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inquiry2-propylimidazole-4,5-dicarbonitrile
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water at 100℃; for 0.0333333h; Temperature; | 96.5% |
With hydrogenchloride; water for 4h; Reflux; Large scale reaction; | 95% |
With hydrogenchloride for 8h; Heating; | 80% |
2-propyl-1H-benzimidazole
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With sodium tungstate; disodium hydrogenphosphate; potassium dihydrogenphosphate; dihydrogen peroxide In water at 100℃; for 1h; pH=4.9; Concentration; pH-value; Temperature; | 85.5% |
With sulfuric acid; dihydrogen peroxide In water at 100 - 120℃; for 0.5h; Concentration; | 72% |
With sulfuric acid; dihydrogen peroxide In water for 3h; Reflux; | 35% |
2-propyl-1H-imidazole-4, 5-diethyl azodicarboxylate
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran at 50℃; for 4h; | 85% |
L-Tartaric acid
butyraldehyde
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
Stage #1: L-Tartaric acid With sulfuric acid; nitric acid at 43 - 46℃; for 1.61667h; Stage #2: butyraldehyde With ammonium hydroxide In 1-methyl-pyrrolidin-2-one at -10 - 4℃; Solvent; Temperature; | 46% |
2-propyl-1H-benzimidazole
A
4,5-imidazoledicarboxylic acid
B
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With sulfuric acid; dihydrogen peroxide In water at 100 - 130℃; | A 31% B 1% |
butyraldehyde
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With ammonia |
di-O-nitro-tartaric acid
butyraldehyde
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With ammonium hydroxide at 0℃; for 0.5h; | 97 g |
1,1,1-trimethoxybutane
diaminomaleonitrile
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
In methanol Reflux; |
methanol
2-propyl-1H-imidazole-4,5-dicarboxylic acid
2-propyl-4,5-bis(methoxycarbonyl)-imidazole
Conditions | Yield |
---|---|
With thionyl chloride at 40 - 45℃; Large scale reaction; | 96% |
With thionyl chloride at 43℃; for 11h; | |
Stage #1: methanol; 2-propyl-1H-imidazole-4,5-dicarboxylic acid With thionyl chloride Reflux; Stage #2: With sodium hydroxide In water for 0.25h; |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
ethanol
2-propyl-1H-imidazole-4, 5-diethyl azodicarboxylate
Conditions | Yield |
---|---|
Stage #1: 2-propyl-1H-imidazole-4,5-dicarboxylic acid; ethanol With hydrogenchloride; thionyl chloride at 5℃; for 0.166667h; Stage #2: for 1.5h; Heating; | 94% |
With hydrogenchloride Ambient temperature; | 86% |
With thionyl chloride In water at 8℃; for 6.6h; Temperature; Reflux; | 77% |
at 0℃; for 12h; Reflux; |
Conditions | Yield |
---|---|
In methanol at 80℃; for 72h; | 88.49% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With triethylamine In water at 170℃; for 96h; Autoclave; | 84% |
Conditions | Yield |
---|---|
In ethanol; water ligand dissolved in H2O at room temp., mixed with EtOH soln. of ZnCl2, heated at 70°C for 8 h; crystd. at room temp. for 5 d, washed (H2O), elem. anal.; | 81.3% |
In ethanol; water imidazole-compd. dissolved in H2O, Zn-compd. dissolved in EtOH, two solution mixed, heated to 70°C for 8 h; filtered, evaporated at room temp. for 5 d, washed with H2O, elem. anal.; | 81.3% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
zinc(II) acetate dihydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide ligand dissolved in H2O at room temp., mixed with DMF soln. of Zn(CH3COO)2*2H2O, refluxed for 8 h; crystd. at room temp. for 15 d, washed (H2O), elem. anal.; | 78% |
In water; N,N-dimethyl-formamide imidazole-compd. dissolved in H2O at room temp., Zn-compd. dissolved in DMF, two solution mixed, refluxed for 8 h; filtered, evaporated at room temp. for 15 d, washed with H2O, elem. anal.; | 78% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
Conditions | Yield |
---|---|
With 3,3',4,4'-biphenyltetracarboxylic acid In water mixt. of acid and Cd(NO3)2*4H2O dissolved in H2O; stirred for 0.5 h; heated at 75°C for 3 d; elem. anal.; | 77% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
copper(II) acetate monohydrate
Conditions | Yield |
---|---|
In water at 20 - 130℃; Sealed tube; | 75% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
With benzidine; terephthalic acid In water; N,N-dimethyl-formamide mixt. of imidazole deriv., Cd nitrate, benzidine, terephthalic adcid heated in mixt. DMF/H2O heated at 75°C for 48 h; washed by water, dried in air; elem. anal.; | 74% |
Conditions | Yield |
---|---|
With 3,3',4,4'-biphenyltetracarboxylic acid In water mixt. of acid and Zn(OAc)2 dissolved in H2O; stirred for 0.5 h; heated at 75°C for 3 d; elem. anal.; | 72% |
4,4'-bipyridine
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water; acetonitrile at 130℃; for 48h; pH=6.5; Sealed tube; High pressure; | 71% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
cadmium(II) acetate dihydrate
Conditions | Yield |
---|---|
Stage #1: 2-propyl-1H-imidazole-4,5-dicarboxylic acid With sodium hydroxide In water at 20℃; pH=6; Stage #2: cadmium(II) acetate dihydrate In ethanol; water at 75℃; for 8h; | 70.8% |
Stage #1: 2-propyl-1H-imidazole-4,5-dicarboxylic acid; cadmium(II) acetate dihydrate In water for 0.333333h; Stage #2: In water at 180℃; for 120h; Sealed tube; | 35.2% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
[Cu(2-propyl-4,5-imidazoledicarboxylic acid(-1H))2]
Conditions | Yield |
---|---|
Stage #1: 2-propyl-1H-imidazole-4,5-dicarboxylic acid With sodium hydroxide In water at 20℃; pH=6.5; Stage #2: copper(II) choride dihydrate In ethanol; water at 70℃; for 8h; | 70.8% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
Stage #1: 2-propyl-1H-imidazole-4,5-dicarboxylic acid With sodium hydroxide In water at 20℃; pH=6; Stage #2: lead(II) acetate trihydrate In ethanol; water at 75℃; for 8h; | 70.8% |
1,10-Phenanthroline
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
[Co(2-propyl-1H-imidazole-4,5-dicarboxylic acid(-3H))(1,10-phenanthroline)]*H2O
Conditions | Yield |
---|---|
In water High Pressure; Co compd., ligand, and phen (1:1:1 molar ratio) in H2O, sealed, heated at 170°C for 3 d; cooled, crystd., septd., washed (H2O); | 70% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
Conditions | Yield |
---|---|
In water High Pressure; mixt. of Pb(ClO4)2*3H2O, acid and water stirred 1 h, sealed in Teflon reactor, heated at 160°C for 5 d; cooled to room temp. at 3°C/h; elem. anal.; | 69.8% |
Conditions | Yield |
---|---|
With hydrogenchloride In acetonitrile at 110℃; for 99h; pH=4; Autoclave; High pressure; | 69% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
cobalt(II) diacetate tetrahydrate
Conditions | Yield |
---|---|
With sodium hydroxide at 80℃; for 2h; pH=3.6; | 68% |
In water High Pressure; stoich. mixt. in H2O, sealed, heated at 130°C for 144 h; cooled to room temp. in 20 h, crystd., septd., washed (H2O), dried in air, elem. anal.; | 56% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
diaquabis(2-propyl-1H-imidazole-4,5-dicarboxylate)cobalt(II)
Conditions | Yield |
---|---|
In water; acetonitrile High Pressure; mixt. of Co(NO3)2*6H2O and imidazole dicarboxylic acid (1:1) in H2O/CH3CN heated in an autoclave at 152°C for 72 h; cooled to room temp. (10°C/h), collected, washed (h2O), dried (air), elem. anal.; | 68% |
1,1'-(1,4-butanediyl)bis(imidazole)
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
Conditions | Yield |
---|---|
In water High Pressure; Zn compd., ligand, and bbi (2:2:1 molar ratio) in H2O, sealed, heated at140°C for 3 h; cooled (5°C), elem. anal.; | 67% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
cobalt(II) diacetate tetrahydrate
1,2-diaminopropan
Conditions | Yield |
---|---|
at 120℃; for 24h; Autoclave; | 67% |
1,3-di(4-pyridyl)propane
2-propyl-1H-imidazole-4,5-dicarboxylic acid
water
Conditions | Yield |
---|---|
In water High Pressure; Cd compd.:H2pimdc:bpp (1:1:5 molar ratio) in water, sealed, heated at 140°C for 3 d; crystd. on cooling to room temp., elem. anal.; | 66% |
1,10-Phenanthroline
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
In water High Pressure; hydrothermal synthesis; 3-propyl-4,5-dicarboxy-1H-imidazole, 1,10-phenanthroline, Cu salt, H2O stirred for 10 min; heated in a sealed Teflon-lined stainless steel autoclave at 170°C for 72 h; cooled to room temp. with 5°C/h; washed with H2O; dried in air; elem. anal.; | 66% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
diaquabis(2-propyl-1H-imidazole-4,5-dicarboxylate)manganese(II)
Conditions | Yield |
---|---|
In water; acetonitrile High Pressure; mixt. of MnSO4*H2O and imidazole dicarboxylic acid (1:1) in H2O/CH3CN heated in an autoclave at 152°C for 72 h; cooled to room temp. (10°C/h), collected, washed (h2O), dried (air), elem. anal.; | 65% |
2-propyl-1H-imidazole-4,5-dicarboxylic acid
1,4-phenylenediacetic acid
Conditions | Yield |
---|---|
In ethanol; water at 130℃; for 78h; pH=6; Autoclave; | 65% |
Conditions | Yield |
---|---|
With hydrogenchloride In acetonitrile at 100℃; for 99h; pH=2; Autoclave; High pressure; | 65% |
[2,2]bipyridinyl
2-propyl-1H-imidazole-4,5-dicarboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water; acetonitrile at 130℃; for 48h; pH=6; Sealed tube; High pressure; | 63% |
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