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Manganese(iii) Fluoride Application:Manganese(iii) Fluoride
Conditions | Yield |
---|---|
In neat (no solvent) passing F2 (dild. with N2 to 20 vol.-%) near 100 °C over MnO (5L/h);; |
Conditions | Yield |
---|---|
In neat (no solvent) react. with F2 below 100 °C;; |
Conditions | Yield |
---|---|
20-120°C, in liq. phase; |
Conditions | Yield |
---|---|
In hydrogen fluoride dissolving freshly pptd. MnO2 in aq. HF-soln.;; |
manganese(IV) oxide
fluorine
A
manganese(III) fluoride
B
oxygen
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; N2 carrier gas; 443 - 478 K, fluorine partial pressure 1.0 - 3.34 kPa; |
Conditions | Yield |
---|---|
In neat (no solvent) heating MnO2 (dried by slight warming in vac.) with F2-N2-gas-mixt. (vol.-ratio 20:80) to 150 °C;; | A <1 B n/a |
manganese(III) fluoride
tert-butylammonium hexafluorophosphate(V)
3,1-dimethyl-3,11,17,18-tetraazatricyclo[11.3.1.1(5,9)]octadeca-1(17),5(18),6,8,13,15-hexaene
[(N,N'-dimethyl-2,11-diaza[3,3][2,6]pyridinophane)Mn(III)F2(PF6)
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol to a soln. of MnF2 in methanol amine-compound in THF was added, stirred for 30 min at room temp., THF-satd. soln. of (C4H9)4NPF6 was added; the soln. was left whithout stirring, ppt. was filtered; elem. anal.; | 80% |
methanol
1,2,3-Benzotriazole
manganese(III) fluoride
triethylamine
Conditions | Yield |
---|---|
In methanol MnF3 and benzotriazole heated in methanol at 50°C under aerobic conditions for 10 min; soln. filtered and triethylamine added; crystals obtained upon evaporation in air after 24 h; elem. anal.; | 80% |
Conditions | Yield |
---|---|
In methanol MnF3 and dimethylbenzotriazole heated in methanol at 50°C under aerobic conditions for 10 min; soln. filtered and crystals obtained upon evaporation in air after 24 h;elem. anal.; | 80% |
Conditions | Yield |
---|---|
In methanol to stirred soln. of org. ligand in MeOH added MnF3; soln. stirred at room temp. for 2 h; soln. filtered; crystals were obtained by slow diffusion of Et2O in thissoln.; elem. anal.; | 76% |
manganese(III) fluoride
N-ethyl-N,N-bis(2-pyridylmethyl)amine
Conditions | Yield |
---|---|
In methanol to stirred soln. of org. ligand in MeOH added MnF3; soln. stirred at room temp. for 1 h; soln. filtered; evapd. to dryness; crystals were obtained by slow diffusion of Et2O in concd. soln. in MeCN; elem. anal.; | 36.4% |
Conditions | Yield |
---|---|
In methanol MnF3 and benzotriazole heated in methanol at 50°C under aerobic conditions for 10 min; soln. filtered and pyridine added dropwise; crystals obtained upon diffusion of diethyl ether after two weeks; elem.anal.; | 20% |
Conditions | Yield |
---|---|
In methanol MnF3 and benzotriazole heated in methanol at 50°C under aerobic conditions for 10 min; solid filtered and crystals obtained upon diffusion of diethyl ether after two weeks; elem. anal.; | 15% |
In neat (no solvent) MnF3 and benzotriazole ground together and heated in a Schlenk tube under inert atmosphere at 100°C for 30 min; melt dried in vacuo, and allowed to cool; solid dissolved in methanol at 50°C; crystals obtained upon diffusion of diethyl ether after two weeks; elem. anal.; | 10% |
Conditions | Yield |
---|---|
In methanol reaction of MnF3 with triazole under inert atmosphere at 100°C followed by extraction in hot CH3OH; elem. anal.; | 5% |
Conditions | Yield |
---|---|
at 160-190°C; | |
at 160-190°C; |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: InF3; solid state exchange react.; |
manganese(III) fluoride
cyanogen chloride
A
carbon tetrafluoride
B
chlorotrifluoromethane
C
pentafluoro chloro azomethane
Conditions | Yield |
---|---|
byproducts: Cl2; at 20-80°C; |
manganese(III) fluoride
cyanogen chloride
A
trifluoro-[1,3,5]triazine
B
carbon tetrafluoride
C
chlorotrifluoromethane
D
pentafluoro chloro azomethane
Conditions | Yield |
---|---|
byproducts: Cl2; at 160-190°C; |
Conditions | Yield |
---|---|
In neat (no solvent) heated to 500 K; |
Conditions | Yield |
---|---|
on heating;; | |
on heating;; |
manganese(III) fluoride
Conditions | Yield |
---|---|
In solid byproducts: F2; in sealed Ni capillary; capillary heated at constant rate of 1/30 °C/s from room temp. to 1370 K by using hot-air blower; sample analyzed in situ by means of Very-High Energy Synchrotron Radiation diffraction; | |
With sulfur byproducts: S-fluoride, SO2, SiF4; with boiling S; | |
In solid byproducts: F2; in open Ni capillary submitted to Ar flux; capillary heated at constant rate of 1/30 °C/s from room temp. to 1370 K by using hot-air blower; sample analyzed in situ by means of Very-High Energy Synchrotron Radiation diffraction; |
Conditions | Yield |
---|---|
In hydrogen fluoride aq. HF; equimolar amts. of satd. solns.; crystn. (24 h), washing (0.01 M HF, alcohol); |
Conditions | Yield |
---|---|
In hydrogen fluoride aq. HF; equimolar amts. of satd. solns.; crystn. (24 h), washing (0.01 M HF, alcohol); |
Conditions | Yield |
---|---|
In further solvent(s) condensing large excess of N2O5 on H2O-free MnF3 at -78 °C, mixing solid substances, heating to room temp., addn. of N2O4 (solvent), stirring for 3 d at 5 °C under exclusion of moisture, filtering off excess MnF3;; removing N2O4 in vac. at room temp. until no more NO(1+) and NO2(1+) can be detected by IR (22.5% Mn, 17,4 N);; |
manganese(III) fluoride
terbium tetrafluoride
A
manganese tetrafluoride
B
terbium(III) fluoride
Conditions | Yield |
---|---|
In neat (no solvent) react. MnF3 and TbF4 at 650-780 K; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; pelletized MnF2 (pretreated at 400°C), 450 - 700°C, partial pressure of fluorine 1.0 - 10.1 kPa, linear gas-flow rate 2 - 3 cm/s (mixt. F2 + N2); determined gravimetrically; elem. anal.; |
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