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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

Tetrabutylammonium hexafluorophosphate Manufacturer/High quality/Best price/In stock

Cas:3109-63-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Wuhan Fortuna Chemical Co.,Ltd

Factory supply Tetrabutylammonium hexafluorophosphate CAS 3109-63-5 with high purity 1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price;

Factory supply Tetrabutylammonium hexafluorophosphate CAS 3109-63-5 with high purity

Cas:3109-63-5

Min.Order:1 Kilogram

FOB Price: $56.0

Type:Trading Company

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Henan Allgreen Chemical Co.,Ltd

he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:Whit

TetrabutylaMMoniuM Hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Tetrabutylammonium Hexafluorophosphate

Cas:3109-63-5

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

discount Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 3109-63-5 with best quality

Cas:3109-63-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen

Tetrabutylammonium hexafluorophosphate Manufacturer/High quality/Best price/In stock CAS NO.3109-63-5

Cas:3109-63-5

Min.Order:20 Kilogram

FOB Price: $10.0 / 100.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Chemical Intermediate, Tetrabutylammonium hexafluorophosphate CAS:3109-63-5

Cas:3109-63-5

Min.Order:1 Gram

FOB Price: $59.0 / 64.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

Tetrabutylammonium hexafluorophosphate CAS:3109-63-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qua

Tetrabutylammonium hexafluorophosphate CAS:3109-63-5

Cas:3109-63-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:3109-63-5

Cas:3109-63-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Tetrabutyl-ammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:0 Metric Ton

FOB Price: $18.0 / 20.0

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

Tetrabutylammonium Hexafluorophosphate

Cas:3109-63-5

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Changzhou Anchor Biological Technology Co., Ltd.

Changzhou Anchor Biological Technology Co.,LTD. is engaged in customizing the benzene ring and pyridine derivative organic intermediates according to customers’ requirements. Meanwhile, under the premise of confidentiality of our customers, o

Tetrabutylammonium hexafluorophosphate Manufacturer/High quality/Best price/In stock CAS NO.3109-63-5

Cas:3109-63-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

Tetrabutyl-ammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:off-white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmac

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

High Purity Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

Tetrabutylammonium hexafluorophosphate Basic information Product Name: Tetrabutylammonium hexafluorophosphate Synonyms: 1-Butanaminium, N,N,N-tributyl-, hexafluorophosphate(1-);tetrabutylammonium-hexafluorphosophat;TETRABUTYLAMMONIUM HEXAFLUOROPHOSP

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Tetrabutyl-ammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Tetrabutyl-ammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Wuhu Nuowei Chemistry Technologies Co., Ltd.

Wuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma

Tetrabutyl ammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:100 Gram

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

Tetrabutylammonium hexafluorophosphate

Cas:3109-63-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

tetrabutylammomium bromide
1643-19-2

tetrabutylammomium bromide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
With trimethyl phosphite; hexafluorophosphoric acid at 0 - 60℃; for 15h; Inert atmosphere; neat (no solvent);96%
With potassium hexafluorophosphate In dichloromethane; water at 20℃; for 24h;88%
With potassium hexafluorophosphate In dichloromethane; water at 20℃; for 24h;88%
[N(nBu)4]X; X = halide

[N(nBu)4]X; X = halide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
With silver(I) hexafluorophosphate In dichloromethane; acetonitrile at 20℃; for 10h; Darkness;92%
tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

phosphonic acid diethyl ester
762-04-9

phosphonic acid diethyl ester

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
Stage #1: phosphonic acid diethyl ester With potassium fluoride; oxalyl dichloride In acetonitrile at 20℃; Glovebox; Sealed tube; Inert atmosphere;
Stage #2: tetrabutyl-ammonium chloride In water at 20℃; for 0.166667h; Glovebox; Sealed tube; Inert atmosphere;
59%
methanol
67-56-1

methanol

C16H36N(1+)*CH4O*F6P(1-)

C16H36N(1+)*CH4O*F6P(1-)

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In dichloromethane at 26℃; Equilibrium constant; 1.3 - 1.5 M-1;
ammonium hexafluorophosphate

ammonium hexafluorophosphate

tetrabutylammomium bromide
1643-19-2

tetrabutylammomium bromide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In not given recrystn.(ethanol/water), drying (vacuo, 24 h, 80°C);
((η3-methallyl)Ni(cod))PF6

((η3-methallyl)Ni(cod))PF6

tri(3-sulfonatophenyl)phosphine tri(tetrabutylammonium)

tri(3-sulfonatophenyl)phosphine tri(tetrabutylammonium)

A

(CH2C(CH3)CH2)Ni(C8H12)P(C6H4SO3Ni(CH2C(CH3)CH2))2(C6H4SO3)(1-)

(CH2C(CH3)CH2)Ni(C8H12)P(C6H4SO3Ni(CH2C(CH3)CH2))2(C6H4SO3)(1-)

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

C

1,5-dicyclooctadiene
5259-72-3, 10060-40-9, 111-78-4

1,5-dicyclooctadiene

Conditions
ConditionsYield
In dichloromethane addn. of TPPTSNBu4 to Ni-compd. (high 2/1 ratio) in CH2Cl2, room temp.; detd. spectr.; sepn. of cod by evapn.; pptn. of NBu4PF6;
((η3-methallyl)Ni(cod))PF6

((η3-methallyl)Ni(cod))PF6

tri(3-sulfonatophenyl)phosphine tri(tetrabutylammonium)

tri(3-sulfonatophenyl)phosphine tri(tetrabutylammonium)

A

(CH2C(CH3)CH2)Ni(C8H12)P(C6H4SO3)3(3-)*2N(C4H9)4(1+)

(CH2C(CH3)CH2)Ni(C8H12)P(C6H4SO3)3(3-)*2N(C4H9)4(1+)

B

(CH2C(CH3)CH2)Ni(C8H12)P(C6H4SO3)2(C6H4SO3Ni(CH2C(CH3)CH2))(2-)*N((CH2)3CH3)4(1+)

(CH2C(CH3)CH2)Ni(C8H12)P(C6H4SO3)2(C6H4SO3Ni(CH2C(CH3)CH2))(2-)*N((CH2)3CH3)4(1+)

C

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

D

1,5-dicyclooctadiene
5259-72-3, 10060-40-9, 111-78-4

1,5-dicyclooctadiene

Conditions
ConditionsYield
In dichloromethane addn. of TPPTSNBu4 to Ni-compd. (low 2/1 ratio) in CH2Cl2, room temp.; detd. spectr.; sepn. of cod by evapn.; pptn. of NBu4PF6;
tetra(n-butyl)ammonium hydroxide
2052-49-5

tetra(n-butyl)ammonium hydroxide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
With hexafluorophosphate In water
With hexafluorophosphoric acid In water
With hexafluorophosphoric acid In water Inert atmosphere; Schlenk technique;
potassium hexafluorophosphate
17084-13-8

potassium hexafluorophosphate

tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In water for 24h;
ammonium hexafluorophosphate

ammonium hexafluorophosphate

tetrabutylammomium bromide
1643-19-2

tetrabutylammomium bromide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In water
hexafluorophosphoric acid

hexafluorophosphoric acid

tetra(n-butyl)ammonium hydroxide
2052-49-5

tetra(n-butyl)ammonium hydroxide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In water
tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
With hexafluorophosphoric acid; sodium hydroxide
C15H16IO3(1+)*F6P(1-)

C15H16IO3(1+)*F6P(1-)

tetrabutylammonium benzoate
18819-89-1

tetrabutylammonium benzoate

A

C25H27IO8

C25H27IO8

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
C15H16IO3(1+)*F6P(1-)

C15H16IO3(1+)*F6P(1-)

tetra-n-butylammonium p-nitrophenoxide
3002-48-0

tetra-n-butylammonium p-nitrophenoxide

A

C24H26INO9

C24H26INO9

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

C15H16IO3(1+)*F6P(1-)

C15H16IO3(1+)*F6P(1-)

A

C18H22ClIO6

C18H22ClIO6

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Thermodynamic data; Inert atmosphere;
(3,5-bis(trifluoromethyl)phenyl)(phenyl)iodonium hexafluorophosphate

(3,5-bis(trifluoromethyl)phenyl)(phenyl)iodonium hexafluorophosphate

tetrabutylammonium benzoate
18819-89-1

tetrabutylammonium benzoate

A

C21H13F6IO2

C21H13F6IO2

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
(perfluorophenyl)(phenyl)iodonium hexafluorophosphate
951037-67-5

(perfluorophenyl)(phenyl)iodonium hexafluorophosphate

tetrabutylammonium benzoate
18819-89-1

tetrabutylammonium benzoate

A

C19H10F5IO2

C19H10F5IO2

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
(3,5-bis(trifluoromethyl)phenyl)(phenyl)iodonium hexafluorophosphate

(3,5-bis(trifluoromethyl)phenyl)(phenyl)iodonium hexafluorophosphate

tetra-n-butylammonium p-nitrophenoxide
3002-48-0

tetra-n-butylammonium p-nitrophenoxide

A

C20H12F6INO3

C20H12F6INO3

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
(perfluorophenyl)(phenyl)iodonium hexafluorophosphate
951037-67-5

(perfluorophenyl)(phenyl)iodonium hexafluorophosphate

tetra-n-butylammonium p-nitrophenoxide
3002-48-0

tetra-n-butylammonium p-nitrophenoxide

A

C18H9F5INO3

C18H9F5INO3

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
(3,5-bis(trifluoromethyl)phenyl)(phenyl)iodonium hexafluorophosphate

(3,5-bis(trifluoromethyl)phenyl)(phenyl)iodonium hexafluorophosphate

tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

A

C14H8ClF6I

C14H8ClF6I

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Thermodynamic data; Inert atmosphere;
tetra-n-butylammonium p-nitrophenoxide
3002-48-0

tetra-n-butylammonium p-nitrophenoxide

diphenyliodonium hexafluorophosphate
58109-40-3

diphenyliodonium hexafluorophosphate

A

diphenyliodonium 4-nitrophenolate

diphenyliodonium 4-nitrophenolate

B

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Conditions
ConditionsYield
In acetonitrile at 20℃; Equilibrium constant; Inert atmosphere;
trans-rhenium(V)-oxo-(Cl)(N,N'-propylenebis(acetylacetone)diimine)

trans-rhenium(V)-oxo-(Cl)(N,N'-propylenebis(acetylacetone)diimine)

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

triethylphosphine
554-70-1

triethylphosphine

cis-[Re(V)O(triethylphosphine)(N,N'-propylenebis(acetylacetonate) diimine)][PF6]

cis-[Re(V)O(triethylphosphine)(N,N'-propylenebis(acetylacetonate) diimine)][PF6]

Conditions
ConditionsYield
In ethanol; dichloromethane Re complex dissolved in ethanol, soln. of triethylphosphine in CH2Cl2 added, reflued for 1 h under N2, tetrabutylammonium hexafluorophosphate added; concd., frozen overnight, crystal collected, washed with toluene, ether;elem. anal.;99%
trans-rhenium(V)-oxo-(Cl)(N,N'-propylenebis(acetylacetone)diimine)

trans-rhenium(V)-oxo-(Cl)(N,N'-propylenebis(acetylacetone)diimine)

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

diethyl-phenyl-phosphine
1605-53-4

diethyl-phenyl-phosphine

cis-[Re(V)O(diethylphenylphosphine)(N,N'-propylenebis(acetylacetonate) diimine)][PF6]

cis-[Re(V)O(diethylphenylphosphine)(N,N'-propylenebis(acetylacetonate) diimine)][PF6]

Conditions
ConditionsYield
In ethanol; dichloromethane Re complex dissolved in ethanol, soln. of diethylphenylphosphine in CH2Cl2 added, heated for 1 h under N2, tetrabutylammonium hexafluorophosphate added to warm soln.; cooled to room temp., ppt. filtered, washed with toluene, cold ethanol, ether; elem. anal.;99%
trans-rhenium(V)-oxo-(Cl)(N,N'-propylenebis(acetylacetone)diimine)

trans-rhenium(V)-oxo-(Cl)(N,N'-propylenebis(acetylacetone)diimine)

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

triphenylphosphine
603-35-0

triphenylphosphine

cis-[Re(V)O(triphenylphosphine)(N,N'-propylenebis(acetylacetonate) diimine)][PF6]

cis-[Re(V)O(triphenylphosphine)(N,N'-propylenebis(acetylacetonate) diimine)][PF6]

Conditions
ConditionsYield
In ethanol; dichloromethane Re complex dissolved in ethanol, soln. of triphenylphosphine in CH2Cl2 added, heated for 1 h under N2, tetrabutylammonium hexafluorophosphate added to warm soln.; cooled to room temp., ppt. filtered, washed with toluene, cold ethanol, ether; elem. anal.;99%
aqua[N,N'-ethylenebis(acetylacetone iminato)]oxotechnetium(V) bromide
87761-77-1

aqua[N,N'-ethylenebis(acetylacetone iminato)]oxotechnetium(V) bromide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

ethyl-diphenyl-phosphane
607-01-2

ethyl-diphenyl-phosphane

trans-bis(diphenylethylphosphine)(N,N'-ethylenebis(acetylacetone iminato))technetium(III) hexafluorophosphate
93427-02-2

trans-bis(diphenylethylphosphine)(N,N'-ethylenebis(acetylacetone iminato))technetium(III) hexafluorophosphate

Conditions
ConditionsYield
In methanol adding of PEtPh2 to MeOH soln. of Tc(V) complex, stirring for 15 min atroom temp., adding of Bu4NPF6; filtration, concn., cooling overnight, filtration, washing with H2O, drying in vac. over P2O5;98%
2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methyl-6-(methylthio)phenol
1186470-04-1

2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methyl-6-(methylthio)phenol

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

copper dichloride

copper dichloride

[Cu3Cl2(2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methyl-6(methylthio)phenolate)2](hexafluorphosphate)2

[Cu3Cl2(2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methyl-6(methylthio)phenolate)2](hexafluorphosphate)2

Conditions
ConditionsYield
With N(CH2CH3)3 In methanol refluxing mixt. of 2 equiv. of copper compd., 3 equiv. of phenol. deriv.and amine deriv. in methanol for 1 h, addn. of hexafluorophosphate salt; filtration, washing with cold methanol, drying in vac., elem. anal.;97%
2Os(3+)*4CH3CO2(1-)*2Cl(1-)=Os2(O2CCH3)4Cl2

2Os(3+)*4CH3CO2(1-)*2Cl(1-)=Os2(O2CCH3)4Cl2

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

(n-Bu4N)2{Os2Cl8}

(n-Bu4N)2{Os2Cl8}

Conditions
ConditionsYield
With HCl In ethanol (under N2), a sample of the Os-compound was suspended in EtOH, which had been chilled in an ice bath and saturated with gaseous HCl, mixture was refluxed for 1.5 h, treated with an EtOH soln. containing an excess of n-Bu4NPF6; removal of the solvent, resulting green oil was dissolved in CH2Cl2, addn. of ethanol, diethyl ether was carefully layered over the soln., pptn., filtn., product was washed (ethanol, diethyl ether), drying under vacuum;96%
{(triphos)Rh(μ-C2S4)Rh(triphos)}Cl2

{(triphos)Rh(μ-C2S4)Rh(triphos)}Cl2

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

{(triphos)Rh(μ-C2Se4)Rh(triphos)}(PF6)2

{(triphos)Rh(μ-C2Se4)Rh(triphos)}(PF6)2

Conditions
ConditionsYield
In dichloromethane under N2; solid (NBu4)(PF6) added to the Rh-complex in CH2Cl2; crystn. on addn. of ethanol, elem. anal.;95%
[(C41H39P3)Rh(C2S4)Rh(C41H39P3)](2+)*2Cl(1-) = [(C41H39P3)Rh(C2S4)Rh(C41H39P3)]Cl2

[(C41H39P3)Rh(C2S4)Rh(C41H39P3)](2+)*2Cl(1-) = [(C41H39P3)Rh(C2S4)Rh(C41H39P3)]Cl2

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

[(C41H39P3)Rh(C2S4)Rh(C41H39P3)](2+)*2PF6(1-)=[(C41H39P3)Rh(C2S4)Rh(C41H39P3)](PF6)2

[(C41H39P3)Rh(C2S4)Rh(C41H39P3)](2+)*2PF6(1-)=[(C41H39P3)Rh(C2S4)Rh(C41H39P3)](PF6)2

Conditions
ConditionsYield
In dichloromethane under N2; solid (NBu4)(PF6) added to the Rh-complex in CH2Cl2; crystn. on addn. of ethanol, elem. anal.;95%
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]
12354-84-6, 12354-85-7

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

2,2'-azopyridine
2633-03-6

2,2'-azopyridine

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

[(η5-C5Me5)Ir(2,2'-azobis(pyridine))Cl]PF6
545436-48-4

[(η5-C5Me5)Ir(2,2'-azobis(pyridine))Cl]PF6

Conditions
ConditionsYield
In methanol suspn. of complex and azo compound in CH3OH stirred for 3 h, concd., treated with 3 equiv of Bu4NPF6 in methanol; ppt. filtered off, washed with methanol and diethyl ether, dried under vac.; elem. anal.;95%
di[1,4-bis(dimethylamino)-η6-benzene]chromium
639518-84-6

di[1,4-bis(dimethylamino)-η6-benzene]chromium

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

di[1,4-bis(dimethylamino)-η6-benzene]chromium hexafluorophosphate
639518-86-8

di[1,4-bis(dimethylamino)-η6-benzene]chromium hexafluorophosphate

Conditions
ConditionsYield
With 4-pyridine carbaldehyde In tetrahydrofuran a soln. of n-Bu4NPF6 added to a soln. of Cr complex, stirred for 10 min at ambient temp., 4-pyridine carbaldehyde added dropwise, stirred for 30min; pptd. (Et2O), collected, washed (Et2O, H2O), dissolved in acetone, layered with Et2O; elem. anal.;95%
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]
12354-84-6, 12354-85-7

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

glyoxalbis(2,6-dimethylphenylimine)

glyoxalbis(2,6-dimethylphenylimine)

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

[(C5Me5)Ir(1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)]PF6

[(C5Me5)Ir(1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)]PF6

Conditions
ConditionsYield
In methanol stirring Ir-complex with 2.5 equiv. of diene for 4 h, pptn. on addn. of excess Bu4NCl; elem. anal.;95%
2-[(bis(2-pyridylmethyl)amino)methyl]-4-methyl-6-(methylthio)phenol
949566-81-8

2-[(bis(2-pyridylmethyl)amino)methyl]-4-methyl-6-(methylthio)phenol

water
7732-18-5

water

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

copper dichloride

copper dichloride

[CuCl(2-[(bis(2-pyridylmethyl)amino)methyl]-4-methyl-6-(methylthio)phenol)](hexafluorphosphate)*0.75water

[CuCl(2-[(bis(2-pyridylmethyl)amino)methyl]-4-methyl-6-(methylthio)phenol)](hexafluorphosphate)*0.75water

Conditions
ConditionsYield
In methanol refluxing 1:1 mixt. of copper compd. and phenol. deriv. in methanol for 1 h, addn. of hexafluorophosphate salt; filtration, washing with cold methanol, drying in vac., elem. anal.;93%
trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

tetra-n-butylammonium mer-tricyanido(trifluorido)phosphate

tetra-n-butylammonium mer-tricyanido(trifluorido)phosphate

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate at 25℃; for 80h; Inert atmosphere; Schlenk technique;93%
methanol
67-56-1

methanol

[Rh2(μ-OOCCH3)2(CH3CN)6](BF4)2

[Rh2(μ-OOCCH3)2(CH3CN)6](BF4)2

2,3,5,6-tetrakis(2-pyridyl)pyrazine
25005-97-4

2,3,5,6-tetrakis(2-pyridyl)pyrazine

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Rh4(μ-OOCCH3)2(2,3,5,6-tetra-2-pyridylpirazine)2(CH3OH)4(PF6)4*2CH3OH

Rh4(μ-OOCCH3)2(2,3,5,6-tetra-2-pyridylpirazine)2(CH3OH)4(PF6)4*2CH3OH

Conditions
ConditionsYield
In methanol; dichloromethane (Rh2(OOCCH3)2(CH3CN)6)(BF4)2 dissolved in CH3OH and added to CH2Cl2 soln. of 2,3,5,6-tetra-2-pyridylpyrazine under N2 and heated for 1 h; treated with excess of (C4H9)4NPF6; soln. concd., treated with diethyl ether, solid collected by filtrn., recrystd. from a CH3OH/benzene soln.;92%
methanol
67-56-1

methanol

2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methylphenol
1186470-02-9

2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methylphenol

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

copper dichloride

copper dichloride

[CuCl(2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methylphenol)](hexafluorphosphate)*methanol

[CuCl(2-[(2-pyridylmethyl)(2'-pyridylethyl)amino-methyl]-4-methylphenol)](hexafluorphosphate)*methanol

Conditions
ConditionsYield
In methanol refluxing 1:1 mixt. of copper compd. and phenol. deriv. in methanol for 1 h, addn. of hexafluorophosphate salt; filtration, washing with cold methanol, drying in vac., elem. anal.;92%
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]
12354-84-6, 12354-85-7

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

2-acetylpyridine hydrazone
59742-91-5

2-acetylpyridine hydrazone

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

(η5-pentamethylcyclopentadienylato)IrCl(2-(1-hydrazonoethyl)pyridine)(PF6)
1370365-92-6

(η5-pentamethylcyclopentadienylato)IrCl(2-(1-hydrazonoethyl)pyridine)(PF6)

Conditions
ConditionsYield
In ethanol Ar, Schlenk technique; mixt. of Ir-complex and pyridine-imine stirred atroom temp. for 5 min, Bu4NPF6 added; filtered, residue washed (THF, ether), dried (vac.); elem. anal.;92%
cobalt(II) chloride hexahydrate

cobalt(II) chloride hexahydrate

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

C20H28CoN6(2+)*2F6P(1-)

C20H28CoN6(2+)*2F6P(1-)

Conditions
ConditionsYield
Stage #1: cobalt(II) chloride hexahydrate; 2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride With sodium hydroxide In water for 2h; pH=7;
Stage #2: tert-butylammonium hexafluorophosphate(V) In water
92%
tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

zinc(II) chloride
7646-85-7

zinc(II) chloride

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

(2,9-bis(2',5'-diazahexanyl)-1,10-phenanthroline)zinc(II) bis(hexafluorophosphate)

(2,9-bis(2',5'-diazahexanyl)-1,10-phenanthroline)zinc(II) bis(hexafluorophosphate)

Conditions
ConditionsYield
Stage #1: zinc(II) chloride; 2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride With sodium hydroxide In water for 2h; pH=7;
Stage #2: tert-butylammonium hexafluorophosphate(V) In water
92%
trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

tetra-n-butylammonium monocyanido(pentafluorido)phosphate

tetra-n-butylammonium monocyanido(pentafluorido)phosphate

Conditions
ConditionsYield
at 25℃; for 20h; Time; Inert atmosphere;92%
trimethylaluminium dimer

trimethylaluminium dimer

(Cl2BC5H4)Co(C5H4BCl3)
214750-04-6

(Cl2BC5H4)Co(C5H4BCl3)

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

Co(C5H4B(CH3)2)2(1+)*PF6(1-)=[Co(C5H4B(CH3)2)2]PF6
848891-30-5

Co(C5H4B(CH3)2)2(1+)*PF6(1-)=[Co(C5H4B(CH3)2)2]PF6

Conditions
ConditionsYield
In dichloromethane; toluene N2-atmosphere; stirring (room temp., 2 h), evapn. (vac.), CH2Cl2 addn., pptn. on hexane addn., filtering, washing (hexane), Bu4NPF6 addn.; crystn. (CH2Cl2, -30°C); elem. anal.;91%
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]
12354-84-6, 12354-85-7

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

N1,N2-bis(o-tolyl)ethane-1,2-diimine
51479-97-1

N1,N2-bis(o-tolyl)ethane-1,2-diimine

[(CH3C6H4NCHCHNC6H4CH3)C5(CH3)5ClIr](1+)*PF6(1-)=[(CH3C6H4NCHCHNC6H4CH3)C5(CH3)5ClIr]PF6
405316-13-4

[(CH3C6H4NCHCHNC6H4CH3)C5(CH3)5ClIr](1+)*PF6(1-)=[(CH3C6H4NCHCHNC6H4CH3)C5(CH3)5ClIr]PF6

Conditions
ConditionsYield
In methanol addn. of diene deriv. to a suspn. of Ir complex in MeOH (in ultrasonic bath), stirred for 3 h at room temp.; concd. of soln., addn. of (C4H9)4NPF6 soln. in MeOH; ppt. collected, washed with MeOH and Et2O, dried under vac.; elem. anal.;90%
nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

(2,9-bis(2',5'-diazahexanyl)-1,10-phenanthroline)nickel(II) bis(hexafluorophosphate)

(2,9-bis(2',5'-diazahexanyl)-1,10-phenanthroline)nickel(II) bis(hexafluorophosphate)

Conditions
ConditionsYield
Stage #1: nickel(II) chloride hexahydrate; 2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride With sodium hydroxide In water for 2h; pH=7;
Stage #2: tert-butylammonium hexafluorophosphate(V) In water
90%
copper(II) nitrate pentahydrate

copper(II) nitrate pentahydrate

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride

C20H28CuN6(2+)*2F6P(1-)

C20H28CuN6(2+)*2F6P(1-)

Conditions
ConditionsYield
Stage #1: copper(II) nitrate pentahydrate; 2,9-di(((2'-methylamino)ethyleneamino)methyl)-1,10-phenanthroline tetrahydrochloride With sodium hydroxide In water for 2h; pH=7;
Stage #2: tert-butylammonium hexafluorophosphate(V) In water
90%
tetraacetatodiruthenium chloride

tetraacetatodiruthenium chloride

2-(pyrazin-2-yl)-1,8-naphthyridine
1338090-17-7

2-(pyrazin-2-yl)-1,8-naphthyridine

water
7732-18-5

water

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

acetonitrile
75-05-8

acetonitrile

cis-[Ru2(2-(2-pyrazinyl)-1,8-naphthyridine)2(OAc)2][PF6]2(CH3CN)(H2O)

cis-[Ru2(2-(2-pyrazinyl)-1,8-naphthyridine)2(OAc)2][PF6]2(CH3CN)(H2O)

Conditions
ConditionsYield
Stage #1: tetraacetatodiruthenium chloride; 2-(pyrazin-2-yl)-1,8-naphthyridine; tert-butylammonium hexafluorophosphate(V) In methanol Inert atmosphere; Schlenk technique; Reflux;
Stage #2: water; acetonitrile Inert atmosphere; Schlenk technique;
90%
N2,N6-bis(diethylcarbamothioyl)pyridine-2,6-dicarboxamide

N2,N6-bis(diethylcarbamothioyl)pyridine-2,6-dicarboxamide

iron(III) chloride hexahydrate

iron(III) chloride hexahydrate

tert-butylammonium hexafluorophosphate(V)
3109-63-5

tert-butylammonium hexafluorophosphate(V)

sodium chloride
7647-14-5

sodium chloride

C51H69Fe2N15NaO6S6(1+)*F6P(1-)

C51H69Fe2N15NaO6S6(1+)*F6P(1-)

Conditions
ConditionsYield
Stage #1: N2,N6-bis(diethylcarbamothioyl)pyridine-2,6-dicarboxamide; iron(III) chloride hexahydrate; sodium chloride In methanol; water at 20℃; for 0.5h;
Stage #2: With triethylamine In methanol; water at 20℃; for 0.5h;
Stage #3: tert-butylammonium hexafluorophosphate(V) In methanol; water at 20 - 50℃; for 2h;
90%

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