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Conditions | Yield |
---|---|
With methylene chloride; sodium at 30 - 40℃; under 375.038 Torr; Flow reactor; Inert atmosphere; | 93% |
indium(III) chloride
magnesium
methyl iodide
trimethyl indium
Conditions | Yield |
---|---|
In diethyl ether a Grignard soln. (prepd. from MeI and Mg in Et2O) is added to the suspn. of InCl3 in ether and refluxed for 3 h; distn. of excess of Et2O at atm. pressure affords Me3In*Et2O; repeated distn. of the etherate at room temp. in vac. affords InMe3; | 92% |
trimethyl indium
Conditions | Yield |
---|---|
In neat (no solvent) metal complex decomposed at 110-135°C for 2-3 h; | 81% |
trimethyl indium
Conditions | Yield |
---|---|
In neat (no solvent) metal complex decomposed at 110-135°C for 2-3 h; | 75% |
Conditions | Yield |
---|---|
at 70℃; | 66% |
Conditions | Yield |
---|---|
With indium(III) chloride | |
With indium(III) chloride In tetrahydrofuran at -78℃; Cooling with dry ice bath; |
Conditions | Yield |
---|---|
With mercury dichloride at 100℃; |
tetrakis(trimethylindium) 1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecane adduct
trimethyl indium
Conditions | Yield |
---|---|
In neat (no solvent) at 80-115°C under vac.; |
trimethylindium bis(N,N,N',N'-tetramethyl-4,4'-methylenebis(aniline)) adduct
trimethyl indium
Conditions | Yield |
---|---|
In neat (no solvent) at 80-115°C under vac.; |
hexakis(trimethylindium) 1,4,7,10,13,16-hexamethyl-1,4,7,10,13,16-hexaazacyclooctadecane adduct
trimethyl indium
Conditions | Yield |
---|---|
In neat (no solvent) at 80-115°C under vac.; |
Conditions | Yield |
---|---|
With mercury dichloride heating for 8 days at 100°C in CO2 atmosphere; cooled by ice then Hg(CH3)2 removed by distillation; | |
With HgCl2 heating for 8 days at 100°C in CO2 atmosphere; cooled by ice then Hg(CH3)2 removed by distillation; |
Conditions | Yield |
---|---|
In diethyl ether InCl3 heated at 80°C in vac. for 1 h, purged Ar, ether added, cooled (ice bath), MeLi added; stirred for 2 h, evapd.; | |
In diethyl ether (inert atmosphere); addn. of MeLi in Et2O to InCl3 in Et2O at 0°C, warming to room temp.; filtration; prepd. as soln.; | |
In not given under Ar; MeLi (3 equiv.) in THF or hexane or Et2O added slowly (15-30 min) to cooled (-78°C) soln. of InCl3 in THF; stirred for 30 min; warmed to room temp.; according to H. C. Clark, A. L. Pickard, J. Organomet. Chem. 8 (1967) 427; |
A
bismuth
B
indium
C
tetrakis(trimethylsilyl)dibismutane
D
trimethyl indium
Conditions | Yield |
---|---|
In not given decompn. at temp. above -30 °C within minutes; |
A
dimethylbis(η5-pentamethylcyclopentadienyl)uranium
B
trimethyl indium
Conditions | Yield |
---|---|
In neat (no solvent) drying under vac.; |
Conditions | Yield |
---|---|
Stage #1: indium; methyl iodide In 2,6,10,15,19,23-hexamethyltetracosane at 110℃; for 2h; Stage #2: trimethylaluminum With tri-n-propylamine In 2,6,10,15,19,23-hexamethyltetracosane at 90℃; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 0.5h; | |
In tetrahydrofuran at -78℃; for 0.5h; | |
In tetrahydrofuran; diethyl ether at 0 - 20℃; for 0.25h; Inert atmosphere; |
A
trimethyl indium
B
dimethylindium chloride
Conditions | Yield |
---|---|
With potassium chloride; sodium chloride at 150 - 250℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With Durasyn 162 for 3.5h; Temperature; | 92 %Spectr. |
Conditions | Yield |
---|---|
In 2-Methylpentane at 20 - 38℃; | 100 %Spectr. |
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane at -78℃; |
Conditions | Yield |
---|---|
In toluene under Ar or N2, stirred, refluxed for 2-3 h; removal of solvent, filtered off, washed with benzene or hexane, dried under vac.; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In toluene molar ratio 3:1; | 100% |
In benzene dry Ar atm.; 3 equiv. of AlMe3, cooling (-15°C), heating (room temp., stirring), refluxing (1,5 h, 70-80°C); concn., standing (5 to -5 degree.C, several days), washing (toluene), drying (vac.); elem. anal.; | 70% |
Conditions | Yield |
---|---|
In toluene molar ratio 3:1; | 100% |
Conditions | Yield |
---|---|
In toluene molar ratio 3:1; | 100% |
In benzene dry Ar atm.; 3 equiv. of AlMe3, cooling (-15°C), heating (room temp., stirring), refluxing (1,5 h, 70-80°C); concn., standing (5 to -5 degree.C, several days), washing (toluene), drying (vac.); elem. anal.; | 84% |
Conditions | Yield |
---|---|
In toluene molar ratio 3:1; | 100% |
In benzene dry Ar atm.; 3 equiv. of AlMe3, cooling (-15°C), heating (room temp., stirring), refluxing (1,5 h, 70-80°C); concn., standing (5 to -5 degree.C, several days), washing (toluene), drying (vac.); elem. anal.; | 79% |
[(CH3)2SnN(CH2CH(CH3)2)]3
trimethyl indium
Conditions | Yield |
---|---|
In toluene molar ratio 3:1; | 100% |
In benzene dry Ar atm.; 3 equiv. of AlMe3, cooling (-15°C), heating (room temp., stirring), refluxing (1,5 h, 70-80°C); concn., standing (5 to -5 degree.C, several days), washing (toluene), drying (vac.); elem. anal.; | 88% |
Conditions | Yield |
---|---|
In toluene molar ratio 3:1; | 100% |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 12h; Inert atmosphere; Schlenk technique; | 100% |
In benzene Inert atmosphere; Schlenk technique; |
tris(tert-butoxy)silanol
trimethyl indium
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 12h; Inert atmosphere; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran | 99% |
Conditions | Yield |
---|---|
In hexane; toluene under Ar, 1 equiv. of metal-compd. was added to 9:1 hexane:toluene soln.of amine; crystn. at -30 °C; elem. anal.; | 99% |
In diethyl ether; Petroleum ether soln. of equimolar amts. of aminopyridine and Me3In in diethyl ether/light petroleum (1:2) cooled to -30°C; crystals collected, washed with light petroleum, and dried in vac.; elem. anal.; | 91% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In toluene (N2); dropwise addn. of InMe3 to methyl salicylate in toluene at -78°C, warming to room temp.; solvent removal (vac.), crystn. (toluene/hexane); elem. anal.; | 99% |
Conditions | Yield |
---|---|
In pentane (N2); filtn., stirring; solvent removal (vac.); | 99% |
Conditions | Yield |
---|---|
In dichloromethane byproducts: CH4; elem. anal.; | 99% |
(1R,2S)-1-Amino-2-indanol
trimethyl indium
Conditions | Yield |
---|---|
In toluene byproducts: CH4; all manipulations under dry oxygen-free N2 atm.; soln. of org. compd. added dropwise to soln. of metal compd. at room temp., stirred for 12 h; solvent removed in vac., crystd. from toluene; elem. anal.; | 99% |
trimethyl indium
(1S,2R)-1-amino-2-indanol
Conditions | Yield |
---|---|
In toluene byproducts: CH4; all manipulations under dry oxygen-free N2 atm.; soln. of org. compd. added dropwise to soln. of metal compd. at room temp., stirred for 12 h; solvent removed in vac., crystd. from toluene; elem. anal.; | 99% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CH4; (Ar); addn. of ligand to indium compd. at -196°C, slow warming toroom temp., keeping at 20°C for 28 d; evapn.; | 98.3% |
(S)-2-dimethylamino-3-phenyl-1-propanol
trimethyl indium
Conditions | Yield |
---|---|
In toluene byproducts: CH4; under N2, 1 equiv. of alc. in toluene was added to a stirred toluene soln. of Me3In at room temp., stirring for 0.5 h; solvent was removed in vac., crystn. from n-pentane at 6 °C, elem. anal.; | 98% |
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