1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:676-75-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryDIMETHYLARSENIC IODIDE CAS:676-75-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
Cas:676-75-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:676-75-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:676-75-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:676-75-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Cas:676-75-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:676-75-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
Cas:676-75-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the Dimethyliodoarsine, CAS:676-75-5 with the most competitive price and the best quality
Arsinous iodide,dimethyl- (9CI)Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,B
Supply top quality products with a reasonable price Application:api
Conditions | Yield |
---|---|
With sulfuric acid; sulfur dioxide; potassium iodide In water for 3h; | 76% |
With sulfuric acid; sulfur dioxide; potassium iodide | |
With hydrogenchloride; sulfur dioxide; potassium iodide | |
Multistep reaction; | |
With sulfuric acid; sulfur dioxide; potassium iodide In water |
Conditions | Yield |
---|---|
With hydrogenchloride; sulfur dioxide; potassium iodide In water for 2h; | 54% |
triphenyl phosphite
A
dimethyliodoarsine
B
O,O,O-triphenyl phosphorothioate
Conditions | Yield |
---|---|
In chloroform-d1 for 6h; | A 22% B n/a |
Conditions | Yield |
---|---|
With ethanol; potassium iodide unter Luftausschluss; | |
With acetone; sodium iodide unter Luftausschluss; |
Conditions | Yield |
---|---|
With hydrogen iodide bei der Destillation; |
Conditions | Yield |
---|---|
Zersetzt sich beim Erhitzen; |
tetramethyldiarsine
methyl iodide
A
dimethyliodoarsine
B
tetramethylarsonium iodide
Conditions | Yield |
---|---|
analog reagiert Aethyljodid; |
Conditions | Yield |
---|---|
With sodium hydroxide; ethanol und reduziert das Reaktionsprodukt in salzsaurer Loesung mit Schwefeldioxyd; | |
With sodium hydroxide anschliessend mit wss.HCl und SO2; |
Conditions | Yield |
---|---|
With arsenic |
Conditions | Yield |
---|---|
With hydrogen iodide In dichloromethane |
Conditions | Yield |
---|---|
With Iodine monochloride |
dimethyliodoarsine
Conditions | Yield |
---|---|
bei der Destillation; |
Dimethylarsinic acid
hydrogen iodide
A
dimethyliodoarsine
B
water
C
iodine
methyl iodide
A
dimethyliodoarsine
B
arsenic triiodide
C
tetramethylarsonium iodide
D
methyldiiodoarsine
Conditions | Yield |
---|---|
In not given reaction of CH3I with amorphous As at room temperature;; |
cacodyl sulfide
dimethyl iodoborane
A
dimethyliodoarsine
B
(CH3)2AsSB(CH3)2
triphenylphosphine
A
dimethyliodoarsine
B
dimethylarsino dimethyldithioarsinate
C
triphenylphosphine sulfide
Conditions | Yield |
---|---|
In chloroform-d1 for 1h; |
Conditions | Yield |
---|---|
In melt Mn2(CO)8Cl2 in ampoule cooled to -196 °C, (CH3)2AsI added, held at 60 °C 4 h, cooled to room temp.; sublimated in vac., elem. anal.; | 100% |
pentacarbonylchloromanganese(I)
dimethyliodoarsine
Mn(CO)4Cl(As(CH3)2I)
Conditions | Yield |
---|---|
In melt byproducts: CO; Mn(CO)5Cl in ampoule cooled to -196 °C, (CH3)2AsI added, held at 60 °C 4 h, cooled to room temp.; sublimated in vac., elem. anal.; | 100% |
iodo(pentacarbonyl)manganese(I)
dimethyliodoarsine
Mn(CO)4I(As(CH3)2I)
Conditions | Yield |
---|---|
In melt byproducts: CO; Mn(CO)5I in ampoule cooled to -196 °C, (CH3)2AsI added, held at 80 °C 4 h, cooled to room temp.; sublimated in vac., elem. anal.; | 100% |
bromopentacarbonylmanganese(I)
dimethyliodoarsine
Mn(CO)4Br(As(CH3)2I)
Conditions | Yield |
---|---|
In melt byproducts: CO; Mn(CO)5Br in ampoule cooled to -196 °C, (CH3)2AsI added, held at 70 °C 4 h, cooled to room temp.; sublimated in vac., elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Mn2(CO)8I2 in ampoule cooled to -196 °C, (CH3)2AsI added, held at80 °C 4 h, cooled to room temp.; sublimated in vac., elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Mn2(CO)8Br2 in ampoule cooled to -196 °C, (CH3)2AsI added, held at 70 °C 4 h, cooled to room temp.; sublimated in vac., elem. anal.; | 100% |
Conditions | Yield |
---|---|
With iodine monofluoride In trichlorofluoromethane 1.) -78 deg C, 15 min, 2.) RT, 30 min; | 95% |
dimethyliodoarsine
3,4,6-tri-O-benzoyl-2-deoxy-1-thio-β-D-arabino-hexopyranose
3,4,6-tri-O-benzoyl-2-deoxy-1-S-dimethylarsino-1-thio-β-D-arabino-hexopyranose
Conditions | Yield |
---|---|
With pyridine In dichloromethane Heating; | 90% |
dimethyliodoarsine
2,2'-bis(dimethylarsinomethyl)-1,1'-binaphthyl
Conditions | Yield |
---|---|
In tetrahydrofuran Ambient temperature; | 90% |
dimethyliodoarsine
Conditions | Yield |
---|---|
In dichloromethane (Ar); addn. of org. compd. to W-complex in CH2Cl2, stirring (-78°C); pptn. on addn. of ether/pentane, recryst. (CH2Cl2/ether/pentane), drying (high vac., room temp.); elem. anal.; | 86% |
dimethyliodoarsine
Carbonyl(η5-cyclopentadienyl)[(dimethylarsino)(4-methylphenyl)keten]iodo(trimethylphosphan)wolfram
Conditions | Yield |
---|---|
In dichloromethane under Ar, dropping of AsI(CH3)2 to the solution of η2-ketenyl complex in dichloromethane at room temp., stirred for 1 h; evapn. in vac., extn. with ether/pentane, recrystn. evapn. in vac., elem. anal.; | 85% |
dimethyliodoarsine
Carbonyl(η5-cyclopentadienyl)[(dimethylarsino)methylketen]iodo(trimethylphosphan)wolfram
Conditions | Yield |
---|---|
In dichloromethane under Ar, dropping of AsI(CH3)2 to the solution of η2-ketenyl complex in dichloromethane at room temp., stirred for 1 h; evapn. in vac., extn. with ether/pentane, recrystn. evapn. in vac., elem. anal.; | 82% |
(tris(2-diphenylphosphinoethyl)amin)Pd
dimethyliodoarsine
sodium tetraphenyl borate
{(N(CH2CH2P(C6H5)2)3)PdAs(CH3)2}(1+)*B(C6H5)4(1-)={(N(CH2CH2P(C6H5)2)3)PdAs(CH3)2}B(C6H5)4
Conditions | Yield |
---|---|
In ethanol; benzene byproducts: NaI; Room temp. reaction of (np3)Pd with equimolar quantities of Me2AsI in benzene-ethanol soln. under a nitrogen atmosphere.; | 80% |
(tris(2-diphenylphosphinoethyl)amin)Pt(PPh3)
dimethyliodoarsine
sodium tetraphenyl borate
{(N(CH2CH2P(C6H5)2)3)PtAs(CH3)2}(1+)*B(C6H5)4(1-)={(N(CH2CH2P(C6H5)2)3)PtAs(CH3)2}B(C6H5)4
Conditions | Yield |
---|---|
In ethanol; benzene byproducts: NaI; Room temp. reaction of (np3)Pt(PPh3) with equimolar quantities of Me2AsI in benzene-ethanol soln. under a nitrogen atmosphere.; | 80% |
(benzene)tricarbonylchromium
dimethyliodoarsine
(η6-phenyl)tricarbonylchromium dimethylarsine
Conditions | Yield |
---|---|
With n-C4H9Li In tetrahydrofuran (Ar); addn. of n-BuLi in hexane to cold soln. of Cr-complex in THF at .-78°C; stirred for 60 min; addn. of Me2AsI in THF; stirred for 60 min at -78°C; slowly warmed to room temp.;; filtration (through SiO2); solvent removed (reduced pressure); crystn. (hexane/CH2Cl2); elem. anal.; | 70% |
With BuLi In tetrahydrofuran; hexane Ar-atmosphere; addn. of 1 equiv. BuLi (in hexane) to Cr-complex (in THF)at -78°C, stirring (-78°C), addn. of arsine, stirring (-7 8°C, then room temp.); evapn., dissoln. in CH2Cl2, filtration, evapn.; elem. anal.; | 70% |
Conditions | Yield |
---|---|
Stage #1: N,N'-dimethylbenzylamine With n-butyllithium In diethyl ether; hexane for 24h; Stage #2: dimethyliodoarsine In diethyl ether for 5h; | 67% |
Stage #1: N,N'-dimethylbenzylamine With n-butyllithium Stage #2: dimethyliodoarsine |
dimethyliodoarsine
sodium
(+/-)-1-Chloro-2-(methylphenylphosphino)benzene
Conditions | Yield |
---|---|
In acetone byproducts: tetramethyldiarsane, methyldiphenylphosphine, methylphenylphosphine; Ar-atmosphere; addn. of Na-foil to Me2AsI (in THF), filtration, addn. to chlorophosphine (-78°C), stirring for 48 h (-20°C), evapn., treatment with CH2Cl2/H2O, evapn. of org. layer, fractional distn., treatment with Ni(ClO4)2 (pptn.); collection, washing (Et2O), drying (vac.); second crop on evapn. of filtrate, extn. into Et2O and addn. of Ni(ClO4)2 (in acetone soln.); elem. anal.; | 67% |
1-diphenylphosphinomethyl-1,2-dicarba-closo-dodecaborane
dimethyliodoarsine
1-dimethylarsino-2-diphenylphosphinomethyl-o-carborane
Conditions | Yield |
---|---|
With hydrogenchloride; n-butyllithium In benzene inert atmosphere; dropwise addn. of BuLi soln. to B-compd., mixt. stirring (1h), Me2AsCl addn., mixt. heating until reaction complete, cooling,treatment with dild. HCl; extn. (ether), extract drying (Na2SO4), evapn., residue chromy. (silicagel); elem. anal.; | 66% |
dimethyliodoarsine
bis-(2-chloroethyl)amine hydrochloride
bis<-2(dimethylarsinoethyl)>amine
Conditions | Yield |
---|---|
In tetrahydrofuran for 3h; | 65% |
dimethyliodoarsine
1,3,4-tri-O-acetyl-2-deoxy-6-thio-β-D-arabino-hexopyranose
1,3,4-tri-O-acetyl-2-deoxy-6-S-dimethylarsino-6-thio-β-D-arabino-hexopyranose
Conditions | Yield |
---|---|
With pyridine In toluene for 1h; Heating; | 65% |
dimethyliodoarsine
B
Fe3(CO)9(μ3-S-t-C4H9)(μ2-As(CH3)2)
Conditions | Yield |
---|---|
In diethyl ether; toluene byproducts: [H3N(t-C4H9)]I; under N2, Fe complex dissolved at 20°C in Et2O, treated with toluene, Me2AsI added, stirred for 1 h at room temp.; SiO2 added, dried in high vac., chromd. (SiO2, -20°C, n-pentane/toluene), evapd., recrystd. from toluene at -30°C; elem. anal.; | A n/a B 64% |
1-{(dimethylarsino)methyl}-o-carbaborane
dimethyliodoarsine
1-(dimethylarsino)-2-[(dimethylarsino)methyl]-o-carbaborane
Conditions | Yield |
---|---|
With hydrogenchloride; n-butyllithium In benzene inert atmosphere; dropwise addn. of BuLi soln. to B-compd., mixt. stirring (1h), Ph2PCl addn., mixt. heating until reaction complete, cooling, treatment with dild. HCl; extn. (ether), extract drying (Na2SO4), evapn., residue chromy. (silicagel); elem. anal.; | 62% |
dimethyliodoarsine
C8H20Li4N4P4
2,4,6,8-Tetrakis-dimethylarsanylmethyl-2,4,6,8-tetramethyl-2λ5,4λ5,6λ5,8λ5-[1,3,5,7,2,4,6,8]tetrazatetraphosphocine
Conditions | Yield |
---|---|
With potassium fluoride In diethyl ether at -78℃; for 0.166667h; | 55% |
Conditions | Yield |
---|---|
With sodium In tetrahydrofuran at 35℃; for 60h; | 51% |
dimethyliodoarsine
(R)-2,3-dibenzyloxypropyl 5-bromo-5-deoxy-2,3-O-isopropylidene-β-D-riboside
(R)-2,3-dibenzyloxypropyl 5-deoxy-5-dimethylarsino-2,3-O-isopropylidene-β-D-riboside
Conditions | Yield |
---|---|
Stage #1: dimethyliodoarsine With sodium In tetrahydrofuran at 20℃; for 1.5h; Stage #2: (R)-2,3-dibenzyloxypropyl 5-bromo-5-deoxy-2,3-O-isopropylidene-β-D-riboside In tetrahydrofuran for 1h; | 41% |
dimethyliodoarsine
(R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside
(R)-2,3-dibenzyloxypropyl 5-deoxy-5-dimethylarsino-2,3-O-isopropylidene-β-D-riboside
Conditions | Yield |
---|---|
Stage #1: dimethyliodoarsine With sodium In tetrahydrofuran at 20℃; for 1.5h; Stage #2: (R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside In tetrahydrofuran for 3h; | 41% |
(R)-N,N-dimethyl-1-ferrocenylethylamine
dimethyliodoarsine
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether the amine was stirred with n-BuLi in diethyl ether for 1.5 h, then the halide was added and stirred for 3 h; aq. slurry of NaHCO3 was added and stirred for 1 h before filtration. the ppt. was washed with ether, the filtrate and washings were washed with water, the organic layer was dried over K2CO3 and evapd., then chromd.; elem. anal.; | 40% |
Conditions | Yield |
---|---|
In diethyl ether reaction at 20°C, 2 hours;; | 35% |
In diethyl ether reaction at 20°C, 2 hours;; | 35% |
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