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inquiryN,N-Dimethylethylamine Chemical Properties Melting point −140 °C(lit.) Boiling point 36-38 °C(lit.) density 0.675 g/mL at 25 °C(lit.) vapor pressure 8.09 psi ( 20 °C) refractive index n20/D 1.372(lit.) Fp
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inquiryN,N-dimethylacetamide dimethyl acetal
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
With [1,4-bis(diphenylphosphino)butane](1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen at 25℃; under 3750.38 Torr; for 0.5h; Reagent/catalyst; | 96% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; Diethylselenium dibromide In tetrahydrofuran at 65℃; for 50h; | 92% |
With triphenylborane; methylphenylsilane In dichloromethane-d2 at 25℃; for 0.3h; Solvent; Temperature; Reagent/catalyst; Inert atmosphere; chemoselective reaction; | 76% |
With sodium tetrahydroborate; Bis-(2-bromoethyl)selenium dibromide In tetrahydrofuran at 65℃; for 50h; Product distribution; various other tertiary amides investigated; | 35% |
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 0.5h; Heating; other 1-alkyl-1,1-dimethylhydrazinium halides; | 57% |
With potassium hydroxide In methanol for 0.5h; Heating; Yield given; |
methyl magnesium iodide
N,N-Dimethylamino acetonitrile
A
N,N-dimethyl-ethanamine
B
dimethylaminoacetone
formic acid
N-ethylhexamethylenetetrammonium bromide
N,N-dimethyl-ethanamine
N,N-Dimethylamino acetonitrile
A
N,N-dimethyl-ethanamine
B
dimethylaminoacetone
Conditions | Yield |
---|---|
With methyl magnesium iodide; diethyl ether |
ethyl-dimethyl-sulfo-ammonium betaine
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
Hydrolysis; |
dimethyldiethylammonium chloride
A
methylene chloride
B
N,N-dimethyl-ethanamine
C
chloroethane
D
N,N-diethylnmethylamine
Conditions | Yield |
---|---|
bei der trocknen Destillation; |
Conditions | Yield |
---|---|
bei der Destillation; |
ethyl-dimethyl-propyl-ammonium; hydroxide
A
propene
B
N,N-dimethyl-ethanamine
C
ethene
D
N,N-dimethylaminopropane
Conditions | Yield |
---|---|
Destillation; |
ethyl-(2-hydroxy-ethyl)-dimethyl-ammonium; hydroxide
A
2-(N,N-dimethylamino)ethanol
B
N,N-dimethyl-ethanamine
C
ethene
D
acetaldehyde
Conditions | Yield |
---|---|
bei der Destillation; |
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
Zersetzt sich bei der Destillation; |
Conditions | Yield |
---|---|
bei der Destillation; |
ethyltrimethylammonium chloride
A
methylene chloride
B
N,N-dimethyl-ethanamine
C
chloroethane
D
trimethylamine
Conditions | Yield |
---|---|
bei der trocknen Destillation; |
Conditions | Yield |
---|---|
at 120 - 160℃; |
Conditions | Yield |
---|---|
at 154℃; Geschwindigkeit der Reaktion; |
diethyldimethylammonium iodide
ethanolamine
A
N,N-dimethyl-ethanamine
B
N,N-diethylnmethylamine
Conditions | Yield |
---|---|
With phenyl sodium; phenyllithium; cyclohexene |
1,3,5-triethyl-1,3,5-triazacyclohexane
mono-trimethylsilylphosphite
A
N,N-dimethyl-ethanamine
B
N-Ethylmethylamine
Conditions | Yield |
---|---|
With sodium butanolate In dimethyl sulfoxide; butan-1-ol at 70℃; Product distribution; study of substitution/elimination products ratio; |
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
With water Electrolysis.bei der Elektrolyse an einer Bleikathode; |
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
With sodium ethanolate at 150 - 160℃; |
A
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
bei der trocknen Destillation; |
N-ethyl-N,N-dimethyl-hydrazinium; chloride
acetic acid
N,N-dimethyl-ethanamine
water
ethyl-dimethyl-phenethyl-ammonium; iodide
A
styrene
B
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
die erhaltene waessrige Loesung der freien Base zersetzt sich von 100grad; |
Conditions | Yield |
---|---|
In dichloromethane at 50℃; for 24h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
In methanol at 125℃; under 2327.17 Torr; for 72h; | 99% |
(1R,2S,5R)-1-(chloromethoxy)-2-isopropyl-5-methylcyclohexane
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
In hexane at 20℃; for 0.5h; Menschutkin reaction; | 99% |
Conditions | Yield |
---|---|
With potassium iodide at 100℃; for 72h; Autoclave; | 99% |
With potassium iodide at 100℃; for 72h; Autoclave; | 99% |
N,N-dimethyl-ethanamine
1-chloro-2-diisopropylaminoethane hydrochloride
1-(2-diisopropylaminoethyl)dimethylethylammonium chloride
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile for 24h; Reflux; | 98% |
N,N-dimethyl-ethanamine
ethyl (3-bromopropyl)(diethoxymethyl)phosphinate
3-[(diethoxymethyl)(ethoxy)phosphoryl]-N-ethyl-N,N-dimethylpropan-1-aminium bromide
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 216h; | 97.6% |
N,N-dimethyl-ethanamine
Conditions | Yield |
---|---|
In diethyl ether at -5℃; for 72h; Substitution; | 97% |
N,N-dimethyl-ethanamine
2-(2-(2-(3-bromopropoxy)naphth-6-yl)-9,9-diethylfluoren-7-yl)-9,9-bis(4-ethoxyphenyl)-7-(4-methoxyphenyl)fluorene
C70H70NO4(1+)*Br(1-)
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 48h; Cooling with ice; | 95.4% |
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 15h; | 95.35% |
N,N-dimethyl-ethanamine
1-(3-bromopropoxy)-3,5-di(3,5-di(1-naphthyl)pheny)benzene
C65H54NO(1+)*Br(1-)
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 48h; Cooling with ice; | 95.2% |
Conditions | Yield |
---|---|
In chloroform at 20℃; for 18h; | 95% |
N,N-dimethyl-ethanamine
4-bromoethylbutanoate
4-ethoxy-N-ethyl-N,N-dimethyl-4-oxobutan-1-aminium bromide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; Product distribution / selectivity; Cooling in ice bath; | 94% |
In dichloromethane at 20℃; Cooling with ice; | 94% |
In acetonitrile at 20℃; for 72h; Product distribution / selectivity; | 94.8% |
In dichloromethane at 20℃; Cooling with ice; | 94% |
2-chlorobenzo[d][1,3]thiazole
N,N-dimethyl-ethanamine
A
2-dimethylaminobenzothiazole
B
Benzothiazol-2-yl-ethyl-methyl-amine
Conditions | Yield |
---|---|
In tetrahydrofuran at 100℃; under 6000480 Torr; for 96h; | A 5.5% B 94% |
N,N-dimethyl-ethanamine
(2-chloroethyl)dimethylamine hydrochloride
(2-dimethylaminoethyl)dimethylethylammonium chloride
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile for 24h; Reflux; | 94% |
N,N-dimethyl-ethanamine
2-(2-(2-(3-bromopropoxy)naphth-6-yl)-9,9-diethylfluoren-7-yl)-9,9-diethyl-7-(4-methoxy-phenyl)fluorene
C58H62NO2(1+)*Br(1-)
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 48h; Cooling with ice; | 94% |
N,N-dimethyl-ethanamine
4-Chloro-2,6-bis(trifluoromethyl)pyridine
A
(2,6-Bis-trifluoromethyl-pyridin-4-yl)-dimethyl-amine
B
(2,6-Bis-trifluoromethyl-pyridin-4-yl)-ethyl-methyl-amine
Conditions | Yield |
---|---|
In tetrahydrofuran at 100℃; under 6000480 Torr; for 96h; | A 7% B 93% |
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; | 93% |
In dichloromethane at 20℃; | 86% |
N,N-dimethyl-ethanamine
1-chloro-2-(2-methoxyethoxy)ethane
Conditions | Yield |
---|---|
With air In methanol at 50℃; for 360h; | 93% |
In tetrahydrofuran at 60℃; Sealed tube; | |
In tetrahydrofuran at 60℃; Sealed tube; |
N,N-dimethyl-ethanamine
Fe(C5H4BH2N(CH3)2C2H5)2
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In diethyl ether byproducts: (CH3)3SiH; (Schlenk, N2) (CH3)3SiCl in diethyl ether was added dropwise with stirring at -78°C to a soln. of complex and amine in diethyl ether, after 30 min the mixt. was allowed to warm to 0°C, stirred for 1 h, warmed to room temp.; filtered, reduced in vol., -30°C, 24 h; elem. anal.; | 92% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; | 91.7% |
In acetone at 5 - 15℃; for 6h; | |
In acetone at 10℃; for 3h; | 13.8g |
Conditions | Yield |
---|---|
With potassium iodide at 150℃; for 22h; Autoclave; | 91% |
With potassium iodide at 150℃; for 22h; Autoclave; | 91% |
Conditions | Yield |
---|---|
In neat (no solvent) (N2) NMe2Et was added at room temp. to Fe complex and stirred for 30 min; soln. was cooled to -78°C and slowly concd. in vacuo overnight; elem. anal.; | 90% |
N,N-dimethyl-ethanamine
C6H2-1,4-(BH2(NMe2Et)2-2,5-(Hex)2
Conditions | Yield |
---|---|
With (CH3)3SiCl In tetrahydrofuran under N2; soln. of amine in THF condensed onto solid B compd., warming to room temp., addn. of THF, addn. of (CH3)3SiCl at -196°C, warming to room temp., mixt. stirred overnight; evapn., residue stirred with ether/pentane (5/1) at room temp. for 1.5 h, filtration, filtrate freed under vac.; elem. anal.; | 90% |
N,N-dimethyl-ethanamine
C6H2-1,4-(BH2(NMe2Et)2-2,5-(Hex)2
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In tetrahydrofuran at -196 - 20℃; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
at 140℃; for 24h; Autoclave; | 90% |
at 140℃; for 24h; Autoclave; | 90% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; | 89.3% |
N,N-dimethyl-ethanamine
3-(Di-tert-butylmethylsilyl)-4,4-dimethyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-sila-1-cyclopenten
A
bis(trimethylsilyl)diazomethane
B
N-(Di-tert-butylmethylsilyl)dimethylsilanimin-Ethyldimethylamin
Conditions | Yield |
---|---|
In diethyl ether at -78℃; | A n/a B 88% |
N,N-dimethyl-ethanamine
dimethylsulfite
A
trimethylethylammonium methylsulfite
Conditions | Yield |
---|---|
In n-heptane at 10 - 20℃; for 4.16h; | A 86% B 86% |
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