Products

Refine

Country

Business Type

Certificate

Display

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 6-Heptynoic Alcohol supplier in China

Cas:63478-76-2

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 6-Heptynoic Alcohol

Cas:63478-76-2

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM--63478-76-2--High purity 6-Heptyn-1-ol in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business

TIANFUCHEM--63478-76-2--High purity 6-Heptyn-1-ol in stock

Cas:63478-76-2

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 6-Heptyn-1-ol CAS No. 63478-76-2

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:1 Gram

FOB Price: $12.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 63478-76-2 with competitive price

Cas:63478-76-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 6-Heptyn-1-ol Synonyms: HCT116[HCT116] Cell;6-HEPTYN-1-OL CAS: 63478-76-2 MF: C7H12O MW: 112.17 Appearance: Colorle

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

6-Heptyn-1-ol 63478-76-2

Cas:63478-76-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

6-Heptyn-1-ol CAS:63478-76-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia

6-Heptyn-1-ol CAS:63478-76-2

Cas:63478-76-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:63478-76-2

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1. Customs clearance 1) By Express: Normally there is no specical need for the recipient to clear the customs. If the customs has an objection,our rich experienced and professional group will help you clear the customs. 2) By Air and by Sea: Our

Best Price CAS 63478-76-2 6-Heptyn-1-ol C7H12O 99%

Cas:63478-76-2

Min.Order:20 Kilogram

FOB Price: $10.0 / 25.0

Type:Trading Company

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

6-Heptynoic Alcohol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 6-Heptynoic Alcohol

Cas:63478-76-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: Hept-6-yn-1-ol CAS No.:63478-76-2 Molecule Formula:C7H12O Molecule Weight:112.17 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPEC

Best Quality Hept-6-yn-1-ol with good supplier

Cas:63478-76-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Name: 6-Heptyn-1-ol. Synonym: 6 muster HEPTYN Mustang 1 Mustang OL Matte 6 HeptynMuth1 Mustol >. CAS No: 63478-76-2. Molecular formula: C7H12O. Molecular weight: 112.17. Appearance: colorless transparent liquid. Purity: 98%. Meltin

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

6-Heptyn-1-ol Cas no.63478-76-2 98%

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 6-Heptyn-1-ol 100g

Cas:63478-76-2

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

6-Heptynoic Alcohol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

6-Heptyn-1-ol

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

6-Heptyn-1-ol CAS No.63478-76-2

Cas:63478-76-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

3-heptyn-1-ol
14916-79-1

3-heptyn-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With sodium hydride; Trimethylenediamine at 20℃; for 0.666667h; Isomerization;100%
With potassium tert-butylate; sodium hydride; Trimethylenediamine In mineral oil at 20 - 70℃; for 3h;99%
With potassium tert-butylate; lithium; Trimethylenediamine at 20℃; for 2h;97%
hept-6-ynoic acid
30964-00-2

hept-6-ynoic acid

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With lithium aluminium tetrahydride100%
Stage #1: hept-6-ynoic acid With lithium aluminium tetrahydride In diethyl ether at 0 - 20℃;
Stage #2: With hydrogenchloride In diethyl ether for 0.5h;
89%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 3h; Inert atmosphere;82%
hep-2-yn-1-ol
1002-36-4

hep-2-yn-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With potassium hydride; 1,2-diaminopropan In tetrahydrofuran; mineral oil at 20℃; for 24h; Inert atmosphere;99%
With potassium salt of 1,3-diaminopropane In tetrahydrofuran at 0℃; for 0.5h;97%
With potassium tert-butylate; lithium; Trimethylenediamine at 20℃; for 3h; Inert atmosphere;90%
tetrahydro-2-(6-heptynyloxy)-2H-pyran
37011-86-2

tetrahydro-2-(6-heptynyloxy)-2H-pyran

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With acid98%
7-(trimethylsilyl)hept-6-yn-1-ol

7-(trimethylsilyl)hept-6-yn-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With water; sodium hydroxide In methanol95%
methyl hept-6-ynoate
56909-02-5

methyl hept-6-ynoate

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 1.5h; Heating;91%
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 2h; Yield given;
With methanol; sodium tetrahydroborate In tetrahydrofuran for 3.25h; Reflux;2.15 g
7-(trimethylsilyl)hept-6-yn-1-yl acetate
1360871-35-7

7-(trimethylsilyl)hept-6-yn-1-yl acetate

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With water; potassium carbonate In methanol at 20℃; for 5h;82%
hept-5-yn-1-ol
58944-42-6

hept-5-yn-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With sodium amide; Trimethylenediamine In ammonia79%
7,7-dibromo-6-hepten-1-ol

7,7-dibromo-6-hepten-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.333333h; Dehydrobromination;70%
3-oxocyclohept-1-en-1-yl trifluoromethanesulfonate

3-oxocyclohept-1-en-1-yl trifluoromethanesulfonate

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With lithium triethylborohydride In tetrahydrofuran at -78 - 20℃;63%
7-chlorohept-1-yne
18804-36-9

7-chlorohept-1-yne

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Ueberfuehrung ueber das Jodid in das Acetat und folgende Hydrolyse;
(i) DMF, KOAc, (ii) NaOH, aq. EtOH; Multistep reaction;
6-bromohept-6-en-1-ol
98434-66-3

6-bromohept-6-en-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With ammonia; sodium amide
5-bromopentan-1-ol
34626-51-2

5-bromopentan-1-ol

lithium acetylide
70277-75-7

lithium acetylide

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With 3,4-dihydro-2H-pyran Multistep reaction;
1-(triisopropylsiloxy)hept-6-yne

1-(triisopropylsiloxy)hept-6-yne

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With hydrogenchloride In methanol at 20℃;
2-nonyn-1-ol
5921-73-3

2-nonyn-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
With potassium tert-butylate; lithium; Trimethylenediamine
hex-1-yne
693-02-7

hex-1-yne

[Co2(CO)8]

[Co2(CO)8]

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 87 percent / n-BuLi / tetrahydrofuran / -78 - 20 °C
2: 79 percent / KH; 1,3-diaminopropane / 2 h / cooling
View Scheme
Multi-step reaction with 2 steps
1: 87 percent / n-BuLi / tetrahydrofuran; hexane / Heating
2: 70 percent / KH; H2N(CH2)2NH2 / 20 °C
View Scheme
hex-1-yne
693-02-7

hex-1-yne

iodo- or bromobenzene

iodo- or bromobenzene

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: n-BuLi / tetrahydrofuran / 1 h / -78 °C
1.2: 99 percent / tetrahydrofuran / 18 h / -78 - 20 °C
2.1: 67 percent / potassium hydride / various solvent(s) / 1.5 h / 10 - 15 °C
View Scheme
non-2-ynyl tetrahydropyran-2-yl ether
83583-29-3

non-2-ynyl tetrahydropyran-2-yl ether

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: PPTS / ethanol / 3 h / 25 °C
2: H2N(CH2)3NH2; Li; t-BuOK
View Scheme
1,6-hexanediol
629-11-8

1,6-hexanediol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: NaH / tetrahydrofuran / 20 °C
2: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C
3: PPh3 / CH2Cl2 / 20 °C
4: n-BuLi / tetrahydrofuran / 0 °C
5: aq. HCl / methanol / 20 °C
View Scheme
6-((triisopropylsilyl)oxy)hexanal
245124-09-8

6-((triisopropylsilyl)oxy)hexanal

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: PPh3 / CH2Cl2 / 20 °C
2: n-BuLi / tetrahydrofuran / 0 °C
3: aq. HCl / methanol / 20 °C
View Scheme
6-{[tris(propan-2-yl)silyl]oxy}hexan-1-ol
146952-70-7

6-{[tris(propan-2-yl)silyl]oxy}hexan-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 °C
2: PPh3 / CH2Cl2 / 20 °C
3: n-BuLi / tetrahydrofuran / 0 °C
4: aq. HCl / methanol / 20 °C
View Scheme
7,7-dibromo-1-(triisopropylsiloxy)hept-6-ene

7,7-dibromo-1-(triisopropylsiloxy)hept-6-ene

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: n-BuLi / tetrahydrofuran / 0 °C
2: aq. HCl / methanol / 20 °C
View Scheme
5-bromopentanoic acid
2067-33-6

5-bromopentanoic acid

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dimethylsulfoxide / 2 h
2: SOCl2 / 3 h / Heating
3: 91 percent / LiAlH4 / tetrahydrofuran / 1.5 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: NH3 / tetrahydrofuran / 15 h
2: diethyl ether
3: LiAlH4 / diethyl ether / 2 h / 0 °C
View Scheme
TETRAHYDROPYRANE
142-68-7

TETRAHYDROPYRANE

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: ZnBr2
2: K2CO3 / methanol
3: 1.) dihydropyran, 2.) deprotection
View Scheme
5-bromo-1-pentanyl acetate
15848-22-3

5-bromo-1-pentanyl acetate

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: K2CO3 / methanol
2: 1.) dihydropyran, 2.) deprotection
View Scheme
2-(chloromethyl)tetrahydropyran
18420-41-2, 130233-13-5, 130233-14-6

2-(chloromethyl)tetrahydropyran

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 83 percent / NaNH2 / liquid ammonia
2: 54 percent / LiNH2 / liquid ammonia
3: 79 percent / NaNH2, H2N-(CH2)3-NH2 / liquid ammonia
View Scheme
Tetrahydropyran-2-methanol
100-72-1

Tetrahydropyran-2-methanol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: SOCl2, pyridine
2: 83 percent / NaNH2 / liquid ammonia
3: 54 percent / LiNH2 / liquid ammonia
4: 79 percent / NaNH2, H2N-(CH2)3-NH2 / liquid ammonia
View Scheme
5-hexyl-1-ol
928-90-5

5-hexyl-1-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 54 percent / LiNH2 / liquid ammonia
2: 79 percent / NaNH2, H2N-(CH2)3-NH2 / liquid ammonia
View Scheme
hex-1-yne
693-02-7

hex-1-yne

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95 percent / n-BuLi / tetrahydrofuran
2: 46 percent / KH, 1,3-Diaminopropane
View Scheme
Multi-step reaction with 2 steps
1: n-butyllithium / diethyl ether / 0 °C
2: sodium hydride; ethylenediamine / 60 °C
View Scheme
3,4-dihydro-2H-pyran
110-87-2

3,4-dihydro-2H-pyran

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

tetrahydro-2-(6-heptynyloxy)-2H-pyran
37011-86-2

tetrahydro-2-(6-heptynyloxy)-2H-pyran

Conditions
ConditionsYield
With toluene-4-sulfonic acid In dichloromethane at 20℃;100%
With toluene-4-sulfonic acid98%
camphor-10-sulfonic acid In dichloromethane at 0 - 20℃;97%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

tert-butyl(hept-6-yn-1-yloxy)dimethylsilane
119837-81-9

tert-butyl(hept-6-yn-1-yloxy)dimethylsilane

Conditions
ConditionsYield
With 1H-imidazole In dichloromethane at 20℃; for 24h;100%
With 1H-imidazole In dichloromethane at 20℃; for 24h;100%
With pyridine; 1H-imidazole at 20℃; for 0.5h;99%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

2-bromo-4'-methoxy-benzophenone
59142-63-1

2-bromo-4'-methoxy-benzophenone

(2-(7-hydroxyhept-1-yn-1-yl)phenyl)(4-methoxyphenyl)methanone

(2-(7-hydroxyhept-1-yn-1-yl)phenyl)(4-methoxyphenyl)methanone

Conditions
ConditionsYield
Stage #1: 2-bromo-4'-methoxy-benzophenone With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine at 20℃; for 0.5h; Sealed tube; Inert atmosphere;
Stage #2: 1-hydroxy-6-heptyne at 85℃; for 48h; Sealed tube; Inert atmosphere;
99%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

o-iodo-methyl-benzoic acid
610-97-9

o-iodo-methyl-benzoic acid

methyl 2-(7-hydroxyhept-1-ynyl)benzoate

methyl 2-(7-hydroxyhept-1-ynyl)benzoate

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 15h; Sonogashira Cross-Coupling; Inert atmosphere;99%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

hept-5-yn-1-ol
58944-42-6

hept-5-yn-1-ol

Conditions
ConditionsYield
With potassium hydroxide98%
With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 3h;88%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

hept-6-ynal
67100-10-1

hept-6-ynal

Conditions
ConditionsYield
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -60 - 0℃; Swern oxidation;98%
With fluorosulfonyl fluoride; potassium carbonate; dimethyl sulfoxide at 20℃; for 12h; chemoselective reaction;89%
With sulfur trioxide pyridine complex; triethylamine In dichloromethane; dimethyl sulfoxide at 20℃; for 1h; Schlenk technique;87%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

tert-butylchlorodiphenylsilane
58479-61-1

tert-butylchlorodiphenylsilane

tert-butyl(hept-6-yn-1-yloxy)diphenylsilane
106027-21-8

tert-butyl(hept-6-yn-1-yloxy)diphenylsilane

Conditions
ConditionsYield
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 25℃;98%
With 1H-imidazole In dichloromethane at 0 - 20℃;94%
With 1H-imidazole In dichloromethane at 0 - 20℃; Inert atmosphere;89%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

7-(trimethylsilyl)hept-6-yn-1-ol

7-(trimethylsilyl)hept-6-yn-1-ol

Conditions
ConditionsYield
Stage #1: 1-hydroxy-6-heptyne With dmap; n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane for 2h; Inert atmosphere;
97%
Stage #1: 1-hydroxy-6-heptyne With dmap; n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane for 2h; Inert atmosphere;
92%
Stage #1: 1-hydroxy-6-heptyne With dmap; n-butyllithium In tetrahydrofuran; hexane at -78℃;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃;
80%
Stage #1: 1-hydroxy-6-heptyne With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; for 15h; Inert atmosphere;
70%
Stage #1: 1-hydroxy-6-heptyne With n-butyllithium In tetrahydrofuran; hexane at -78 - 0℃; for 0.333333h;
Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃;
61%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

1-Bromo-3-iodobenzene
591-18-4

1-Bromo-3-iodobenzene

7-(3-bromophenyl)hept-6-yn-1-ol

7-(3-bromophenyl)hept-6-yn-1-ol

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine for 7h; Sonogashira Cross-Coupling; Inert atmosphere;97%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

7-iodo-6-heptyn-1-ol
164470-73-9

7-iodo-6-heptyn-1-ol

Conditions
ConditionsYield
With potassium hydroxide; iodine In methanol; water at 20℃; for 4h;94%
With potassium hydroxide; iodine In methanol at 20℃; for 4h;94%
Stage #1: 1-hydroxy-6-heptyne With potassium hydroxide In methanol; water at 0℃; for 0.166667h;
Stage #2: With iodine In methanol; water at 0 - 20℃;
77%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

C10H12ClIO4

C10H12ClIO4

C17H23ClO5

C17H23ClO5

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; for 3h; Sonogashira Cross-Coupling; Inert atmosphere;93%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

C7H13N3O

C7H13N3O

Conditions
ConditionsYield
With silver(I) azide; trimethylsilylazide; water In dimethyl sulfoxide at 80℃; Reagent/catalyst;93%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

benzyl bromide
100-39-0

benzyl bromide

((hept-6-yn-1-yloxy)methyl)benzene
565473-04-3

((hept-6-yn-1-yloxy)methyl)benzene

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide; potassium hydride In tetrahydrofuran; diethyl ether for 3h; cooling;92%
With sodium hydride In tetrahydrofuran at 0℃;78%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

p-methoxybenzyl chloride
824-94-2

p-methoxybenzyl chloride

1-((hept-6-yn-1-yloxy)methyl)-4-methoxybenzene
1226762-13-5

1-((hept-6-yn-1-yloxy)methyl)-4-methoxybenzene

Conditions
ConditionsYield
Stage #1: 1-hydroxy-6-heptyne With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Inert atmosphere;
Stage #2: p-methoxybenzyl chloride With tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere;
92%
Stage #1: 1-hydroxy-6-heptyne With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Inert atmosphere;
Stage #2: p-methoxybenzyl chloride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 18h; Inert atmosphere;
87%
4-cyanopyridine N-oxide
14906-59-3

4-cyanopyridine N-oxide

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

7-hydroxy-2-methyleneheptanenitrile

7-hydroxy-2-methyleneheptanenitrile

Conditions
ConditionsYield
With potassium fluoride; water; trifluoroacetic acid; nickel dichloride; zinc In N,N-dimethyl acetamide at 30℃; for 24h;92%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

hept-6-yn-1-yl 4-methylbenzenesulfonate
87462-63-3

hept-6-yn-1-yl 4-methylbenzenesulfonate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃; Inert atmosphere;91%
With pyridine87%
With dmap; triethylamine Inert atmosphere;84%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

benzoyl chloride
98-88-4

benzoyl chloride

hept-6-yn-1-yl benzoate
159614-47-8

hept-6-yn-1-yl benzoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 1h;91%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

4-Iodobenzotrifluoride
455-13-0

4-Iodobenzotrifluoride

7-(4-trifluoromethyl-phenyl)-hept-6-yn-1-ol

7-(4-trifluoromethyl-phenyl)-hept-6-yn-1-ol

Conditions
ConditionsYield
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) at 20℃; Sonogashira reaction;91%
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

7-bromo-hept-1-yne
81216-14-0

7-bromo-hept-1-yne

Conditions
ConditionsYield
With carbon tetrabromide; triphenylphosphine In dichloromethane at 20℃; for 1h; Cooling with ice;91%
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0℃; for 1.5h; Inert atmosphere;86%
With carbon tetrabromide; triphenylphosphine In dichloromethane at 20℃; for 1h; Inert atmosphere;83%
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃;54%
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; Appel Halogenation;
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

acetic anhydride
108-24-7

acetic anhydride

hept-6-yn-1-yl acetate
93184-64-6

hept-6-yn-1-yl acetate

Conditions
ConditionsYield
With pyridine90%
With dmap; triethylamine In dichloromethane at 20℃; for 5h;86%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere;3.44 g
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

1-iodo-octa-1,3-diyne
333754-02-2

1-iodo-octa-1,3-diyne

pentadeca-6,8,10-triyn-1-ol
333753-97-2

pentadeca-6,8,10-triyn-1-ol

Conditions
ConditionsYield
With pyrrolidine; copper(l) iodide90%
iodobenzene
591-50-4

iodobenzene

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

7-phenyl-hept-6-yn-1-ol
335353-53-2

7-phenyl-hept-6-yn-1-ol

Conditions
ConditionsYield
With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine In tetrahydrofuran at 20℃; Sonogashira Cross-Coupling; Inert atmosphere;90%
With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) at 20℃; Sonogashira reaction;87%
With bis-triphenylphosphine-palladium(II) chloride; diethylamine; copper(l) chloride at 0 - 20℃; Sonogashira coupling; Inert atmosphere;39%
With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In toluene at 20℃; for 2h;
1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

1-bromo-octane
111-83-1

1-bromo-octane

pentadec-6-yn-1-ol
105090-57-1

pentadec-6-yn-1-ol

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere;90%
4-bromo-2-methylbut-3-yn-2-ol
2063-19-6

4-bromo-2-methylbut-3-yn-2-ol

1-hydroxy-6-heptyne
63478-76-2

1-hydroxy-6-heptyne

10-methylundeca-6,8-diyne-1,10-diol
1308271-41-1

10-methylundeca-6,8-diyne-1,10-diol

Conditions
ConditionsYield
Stage #1: 1-hydroxy-6-heptyne With propylamine; hydroxylamine hydrochloride; copper(l) chloride In water at 0℃; for 0.166667h; Cadiot-Chodkiewicz procedure;
Stage #2: 4-bromo-2-methylbut-3-yn-2-ol In tetrahydrofuran at 0℃; Cadiot-Chodkiewicz procedure;
90%

Hot Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View