Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Good quantity Storage:R.T. Package:as per buyers Application:intermediate Transportation:by air/sea
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Ouabain Application:Ouabain
Ouabain Package:inquiry Application:research use Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/FCL for large amount.
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of plant
Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHenan Fine Chemicals Co., LTD. is a diversified technology - oriented integrated company, which mainly concentrates on fine chemicals. Our company is committed to becom
Cas:630-60-4
Min.Order:0
Negotiable
Type:Trading Company
inquiryUnited Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
Ouabain Application:821353
Ouabain 630-60-4Appearance:solid or liquid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/
Ouabain Application:research use
Do best quality products, erect the morality model Application:please email us, thanks
Cas:630-60-4
Min.Order:0
Negotiable
Type:Other
inquiryOuabain Application:Ouabain
Supply top quality products with a reasonable price Application:api
Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
high purity Application:Drug intermediates Materials intermediates and active molecules
C52H58O16
ouabain
Conditions | Yield |
---|---|
With sodium carbonate In methanol at 20℃; for 1h; | 88% |
ouabain
trimethylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With pyridine at 20℃; for 1h; | 95% |
ouabain
Conditions | Yield |
---|---|
With 4-methyl-morpholine; 6C6H15P*4CF3O3S(1-)*2Ru(2+); acetone at 65℃; for 3.5h; Inert atmosphere; Sealed tube; | 92% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In tetrahydrofuran at 23℃; for 16h; | 91% |
ouabain
acetone
4-((3R,3aR,5R,5aS,5bR,9aR,11S,12aS,14aR,14bS)-5,12a,14b-trihydroxy-11-(((3aR,4R,6S,7S,7aR)-7-hydroxy-2,2,6-trimethyltetrahydro-4H-[1,3]dioxolo[4,5-c]pyran-4-yl)oxy)-3a,8,8-trimethylhexadecahydro-6H-cyclopenta[7,8]phenanthro[4,4a-d][1,3]dioxin-3-yl)furan-2(5H)-one
Conditions | Yield |
---|---|
With hydrogenchloride at 25℃; for 2h; | 89% |
With hydrogenchloride at 20℃; | 84% |
With hydrogenchloride In water at 20℃; for 2h; | 84% |
ouabain
acetic anhydride
(2R,3R,4R,5S,6S)-2-(((1R,3S,5S,10R,11R,13R,14S,17R)-1,11-diacetoxy-10-(acetoxymethyl)-5,14-dihydroxy-13-methyl-17-(5-oxo-2,5-dihydrofuran-3-yl)hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)oxy)-6-methyltetrahydro-2H-pyran-3,4,5-triyl triacetate
Conditions | Yield |
---|---|
Reflux; | 88% |
for 1.5h; Heating; | 71% |
With pyridine |
ouabain
triisopropylsilyl trifluoromethanesulfonate
3',19-di-[(triisopropylsilyl)oxy]-3β-[(α-L-rhamnopyranosyl)oxy]-1β,5,11α,14-tetrahydroxycard-20(22)-enolide
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 1.5h; | 88% |
With pyridine at 20℃; for 1h; | 33% |
ouabain
triisopropylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With pyridine at 20℃; for 1h; | 87% |
ouabain
(Z)-4-hydroxy-3-((1R,3S,5S,8R,9S,10R,11R,13R,14S,17R)-1,5,11,14-tetrahydroxy-10-(hydroxymethyl)-13-methyl-3-((2R,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyltetrahydro-2H-pyran-2-yloxy)hexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)but-2-enoic acid
Conditions | Yield |
---|---|
With lithium hydroxide In tetrahydrofuran at 20℃; Saponification; | 79% |
Conditions | Yield |
---|---|
Stage #1: ouabain With dihydroxy-methyl-borane In tetrahydrofuran; isopropyl alcohol Glovebox; Inert atmosphere; Stage #2: tert-butyl allyl carbonate With tris(dibenzylideneacetone)dipalladium chloroform complex; triphenylphosphine In tetrahydrofuran; isopropyl alcohol at 25℃; for 16.16h; Glovebox; Inert atmosphere; Sealed tube; | 74% |
ouabain
tert-butyldimethylsilyl chloride
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 2h; | 72% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen | 65% |
With water; palladium Hydrogenation; |
Conditions | Yield |
---|---|
Stage #1: tert-butyl allyl carbonate With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine In tetrahydrofuran for 0.5h; Glovebox; Inert atmosphere; Stage #2: ouabain With 1,3-dihydro-1-hydroxy-3-phenyl-2,1-benzoxaborole In tetrahydrofuran; isopropyl alcohol at 25℃; for 16h; Inert atmosphere; Glovebox; | 64.6% |
ouabain
1-epi-ouabain
Conditions | Yield |
---|---|
With 4-methyl-morpholine; 6C6H15P*4CF3O3S(1-)*2Ru(2+) In 2,2,2-trifluoroethanol at 70℃; for 11h; | 60% |
Multi-step reaction with 2 steps 1: 6C6H15P*4CF3O3S(1-)*2Ru(2+); 4-methyl-morpholine; acetone / 3.5 h / 65 °C / Inert atmosphere; Sealed tube 2: 6C6H15P*4CF3O3S(1-)*2Ru(2+); 4-methyl-morpholine; isopropyl alcohol / 2,2,2-trifluoroethanol / 1 h / 65 °C View Scheme |
ouabain
acetone
4-((3R,3aR,5R,5aS,5bR,9aR,11S,12aS,14aR,14bS)-5,11,12a,14b-tetrahydroxy-3a,8,8-trimethylhexadecahydro-6H-cyclopenta[7,8]phenanthro[4,4a-d][1,3]dioxin-3-yl)furan-2(5H)-one
Conditions | Yield |
---|---|
With hydrogenchloride at 20℃; | 55% |
With hydrogenchloride at 20℃; for 120h; Inert atmosphere; | 55% |
With hydrogenchloride |
Conditions | Yield |
---|---|
With copper(II) sulfate | 54% |
ouabain
triisopropylsilyl trifluoromethanesulfonate
B
3',19-di-[(triisopropylsilyl)oxy]-3β-[(α-L-rhamnopyranosyl)oxy]-1β,5,11α,14-tetrahydroxycard-20(22)-enolide
Conditions | Yield |
---|---|
With pyridine at 20℃; for 1h; | A 50% B 14% |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water | 43% |
Multi-step reaction with 3 steps 1: HCl / 23 °C 2: 97 percent / imidazole / acetonitrile; dimethylformamide / 12 h / 23 °C 3: 72 percent / aq. HCl / methanol / 4 h / 23 °C View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
With perchloric acid; acetic acid 1β,11α,19-triacetoxy-5-hydroxy-3β-O-acetyl-α-L-rhamnopyranosyloxy>-5β-carda-14,20(22)-dienolide; |
Conditions | Yield |
---|---|
With zinc(II) chloride |
Conditions | Yield |
---|---|
With copper(II) sulfate | |
With hydrogenchloride |
Conditions | Yield |
---|---|
With hydrogenchloride |
ouabain
Conditions | Yield |
---|---|
With water; oxygen; platinum β-dehydro-g-stropanthin; |
ouabain
Conditions | Yield |
---|---|
With methanol; potassium hydroxide Ansaeuern der Reaktionsloesung mit wss. Salzsaeure; |
ouabain
Conditions | Yield |
---|---|
With water; oxygen; platinum α-dehydro-g-stropanthin; |
Conditions | Yield |
---|---|
15 min; |
Conditions | Yield |
---|---|
With perchloric acid; acetic acid |
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