As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
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inquiryProduct name 2-Chloro-4,6-dimethylpyrimidine CAS NO. 4472-44-0 MF C6H7ClN2 Appearance White Powder Purity 99
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiry2-Chloro-4,6-dimethylpyrimidine CAS:4472-44-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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Min.Order:10 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiryroduct Name: 2-Chloro-4,6-dimethylpyrimidine CAS: 4472-44-0 MF: C6H7ClN2 MW: 142.59 EINECS: Mol File: 4472-44-0.mol 2-Chloro-4,6-dimethylpyrimidine Structure 2-Chloro-4,6-dimethylpyrimidine Chemical Properties Melting point 3
Cas:4472-44-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
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Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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inquiryWuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
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Min.Order:100 Gram
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Type:Manufacturers
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Cas:4472-44-0
Min.Order:0
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Negotiable
Type:Lab/Research institutions
inquiry4,6-dimethyl-2-hydroxy-pyrimidine hydrochloride
2-chloro-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
With trichlorophosphate for 10h; Inert atmosphere; Reflux; | 91% |
With trichlorophosphate for 10h; Heating; | 77% |
With trichlorophosphate for 10h; Reflux; | 77% |
With trichlorophosphate In neat (no solvent) for 10h; Inert atmosphere; Reflux; | 77% |
2-oxo-4,6-dimethyl-1,2-dihydropyrimidine hydrochloride
2-chloro-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
With trichlorophosphate for 18h; Heating / reflux; | 56% |
With trichlorophosphate |
Conditions | Yield |
---|---|
In diethyl ether; trichlorophosphate | 55% |
4-amino-1-[9,10-dihydro-9,10-methanoanthracen-9-ylmethyl]piperidine
A
2-chloro-4,6-dimethylpyrimidine
B
2-[1-(9,10-Dihydro-9,10-methanoanthracen-9-ylmethyl)-4-piperidylamino]-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
A n/a B 55% |
Conditions | Yield |
---|---|
With trichlorophosphate for 23h; Heating / reflux; | 55% |
benzylamine
4,6-dimethyl-2-meraptopyrimidine
A
2-chloro-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
Stage #1: 4,6-dimethyl-2-meraptopyrimidine With hydrogenchloride; sodium hypochlorite In dichloromethane; water at -10 - -5℃; for 0.25h; Stage #2: benzylamine In dichloromethane at 0℃; for 0.5h; | A n/a B 19% |
1-benzyl-3,5-dimethyl-1H-pyrazole
chloroform
A
2-chloro-4-methylpyrimidine
B
2-chloro-4,6-dimethylpyrimidine
C
2-phenylpyrimidine
D
4,6-dimethyl-2-phenylpyrimidine
Conditions | Yield |
---|---|
at 550 - 555℃; Further byproducts given. Title compound not separated from byproducts; |
1-benzyl-3,5-dimethyl-1H-pyrazole
chloroform
A
2-chloro-4-methylpyrimidine
B
2-chloro-4,6-dimethylpyrimidine
C
4,6-dimethyl-2-phenylpyrimidine
D
3-Methylpyrazole
Conditions | Yield |
---|---|
at 550 - 555℃; Further byproducts given. Title compound not separated from byproducts; |
1-benzyl-3,5-dimethyl-1H-pyrazole
A
NH-pyrazole
B
2-chloro-4-methylpyrimidine
C
2-chloro-4,6-dimethylpyrimidine
D
4,6-dimethyl-2-phenylpyrimidine
Conditions | Yield |
---|---|
With chloroform at 550 - 555℃; Further byproducts given. Title compound not separated from byproducts; |
1-benzyl-3,5-dimethyl-1H-pyrazole
A
2-chloro-4-methylpyrimidine
B
2-chloro-4,6-dimethylpyrimidine
C
4,6-dimethyl-2-phenylpyrimidine
D
3-Methylpyrazole
Conditions | Yield |
---|---|
With chloroform at 550 - 555℃; Further byproducts given. Title compound not separated from byproducts; |
hydrogenchloride
4,6-dimethylpirimidin-2-one
trichlorophosphate
2-chloro-4,6-dimethylpyrimidine
2-chloro-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
With trichlorophosphate |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite | |
With hydrogenchloride; zinc(II) chloride; sodium nitrite In dichloromethane; water | |
With hydrogenchloride; zinc(II) chloride; sodium nitrite In dichloromethane; water |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / Heating 2: aq. NaNO2; HCl View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride / ethanol; water / 24 h / Inert atmosphere; Reflux 2: trichlorophosphate / 10 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride 2: trichlorophosphate / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride / ethanol / 3 h / Heating / reflux 2: trichlorophosphate / 18 h / Heating / reflux View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride 2: trichlorophosphate / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / conc. HCl / ethanol / 24 h / Heating 2: 77 percent / phosphorus oxychloride / 10 h / Heating View Scheme |
Conditions | Yield |
---|---|
With trichlorophosphate for 1h; Heating / reflux; | |
With sodium hydroxide In trichlorophosphate | |
With sodium bicarbonate; trichlorophosphate In water |
Conditions | Yield |
---|---|
With trichlorophosphate |
2-chloro-4,6-dimethylpyrimidine
p-toluidine
4,6-dimethyl-N-(4-methylphenyl)-2-pyrimidinamine
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 99% |
2-chloro-4,6-dimethylpyrimidine
4-bromo-aniline
N-(4-bromophenyl)-4,6-dimethyl-2-pyrimidinamine
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 98% |
2-chloro-4,6-dimethylpyrimidine
sodium diphenylphosphinodithioate
diphenyl (4,6-dimethyl-2-pyrimidyl) dithiophosphinate
Conditions | Yield |
---|---|
In toluene for 9h; Condensation; Heating; | 98% |
Conditions | Yield |
---|---|
With C50H61Cl2N3Pd; potassium tert-butylate In 1,4-dioxane at 100℃; for 2h; | 97% |
Conditions | Yield |
---|---|
Stage #1: decylthiol With 18-crown-6 ether; potassium hydroxide In tetrahydrofuran; water for 2h; Reflux; Stage #2: 2-chloro-4,6-dimethylpyrimidine In tetrahydrofuran; water for 24h; Reflux; | 97% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 97% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 97% |
piperazine
2-chloro-4,6-dimethylpyrimidine
1-(4,6-dimethyl-pyrimidin-2-yl)piperazine
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran; water at 20℃; for 24h; | 96% |
In dimethyl sulfoxide at 100℃; for 16h; | 93% |
Stage #1: piperazine With potassium carbonate In water at 45 - 50℃; for 4.5h; Inert atmosphere; Stage #2: 2-chloro-4,6-dimethylpyrimidine In water at 20℃; Inert atmosphere; | 93% |
2-chloro-4,6-dimethylpyrimidine
2-benzyloctahydropyrrolo[3,4-c]pyrrole
2-benzyl-5-(4,6-dimethyl-pyrimidin-2-yl )-octahydro-pyrrolo[3,4-c]pyrrole
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 15h; | 96% |
With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 15h; Inert atmosphere; | 96% |
1-methyl-piperazine
2-chloro-4,6-dimethylpyrimidine
4,6-dimethyl-2-(4-methylpiperazin-1-yl)pyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 50℃; for 72h; | 96% |
In N,N-dimethyl-formamide at 90℃; for 2.5h; Inert atmosphere; | 93% |
2-chloro-4,6-dimethylpyrimidine
cis-3-benzyl-3,7-diazabicyclo[3.3.0]octane
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 100℃; for 15h; Inert atmosphere; | 96% |
methanol
2-chloro-4,6-dimethylpyrimidine
2-methoxy-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil for 2h; | 96% |
morpholine
2-chloro-4,6-dimethylpyrimidine
4-(4,6-dimethylpyrimidin-2-yl)morpholine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90℃; for 2.5h; Inert atmosphere; | 95% |
at 210℃; for 0.166667h; Microwave irradiation; | 92% |
With ethanol |
2-chloro-4,6-dimethylpyrimidine
benzylamine
N-benzyl-2-amino-4,6-dimethylpyrimidine
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil for 2h; | 95% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil for 1h; | 94% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; mineral oil for 3h; | 94% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 92% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 91% |
2-chloro-4,6-dimethylpyrimidine
trimethylamine
(4,6-dimethylpyrimid-2′-yl)-trimethylammonium chloride
Conditions | Yield |
---|---|
In benzene 1) 0 deg C; 2) room temperature, 1h; | 91% |
In water at 0℃; | 88% |
With benzene |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 91% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 91% |
2-chloro-4,6-dimethylpyrimidine
4-methoxy-aniline
N-(4-methoxylphenyl)-4,6-dimethyl-2-pyrimidinamine
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 90% |
2-chloro-4,6-dimethylpyrimidine
3,4,5-Trimethoxyaniline
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 90% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 90% |
Conditions | Yield |
---|---|
In ethanol at 160℃; for 0.166667h; Microwave irradiation; Sealed tube; Green chemistry; | 90% |
2-chloro-4,6-dimethylpyrimidine
2-(methoxymethyl)-4-(piperazin-1-yl)pyrimidine
2-methoxymethyl-4-[4-(4,6-dimethyl-pyrimidinin-2-yl)-piperazin-1-yl]-pyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In butan-1-ol Heating; | 89% |
2-chloro-4,6-dimethylpyrimidine
phenylmagnesium chloride
4,6-dimethyl-2-phenylpyrimidine
Conditions | Yield |
---|---|
With quinoline; ferric(III) bromide In tetrahydrofuran; tert-butyl methyl ether at 25℃; for 0.0833333h; Reagent/catalyst; Inert atmosphere; | 89% |
With ferric(III) bromide In tetrahydrofuran; tert-butyl methyl ether at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 76% |
2-chloro-4,6-dimethylpyrimidine
tributyl(thien-2-yl)stannane
4,6-dimethyl-2-(thiophen-2-yl)pyrimidine
Conditions | Yield |
---|---|
With potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium chloride In N,N-dimethyl-formamide at 110℃; for 2h; | 88% |
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