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Cas:89-84-9
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 2'.4'-Dihydroxyacetophenone CAS No.
Cas:89-84-9
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:89-84-9
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
About Product Details 2,4-Dihydroxyacetophenone Chemical Properties
Cas:89-84-9
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:89-84-9
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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Cas:89-84-9
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
Cas:89-84-9
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inquiry2,4-Dihydroxyacetophenone CAS:89-84-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:89-84-9
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:89-84-9
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inquiry1.High Quality: Quality is life. Quality is the most important element for all goods. We have a lab doing research in Wuhan China and produce sarms in bulk quantity. We have 8 years experience making all kinds of sarms. And all our old customers
Cas:89-84-9
Min.Order:10 Gram
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inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional in lead acetate, diphenyl ethylamine and other chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countrie
Cas:89-84-9
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Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
Cas:89-84-9
Min.Order:500 Gram
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Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:89-84-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
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Cas:89-84-9
Min.Order:100 Gram
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Type:Other
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:89-84-9
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryProduct Description Advantage: High quality and competitive price. 1. We can provide samples for testing. 2. All purity >99%. As a manufacturer, we can supply high quality products at ex-factory prices. Fast and safe delivery. 1. The package c
Cas:89-84-9
Min.Order:10 Gram
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inquiryFactory 2,4-Dihydroxyacetophenone in stock CAS No.89-84-9Appearance:powder Storage:dry and cool place Package:according to customers' requirements Application:API ,Used as pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT
Cas:89-84-9
Min.Order:1 Gram
Negotiable
Type:Other
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:89-84-9
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry2-hydroxy-4-(methoxymethoxy)acetophenone
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
H6P2W18O62; silica gel In tetrahydrofuran; methanol at 70℃; for 0.75h; Product distribution; Further Variations:; Catalysts; Solvents; Temperatures; | 100% |
With toluene-4-sulfonic acid In neat (no solvent, solid phase) at 20℃; for 0.583333h; Green chemistry; | 90% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate for 0.0333333h; microwave irradiation; | 98% |
With iron(III) chloride for 0.0221667h; Friedel Crafts acylation; Microwave irradiation; regioselective reaction; | 98% |
With zinc(II) chloride Reflux; | 98% |
2,4-diacetoxy acetophenone
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
With water; sodium acetate In ethanol for 5h; Reflux; | 98% |
Conditions | Yield |
---|---|
With acyltransferase from bacterium Pseudomonas sp.YGJ3 In aq. phosphate buffer; dimethyl sulfoxide at 35℃; for 18h; pH=7.5; Friedel-Crafts Acylation; Enzymatic reaction; regioselective reaction; | 97% |
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In neat (no solvent, solid phase) at 20℃; for 0.583333h; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With periodic acid at 20℃; for 0.0833333h; | 92% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; acetic acid Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With acetic acid; zinc(II) chloride at 60℃; for 4h; Temperature; Large scale; | 90.6% |
With PPA Reflux; | 68% |
With phosphorus pentoxide; silica gel at 100℃; for 24h; | 65% |
1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
With formic acid; sodium formate; palladium on activated charcoal In methanol for 1h; Product distribution; Heating; other aryl benzyl ethers; | 90% |
With formic acid; sodium formate; palladium on activated charcoal In methanol for 1h; Heating; | 90% |
acetic anhydride
recorcinol
A
2',4'-dihydroxy-4-acetophenone
B
2,4-diacetylresorcinol
C
1-(5-acetyl-2,4-dihydroxyphenyl)-1-ethanone
Conditions | Yield |
---|---|
With zinc(II) chloride at 145 - 150℃; for 0.25h; | A 2% B 7% C 90% |
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate for 0.0333333h; microwave irradiation; | 80% |
4-allyloxy-2-hydroxyacetophenone
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
With iodine In dimethyl sulfoxide at 130℃; for 0.5h; | 79% |
Conditions | Yield |
---|---|
With zinc at 64 - 66℃; for 0.0208333h; Friedel-Crafts acylation; microwave irradiation; | 77% |
Conditions | Yield |
---|---|
With acetic acid; zinc(II) chloride at 20℃; for 12h; | 73% |
With sulfuric acid; acetic acid In di-isopropyl ether; water | 72% |
With sulfuric acid; acetic anhydride; acetic acid In water | 68% |
Conditions | Yield |
---|---|
With 1H-imidazole; acyltransferase from bacterium Pseudomonas sp.YGJ3 In aq. phosphate buffer at 35℃; for 24h; pH=8.3; Friedel-Crafts Acylation; Enzymatic reaction; regioselective reaction; | 68% |
With 1H-imidazole; acyltransferase from pseudomonas protegens In aq. buffer at 35℃; for 18h; pH=8.3; Catalytic behavior; Reagent/catalyst; Concentration; pH-value; Friedel-Crafts Acylation; | 98 %Chromat. |
With 1H-imidazole; acyltransferase from Pseudomonas protegens W211A mutant In aq. phosphate buffer; acetonitrile at 35℃; for 1.5h; pH=7.5; Catalytic behavior; Reagent/catalyst; Friedel-Crafts Acylation; Enzymatic reaction; | 66 %Chromat. |
2,4-diacetylphloroglucinol
recorcinol
A
2',4'-dihydroxy-4-acetophenone
B
3,5-dihydroxyphenol
Conditions | Yield |
---|---|
With cell-free E. coli extract containing the recombinant acyltransferase from Pseudomonas protegens In aq. phosphate buffer; dimethyl sulfoxide at 35℃; for 0.5h; pH=7.5; Catalytic behavior; Solvent; pH-value; Temperature; Enzymatic reaction; | A 65% B n/a |
N-acetyl-(4-methylbenzene)sulfonamide
recorcinol
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
With zinc(II) chloride at 110 - 120℃; | 60% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In benzene for 3h; crossover Friess rearrangement; Heating; | 60% |
With 1H-imidazole; acyltransferase from pseudomonas protegens In aq. buffer at 35℃; for 18h; pH=8.3; Friedel-Crafts Acylation; | > 99 %Chromat. |
2,4-diacetoxy acetophenone
A
2',4'-dihydroxy-4-acetophenone
B
2'-acetoxy-4'-hydroxyacetophenone
Conditions | Yield |
---|---|
With Candida cylindracea lipase In di-isopropyl ether; butan-1-ol at 28 - 30℃; for 11h; | A 40% B 50% |
Conditions | Yield |
---|---|
With acyltransferase from bacterium Pseudomonas sp.YGJ3 In aq. phosphate buffer at 35℃; for 18h; pH=7.5; Friedel-Crafts Acylation; Enzymatic reaction; regioselective reaction; | 41% |
2',4'-dimethoxyacetophenone
A
2',4'-dihydroxy-4-acetophenone
B
1-(2-hydroxy-4-methoxyphenyl)ethanone
C
1-(4-hydroxy-2-methoxy-phenyl)ethanone
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; potassium carbonate; thiophenol for 0.5h; Heating; | A 22% B 16.3% C 38% |
isoliquirtigenin
A
2',4'-dihydroxy-4-acetophenone
B
5-hydroxy-2-(4-hydroxphenyl)chroman-4-one
C
4-hydroxy-benzaldehyde
D
chalaurenol
Conditions | Yield |
---|---|
With Tris-HCl buffer; peroxidase from Amorpha fruticosa In 2-methoxy-ethanol at 30℃; for 3h; | A n/a B n/a C n/a D 25% |
With Tris-HCl buffer; peroxidase from Amorpha fruticosa In 2-methoxy-ethanol at 30℃; for 3h; Mechanism; | A n/a B n/a C n/a D 25% |
2,4,6-trihydroxyacetophenone
recorcinol
A
2',4'-dihydroxy-4-acetophenone
B
3,5-dihydroxyphenol
Conditions | Yield |
---|---|
With cell-free E. coli extract containing the recombinant acyltransferase from Pseudomonas protegens In aq. phosphate buffer; dimethyl sulfoxide at 35℃; for 0.5h; pH=7.5; Enzymatic reaction; | A 13% B n/a |
7-hydroxy-4-methyl-chromen-2-one
2',4'-dihydroxy-4-acetophenone
Conditions | Yield |
---|---|
With potassium carbonate |
Conditions | Yield |
---|---|
With aluminium trichloride at 185℃; | |
With zinc(II) chloride |
Conditions | Yield |
---|---|
With aluminium trichloride at 185℃; |
A
2',4'-dihydroxy-4-acetophenone
B
acetic acid
C
2',4'-dimethoxyacetophenone
D
recorcinol
4,7-dihydroxy-3-[3,7,11-trimethyl-2(E),6(E),10-dodecatrienyl]coumarin
A
2',4'-dihydroxy-4-acetophenone
B
4,7-dihydroxy-3-methyl-2H-chromen-2-one
Conditions | Yield |
---|---|
at 230℃; under 0.3 Torr; |
3,4-dihydro-2H-pyran
2',4'-dihydroxy-4-acetophenone
2-hydroxy-4-(tetrahydropyran-2-yloxy)acetophenone
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In dichloromethane for 1.5h; Ambient temperature; | 100% |
With pyridinium p-toluenesulfonate In dichloromethane at 20℃; for 4h; | 98.3% |
With pyridinium p-toluenesulfonate In dichloromethane for 12h; Ambient temperature; | 90% |
2',4'-dihydroxy-4-acetophenone
benzyl bromide
2,4-bis(benzyloxy)acetophenone
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 48h; Heating / reflux; | 100% |
Stage #1: 2',4'-dihydroxy-4-acetophenone With potassium carbonate In acetonitrile at 85℃; for 0.0833333h; Inert atmosphere; Stage #2: benzyl bromide at 85℃; for 12h; Inert atmosphere; | 99% |
With potassium carbonate In acetonitrile for 18h; Heating; | 97% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h; | 100% |
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h; | 100% |
With triethylamine In tetrahydrofuran for 3h; Ambient temperature; | 94% |
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h; | 105 g |
With triethylamine In tetrahydrofuran at 0 - 20℃; for 3h; |
2',4'-dihydroxy-4-acetophenone
benzyl bromide
1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone
Conditions | Yield |
---|---|
Stage #1: 2',4'-dihydroxy-4-acetophenone With potassium carbonate In acetonitrile for 1h; Reflux; Stage #2: benzyl bromide In acetonitrile Reflux; | 99% |
Stage #1: 2',4'-dihydroxy-4-acetophenone With potassium carbonate; potassium iodide In acetone at 50℃; for 0.5h; Stage #2: benzyl bromide In acetone for 5h; Reflux; | 97% |
With potassium carbonate In acetone for 24h; Reflux; | 93% |
2',4'-dihydroxy-4-acetophenone
chloromethyl methyl ether
2-hydroxy-4-(methoxymethoxy)acetophenone
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 4.5h; | 99% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 96.8% |
With potassium carbonate In acetone for 0.5h; | 95.6% |
2',4'-dihydroxy-4-acetophenone
1-(2,4-dihydroxyphenyl)ethylamine
Conditions | Yield |
---|---|
With formate dehydrogenase; Arthrobacter citreus S9 ω-transaminase; ATA-113 ω-transaminase; sodium formate; isopropylamine; NADH; yeast alcohol dehydrogenase pH=7; aq. phosphate buffer; Enzymatic reaction; optical yield given as %ee; | 99% |
2',4'-dihydroxy-4-acetophenone
tert-butyldimethylsilyl chloride
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In dichloromethane at 0℃; Inert atmosphere; | 99% |
With 1H-imidazole In N,N-dimethyl-formamide at 40℃; for 5.5h; | 78% |
With 1H-imidazole In N,N-dimethyl-formamide at 40℃; for 5.5h; |
2',4'-dihydroxy-4-acetophenone
bromethyl methyl ether
2-hydroxy-4-(methoxymethoxy)acetophenone
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere; | 99% |
With potassium carbonate In acetone at 50℃; | 64% |
With potassium carbonate In acetone Reflux; | 59% |
2',4'-dihydroxy-4-acetophenone
benzoyl chloride
2,4-dibenzoyloxyacetophenone
Conditions | Yield |
---|---|
With pyridine In diethyl ether at 0℃; for 1h; | 98.5% |
With pyridine at 20℃; for 2h; Acylation; | 98% |
With pyridine for 1h; | 83% |
2',4'-dihydroxy-4-acetophenone
chloromethyl methyl ether
2',4'-bis(methoxymethoxy)acetophenone
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate | 98.3% |
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 6.5h; | 98% |
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 5h; Ambient temperature; | 90% |
2',4'-dihydroxy-4-acetophenone
1-(2,4-dihydroxy-3-iodophenyl)ethanone
Conditions | Yield |
---|---|
With potassium iodate; iodine In ethanol; water at 20℃; Inert atmosphere; | 98% |
With potassium iodate; iodine In ethanol; water at 20℃; Inert atmosphere; regiospecific reaction; | 98% |
With potassium iodate; iodine In ethanol; water at 20℃; Inert atmosphere; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In water at 100℃; for 6h; | 98% |
With hydroxylamine hydrochloride; sodium acetate In water for 6h; Reflux; | 98% |
With hydroxylamine hydrochloride; sodium acetate In water at 70℃; for 6h; | 79% |
Conditions | Yield |
---|---|
With zirconyl nitrate In acetone at 50℃; for 5h; | 98% |
With yttrium(lll) nitrate hexahydrate In acetic acid at 20℃; for 3h; | 94% |
With nitric acid; acetic acid at 20℃; for 7h; regioselective reaction; | 53.7% |
2-(4-bromophenyl)acetyl chloride
2',4'-dihydroxy-4-acetophenone
3-(p-bromophenyl)-7-(p-bromophenylacetoxy)-4-methylcoumarin
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate In benzene for 4h; Ambient temperature; | 98% |
2',4'-dihydroxy-4-acetophenone
(2-trimethylethylsilylethoxy)methyl chloride
2,4-bis<<2-(trimethylsilyl)ethoxy>methoxy>acetophenone
Conditions | Yield |
---|---|
With dmap; triethylamine In benzene at 110℃; for 3h; | 98% |
2',4'-dihydroxy-4-acetophenone
allyl bromide
1-(2,4-bis(allyloxy)phenyl)ethanone
Conditions | Yield |
---|---|
With potassium carbonate Inert atmosphere; | 98% |
With potassium carbonate In N,N-dimethyl-formamide | 98% |
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 60℃; for 5h; Inert atmosphere; | 98% |
With caesium carbonate In N,N-dimethyl-formamide at 60℃; for 5h; | 98% |
With potassium carbonate In acetone for 12h; Heating; | 59.2% |
2',4'-dihydroxy-4-acetophenone
phenylacetyl chloride
4-methyl-3-phenyl-7-phenylacetoxy coumarin
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate In benzene for 4h; Ambient temperature; | 98% |
2',4'-dihydroxy-4-acetophenone
acetone
7-hydroxy-2,2-dimethyl-chroman-4-one
Conditions | Yield |
---|---|
With piperidine for 0.166667h; Neat (no solvent); Microwave irradiation; | 98% |
With Amberlite IRA 400 basic resin for 0.0833333h; Microwave irradiation; Neat (no solvent); | 89% |
With pyrrolidine In toluene for 14h; Heating; | 86.7% |
2',4'-dihydroxy-4-acetophenone
hydroxylamine hydrochloride
(1Z)-1-(2,4-dihydroxyphenyl)ethanone oxime
Conditions | Yield |
---|---|
In pyridine at 20℃; | 98% |
2',4'-dihydroxy-4-acetophenone
butanone
2-ethyl-7-hydroxy-2-methyl-chroman-4-one
Conditions | Yield |
---|---|
With piperidine for 0.166667h; Neat (no solvent); Microwave irradiation; | 98% |
With Amberlite IRA 400 basic resin for 0.133333h; Microwave irradiation; Neat (no solvent); | 85% |
2',4'-dihydroxy-4-acetophenone
propargyl bromide
1-(2,4-bis(prop-2-yn-1-yloxy)phenyl)ethan-1-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 12h; Reflux; | 98% |
With potassium carbonate In acetone for 48h; Reflux; | |
With potassium carbonate In toluene for 12h; Reflux; | |
Stage #1: 2',4'-dihydroxy-4-acetophenone With potassium carbonate In N,N-dimethyl-formamide at 0℃; for 0.25h; Inert atmosphere; Stage #2: propargyl bromide In N,N-dimethyl-formamide; toluene at 0 - 20℃; for 17h; Inert atmosphere; |
2',4'-dihydroxy-4-acetophenone
(E)-4-(1-hydrazonoethyl)benzene-1,3-diol
Conditions | Yield |
---|---|
With hydrazine hydrate In N,N-dimethyl-formamide at 20℃; for 4h; | 97% |
With hydrazine hydrate; acetic acid In methanol at 20℃; | 82% |
With ethanol; hydrazine | |
With hydrazine hydrate In water for 0.0333333h; Microwave irradiation; |
2',4'-dihydroxy-4-acetophenone
acetic anhydride
2,4-diacetoxy acetophenone
Conditions | Yield |
---|---|
With magnesium(II) perchlorate at 20℃; for 0.5h; | 97% |
With pyridine; aluminum oxide at 120 - 122℃; for 1h; microwave irradiation; | 54% |
With sodium acetate bei 0.5 Minuten langem Kochen; |
2',4'-dihydroxy-4-acetophenone
prenyl bromide
1-[2-hydroxy-4-(3-methylbut-2-enyloxy)phenyl]ethanone
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 80℃; Williamson Ether Synthesis; | 97% |
With potassium carbonate In acetone for 8h; Reflux; | 89% |
With potassium carbonate In acetone at 80℃; for 6h; | 82% |
2',4'-dihydroxy-4-acetophenone
ethyl iodide
1-(4-ethoxy-2-hydroxyphenyl)ethanone
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 80℃; for 6h; | 97% |
With potassium carbonate In N,N-dimethyl-formamide for 4h; | 63% |
2',4'-dihydroxy-4-acetophenone
isobutyryl chloride
2',4'-di-(2-methylpropanoyloxy)-acetophenone
Conditions | Yield |
---|---|
With pyridine at 20℃; | 97% |
2',4'-dihydroxy-4-acetophenone
cyclohexanone
7-hydroxy-spiro<2H-1-benzopyran-2,1'-cyclohexane>-4(3H)-one
Conditions | Yield |
---|---|
With piperidine for 0.166667h; Neat (no solvent); Microwave irradiation; | 97% |
With Amberlite IRA 400 basic resin for 0.1h; Microwave irradiation; Neat (no solvent); | 90% |
With pyrrolidine In acetonitrile at 45℃; for 8h; | 84% |
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