Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:63478-76-2
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Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
TIANFUCHEM--63478-76-2--High purity 6-Heptyn-1-ol in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 6-Heptyn-1-ol CAS No. 63478-76-2
Cas:63478-76-2
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: 6-Heptyn-1-ol Synonyms: HCT116[HCT116] Cell;6-HEPTYN-1-OL CAS: 63478-76-2 MF: C7H12O MW: 112.17 Appearance: Colorle
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inquiry6-Heptyn-1-ol CAS:63478-76-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
Cas:63478-76-2
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:63478-76-2
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:63478-76-2
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:63478-76-2
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inquiryProduct name: Hept-6-yn-1-ol CAS No.:63478-76-2 Molecule Formula:C7H12O Molecule Weight:112.17 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPEC
Cas:63478-76-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Name: 6-Heptyn-1-ol. Synonym: 6 muster HEPTYN Mustang 1 Mustang OL Matte 6 HeptynMuth1 Mustol >. CAS No: 63478-76-2. Molecular formula: C7H12O. Molecular weight: 112.17. Appearance: colorless transparent liquid. Purity: 98%. Meltin
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:63478-76-2
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:63478-76-2
Min.Order:1 bottle
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Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
3-heptyn-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With sodium hydride; Trimethylenediamine at 20℃; for 0.666667h; Isomerization; | 100% |
With potassium tert-butylate; sodium hydride; Trimethylenediamine In mineral oil at 20 - 70℃; for 3h; | 99% |
With potassium tert-butylate; lithium; Trimethylenediamine at 20℃; for 2h; | 97% |
hept-6-ynoic acid
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | 100% |
Stage #1: hept-6-ynoic acid With lithium aluminium tetrahydride In diethyl ether at 0 - 20℃; Stage #2: With hydrogenchloride In diethyl ether for 0.5h; | 89% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 3h; Inert atmosphere; | 82% |
hep-2-yn-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With potassium hydride; 1,2-diaminopropan In tetrahydrofuran; mineral oil at 20℃; for 24h; Inert atmosphere; | 99% |
With potassium salt of 1,3-diaminopropane In tetrahydrofuran at 0℃; for 0.5h; | 97% |
With potassium tert-butylate; lithium; Trimethylenediamine at 20℃; for 3h; Inert atmosphere; | 90% |
tetrahydro-2-(6-heptynyloxy)-2H-pyran
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With acid | 98% |
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With water; sodium hydroxide In methanol | 95% |
methyl hept-6-ynoate
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 1.5h; Heating; | 91% |
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 2h; Yield given; | |
With methanol; sodium tetrahydroborate In tetrahydrofuran for 3.25h; Reflux; | 2.15 g |
7-(trimethylsilyl)hept-6-yn-1-yl acetate
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With water; potassium carbonate In methanol at 20℃; for 5h; | 82% |
hept-5-yn-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With sodium amide; Trimethylenediamine In ammonia | 79% |
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.333333h; Dehydrobromination; | 70% |
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran at -78 - 20℃; | 63% |
7-chlorohept-1-yne
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Ueberfuehrung ueber das Jodid in das Acetat und folgende Hydrolyse; | |
(i) DMF, KOAc, (ii) NaOH, aq. EtOH; Multistep reaction; |
6-bromohept-6-en-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With ammonia; sodium amide |
Conditions | Yield |
---|---|
With 3,4-dihydro-2H-pyran Multistep reaction; |
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20℃; |
2-nonyn-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With potassium tert-butylate; lithium; Trimethylenediamine |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 87 percent / n-BuLi / tetrahydrofuran / -78 - 20 °C 2: 79 percent / KH; 1,3-diaminopropane / 2 h / cooling View Scheme | |
Multi-step reaction with 2 steps 1: 87 percent / n-BuLi / tetrahydrofuran; hexane / Heating 2: 70 percent / KH; H2N(CH2)2NH2 / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-BuLi / tetrahydrofuran / 1 h / -78 °C 1.2: 99 percent / tetrahydrofuran / 18 h / -78 - 20 °C 2.1: 67 percent / potassium hydride / various solvent(s) / 1.5 h / 10 - 15 °C View Scheme |
non-2-ynyl tetrahydropyran-2-yl ether
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: PPTS / ethanol / 3 h / 25 °C 2: H2N(CH2)3NH2; Li; t-BuOK View Scheme |
1,6-hexanediol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: NaH / tetrahydrofuran / 20 °C 2: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C 3: PPh3 / CH2Cl2 / 20 °C 4: n-BuLi / tetrahydrofuran / 0 °C 5: aq. HCl / methanol / 20 °C View Scheme |
6-((triisopropylsilyl)oxy)hexanal
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: PPh3 / CH2Cl2 / 20 °C 2: n-BuLi / tetrahydrofuran / 0 °C 3: aq. HCl / methanol / 20 °C View Scheme |
6-{[tris(propan-2-yl)silyl]oxy}hexan-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C 2: PPh3 / CH2Cl2 / 20 °C 3: n-BuLi / tetrahydrofuran / 0 °C 4: aq. HCl / methanol / 20 °C View Scheme |
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: n-BuLi / tetrahydrofuran / 0 °C 2: aq. HCl / methanol / 20 °C View Scheme |
5-bromopentanoic acid
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dimethylsulfoxide / 2 h 2: SOCl2 / 3 h / Heating 3: 91 percent / LiAlH4 / tetrahydrofuran / 1.5 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: NH3 / tetrahydrofuran / 15 h 2: diethyl ether 3: LiAlH4 / diethyl ether / 2 h / 0 °C View Scheme |
TETRAHYDROPYRANE
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ZnBr2 2: K2CO3 / methanol 3: 1.) dihydropyran, 2.) deprotection View Scheme |
5-bromo-1-pentanyl acetate
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3 / methanol 2: 1.) dihydropyran, 2.) deprotection View Scheme |
2-(chloromethyl)tetrahydropyran
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 83 percent / NaNH2 / liquid ammonia 2: 54 percent / LiNH2 / liquid ammonia 3: 79 percent / NaNH2, H2N-(CH2)3-NH2 / liquid ammonia View Scheme |
Tetrahydropyran-2-methanol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: SOCl2, pyridine 2: 83 percent / NaNH2 / liquid ammonia 3: 54 percent / LiNH2 / liquid ammonia 4: 79 percent / NaNH2, H2N-(CH2)3-NH2 / liquid ammonia View Scheme |
5-hexyl-1-ol
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 54 percent / LiNH2 / liquid ammonia 2: 79 percent / NaNH2, H2N-(CH2)3-NH2 / liquid ammonia View Scheme |
hex-1-yne
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / n-BuLi / tetrahydrofuran 2: 46 percent / KH, 1,3-Diaminopropane View Scheme | |
Multi-step reaction with 2 steps 1: n-butyllithium / diethyl ether / 0 °C 2: sodium hydride; ethylenediamine / 60 °C View Scheme |
3,4-dihydro-2H-pyran
1-hydroxy-6-heptyne
tetrahydro-2-(6-heptynyloxy)-2H-pyran
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In dichloromethane at 20℃; | 100% |
With toluene-4-sulfonic acid | 98% |
camphor-10-sulfonic acid In dichloromethane at 0 - 20℃; | 97% |
1-hydroxy-6-heptyne
tert-butyldimethylsilyl chloride
tert-butyl(hept-6-yn-1-yloxy)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; for 24h; | 100% |
With 1H-imidazole In dichloromethane at 20℃; for 24h; | 100% |
With pyridine; 1H-imidazole at 20℃; for 0.5h; | 99% |
1-hydroxy-6-heptyne
2-bromo-4'-methoxy-benzophenone
Conditions | Yield |
---|---|
Stage #1: 2-bromo-4'-methoxy-benzophenone With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 20℃; for 0.5h; Sealed tube; Inert atmosphere; Stage #2: 1-hydroxy-6-heptyne at 85℃; for 48h; Sealed tube; Inert atmosphere; | 99% |
1-hydroxy-6-heptyne
o-iodo-methyl-benzoic acid
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 15h; Sonogashira Cross-Coupling; Inert atmosphere; | 99% |
1-hydroxy-6-heptyne
hept-5-yn-1-ol
Conditions | Yield |
---|---|
With potassium hydroxide | 98% |
With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 3h; | 88% |
1-hydroxy-6-heptyne
hept-6-ynal
Conditions | Yield |
---|---|
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -60 - 0℃; Swern oxidation; | 98% |
With fluorosulfonyl fluoride; potassium carbonate; dimethyl sulfoxide at 20℃; for 12h; chemoselective reaction; | 89% |
With sulfur trioxide pyridine complex; triethylamine In dichloromethane; dimethyl sulfoxide at 20℃; for 1h; Schlenk technique; | 87% |
1-hydroxy-6-heptyne
tert-butylchlorodiphenylsilane
tert-butyl(hept-6-yn-1-yloxy)diphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 25℃; | 98% |
With 1H-imidazole In dichloromethane at 0 - 20℃; | 94% |
With 1H-imidazole In dichloromethane at 0 - 20℃; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
Stage #1: 1-hydroxy-6-heptyne With dmap; n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane for 2h; Inert atmosphere; | 97% |
Stage #1: 1-hydroxy-6-heptyne With dmap; n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane for 2h; Inert atmosphere; | 92% |
Stage #1: 1-hydroxy-6-heptyne With dmap; n-butyllithium In tetrahydrofuran; hexane at -78℃; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; | 80% |
Stage #1: 1-hydroxy-6-heptyne With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; for 15h; Inert atmosphere; | 70% |
Stage #1: 1-hydroxy-6-heptyne With n-butyllithium In tetrahydrofuran; hexane at -78 - 0℃; for 0.333333h; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; | 61% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine for 7h; Sonogashira Cross-Coupling; Inert atmosphere; | 97% |
1-hydroxy-6-heptyne
7-iodo-6-heptyn-1-ol
Conditions | Yield |
---|---|
With potassium hydroxide; iodine In methanol; water at 20℃; for 4h; | 94% |
With potassium hydroxide; iodine In methanol at 20℃; for 4h; | 94% |
Stage #1: 1-hydroxy-6-heptyne With potassium hydroxide In methanol; water at 0℃; for 0.166667h; Stage #2: With iodine In methanol; water at 0 - 20℃; | 77% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 3h; Sonogashira Cross-Coupling; Inert atmosphere; | 93% |
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With silver(I) azide; trimethylsilylazide; water In dimethyl sulfoxide at 80℃; Reagent/catalyst; | 93% |
1-hydroxy-6-heptyne
benzyl bromide
((hept-6-yn-1-yloxy)methyl)benzene
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium hydride In tetrahydrofuran; diethyl ether for 3h; cooling; | 92% |
With sodium hydride In tetrahydrofuran at 0℃; | 78% |
1-hydroxy-6-heptyne
p-methoxybenzyl chloride
1-((hept-6-yn-1-yloxy)methyl)-4-methoxybenzene
Conditions | Yield |
---|---|
Stage #1: 1-hydroxy-6-heptyne With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Inert atmosphere; Stage #2: p-methoxybenzyl chloride With tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; | 92% |
Stage #1: 1-hydroxy-6-heptyne With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Inert atmosphere; Stage #2: p-methoxybenzyl chloride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 18h; Inert atmosphere; | 87% |
4-cyanopyridine N-oxide
1-hydroxy-6-heptyne
Conditions | Yield |
---|---|
With potassium fluoride; water; trifluoroacetic acid; nickel dichloride; zinc In N,N-dimethyl acetamide at 30℃; for 24h; | 92% |
1-hydroxy-6-heptyne
p-toluenesulfonyl chloride
hept-6-yn-1-yl 4-methylbenzenesulfonate
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; Inert atmosphere; | 91% |
With pyridine | 87% |
With dmap; triethylamine Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 1h; | 91% |
1-hydroxy-6-heptyne
4-Iodobenzotrifluoride
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) at 20℃; Sonogashira reaction; | 91% |
1-hydroxy-6-heptyne
7-bromo-hept-1-yne
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine In dichloromethane at 20℃; for 1h; Cooling with ice; | 91% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0℃; for 1.5h; Inert atmosphere; | 86% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 20℃; for 1h; Inert atmosphere; | 83% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; | 54% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; Appel Halogenation; |
Conditions | Yield |
---|---|
With pyridine | 90% |
With dmap; triethylamine In dichloromethane at 20℃; for 5h; | 86% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 3.44 g |
1-hydroxy-6-heptyne
1-iodo-octa-1,3-diyne
pentadeca-6,8,10-triyn-1-ol
Conditions | Yield |
---|---|
With pyrrolidine; copper(l) iodide | 90% |
Conditions | Yield |
---|---|
With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine In tetrahydrofuran at 20℃; Sonogashira Cross-Coupling; Inert atmosphere; | 90% |
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) at 20℃; Sonogashira reaction; | 87% |
With bis-triphenylphosphine-palladium(II) chloride; diethylamine; copper(l) chloride at 0 - 20℃; Sonogashira coupling; Inert atmosphere; | 39% |
With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In toluene at 20℃; for 2h; |
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; | 90% |
4-bromo-2-methylbut-3-yn-2-ol
1-hydroxy-6-heptyne
10-methylundeca-6,8-diyne-1,10-diol
Conditions | Yield |
---|---|
Stage #1: 1-hydroxy-6-heptyne With propylamine; hydroxylamine hydrochloride; copper(l) chloride In water at 0℃; for 0.166667h; Cadiot-Chodkiewicz procedure; Stage #2: 4-bromo-2-methylbut-3-yn-2-ol In tetrahydrofuran at 0℃; Cadiot-Chodkiewicz procedure; | 90% |
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