrahydrofuran at 20℃; Mitsunobu Displacement; | 2.1 g |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0℃; for 0.166667h; | 2.1 g |
Conditions | Yield |
---|---|
In acetonitrile for 4h; Reflux; | 86% |
In acetonitrile for 4h; Reflux; | 86% |
In diethyl ether for 20h; Ambient temperature; | 84% |
In acetone; acetonitrile | 139 g (0.45 mol, 90%) |
1-piperidinoethanol
[2-(4-hydroxyphenyl)-6-hydroxybenzo[b]thien-3-yl] [4-fluorophenyl]methanone
Raloxifen
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 50℃; for 5h; | 86% |
About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia
Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog
©2008 LookChem.com,License: ICP
NO.:Zhejiang16009103
complaints:service@lookchem.com Desktop View