Xingshun's expertise and flexibility have made the company become one of the leading manufacturer of Naphthalene series, Biphenylseries , Phenanthrene series, Anthracene series, which are wildly used in the field of electronic chemical and polyam
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryProduct Name: 1'-Acetonaphthone Synonyms: 1-(1-naphthalenyl)-ethanon;1-(1-Naphthalenyl)ethanone;1-(1-naphthalenyl)-Ethanone;1-(1-Naphthyl)ethanone;1-(1-Naphthylenyl)ethanone;1-Acetonaphthalene;1-naphtha
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAbout Product Details
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inquiryProduct name 1-Acetonaphthone Product category Naphthalene series CAS NO. 941-98-0 Structural formula Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtig
Appearance:Clear pale yellow to yellow liquid Storage:Sealed in dry,Room Temperature Package:25kg/barrel Application:intermediates Transportation:Express/Sea/Air Port:any port in China
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inquiryBeluga chemical professional supply High quality 1'-Acetonaphthone CAS 941-98-0 Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in Chin
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
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inquiryProduct Name: 1'-Acetonaphthone CAS: 941-98-0 MF: C12H10O MW: 170.21 EINECS: 213-384-1 Mol File: 941-98-0.mol 1'-Acetonaphthone Structure 1'-Acetonaphthone Chemical Properties Melting point 10.5 °C (lit.) Boili
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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1-(1-naphthyl)ethanol
1'-naphthacetophenone
Conditions | Yield |
---|---|
With ruthenium trichloride; iodobenzene; potassium peroxomonosulfate In water; acetonitrile at 20℃; for 7h; | 100% |
With ruthenium trichloride; iodobenzene; potassium peroxymonosulfate In water; acetonitrile at 20℃; for 7h; Inert atmosphere; | 100% |
With silica gel supported bis(trimethylsilyl) chromate In dichloromethane at 25℃; for 0.333333h; | 99% |
Conditions | Yield |
---|---|
Stage #1: methyllithium; 1-Cyanonaphthalene In tetrahydrofuran at -90℃; for 0.5h; Stage #2: With water | 100% |
naphthalene
acetyl chloride
A
1'-naphthacetophenone
B
methyl 2-naphthyl ketone
Conditions | Yield |
---|---|
aluminium trichloride In 1,2-dichloro-ethane at 0℃; Rate constant; Kinetics; Mechanism; other temperature; other concentrations; | A 99% B 1% |
aluminium trichloride In 1,2-dichloro-ethane at 0℃; Thermodynamic data; ΔH<*>(activation); Σ<*>(activation); | A 99% B 1% |
With aluminium trichloride; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride at 0℃; for 1h; | A 89% B 2% |
4-methyl-N'-(1-(naphthalen-1-yl)ethylidene)benzenesulfonohydrazide
1'-naphthacetophenone
Conditions | Yield |
---|---|
With silica-supported selenamide; dihydrogen peroxide In tert-butyl alcohol at 55℃; for 20h; | 99% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; water; palladium diacetate; 2-(3,5-dimethyl-1H-pyrazol-1-yl)pyridine at 60℃; for 5h; | 98% |
Conditions | Yield |
---|---|
With triethylamine; Pd(Ac2O)2-DPPP In N,N-dimethyl-formamide at 80℃; for 0.5h; | 97% |
With triethylamine; Pd(Ac2O)2-DPPP In N,N-dimethyl-formamide at 80℃; for 0.5h; reaction with other aryl triflates; | 97% |
With hydrogenchloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate 1) DMF, 80 deg C, 1 h; Yield given. Multistep reaction; | |
With hydrogenchloride; triethylamine; palladium diacetate; 2.9-dimethyl-1,10-phenanthroline 1.) DMF, 40 deg C, 2.5 h, 2.) 0.5 h; Yield given. Multistep reaction; |
1-ethynylnaphthalene
1'-naphthacetophenone
Conditions | Yield |
---|---|
With cobalt(III)((CH2NCHC6H4(O))2)(OAc); sulfuric acid In methanol; water at 80℃; for 20h; Schlenk technique; | 97% |
With sulfuric acid; C18H15CoN2O10S2(2-)*2Na(1+); water In methanol at 80℃; for 20h; Schlenk technique; | 96% |
With methanol; [Co((dimethylglyoximate)BF2)2•2H2O] at 65℃; for 2.5h; Sealed tube; Neutral conditions; regioselective reaction; | 93% |
Conditions | Yield |
---|---|
Stage #1: -butyl vinyl ether; 1-Bromonaphthalene With palladium diacetate; 1,3-bis-(diphenylphosphino)propane; triethylamine In various solvent(s) at 100℃; for 24h; Heck reaction; Stage #2: With hydrogenchloride Further stages.; | 95% |
Stage #1: -butyl vinyl ether; 1-Bromonaphthalene With meso-2,4-bis(diphenylphosphino)pentane; triethylamine; palladium diacetate In dimethyl sulfoxide at 115℃; for 36h; Heck arylation; Stage #2: With hydrogenchloride In dimethyl sulfoxide at 20℃; | 94% |
Stage #1: -butyl vinyl ether; 1-Bromonaphthalene With triethylamine; tris-(o-tolyl)phosphine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; 1,3-bis-(diphenylphosphino)propane; palladium dichloride at 130℃; for 2h; Heck reaction; microwave irradiation; Stage #2: With hydrogenchloride In water Further stages.; | 71% |
With hydrogenchloride; triethylamine; palladium diacetate; 2.9-dimethyl-1,10-phenanthroline 1.) DMF, 80 deg C, 24 h, 2.) 0.5 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: naphthalene With copper(I) oxide In acetonitrile at 25℃; for 0.666667h; Stage #2: formyl acetic anhydride With oxalic acid In acetonitrile for 2h; Temperature; | 95% |
1'-naphthacetophenone
Conditions | Yield |
---|---|
With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol; water at 60℃; for 10h; Tamao-Kumada Oxidation; Schlenk technique; Glovebox; | 94% |
1-(1-naphthalenyl)ethanone oxime
1'-naphthacetophenone
Conditions | Yield |
---|---|
With potassium permanganate; montmorillonite K-10 for 0.333333h; | 93% |
With bismuth(III) nitrate; silica gel In tetrahydrofuran; water for 9h; Heating; | 87% |
Conditions | Yield |
---|---|
With hydrogenchloride In toluene 1.) 0 deg C, 3 min, then 15 deg C, 5 min, 2.) -10 deg C; | 92% |
(S)-1-(1-Naphthyl)ethanol
1'-naphthacetophenone
Conditions | Yield |
---|---|
With 2-azaadamantane-N-oxyl; oxygen In aq. acetate buffer at 20℃; for 8h; pH=4.5; Reagent/catalyst; Green chemistry; Enzymatic reaction; chemoselective reaction; | 92% |
2-(naphthalen-1-yl)propanenitrile
1'-naphthacetophenone
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; oxygen In dimethyl sulfoxide for 3h; | 91% |
1'-naphthacetophenone
Conditions | Yield |
---|---|
With 2,2,2-trifluoroethanol; oxygen; vanadium(V) oxychloride for 3h; deprotection; Heating; | 91% |
With 2,2,6,6-tetramethylpiperidinyl-lithium In tetrahydrofuran; hexane at -78℃; for 4h; Inert atmosphere; | 88% |
With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate at 20℃; for 0.75h; | 88% |
2-methyl-2-(naphthalen-1-yl)-1,3-dithiane
1'-naphthacetophenone
Conditions | Yield |
---|---|
With dihydrogen peroxide; tantalum pentachloride; sodium iodide In water; ethyl acetate at 20℃; for 2.5h; | 91% |
With dihydrogen peroxide; tantalum pentachloride; sodium iodide In water; ethyl acetate at 20℃; for 2.5h; | 91% |
With Amberlite IR-120; palladium on activated charcoal In methanol for 18h; Heating; | 81% |
trimethyl indium
naphthalene-1-carbonic acid chloride
1'-naphthacetophenone
Conditions | Yield |
---|---|
With mesoporous MCM-41-immobilized phosphine-free heterogeneous palladium(0)-schiff base complex In tetrahydrofuran at 68℃; for 2h; Inert atmosphere; Green chemistry; | 91% |
Conditions | Yield |
---|---|
With 2C60H80NaO12(2+)*Cl6Pd2(2-); potassium hydrogencarbonate; triphenylphosphine In toluene at 110℃; for 3h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; palladium diacetate; trifluoroacetic acid In tetrahydrofuran; water at 80℃; for 36h; Schlenk technique; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
Stage #1: 1-(2-hydroxy-1-naphthyl)ethan-1-one With TentaGel-N(R)C(O)CH2C2F4OC2F4SO2F; potassium carbonate In N,N-dimethyl-formamide at 20℃; Stage #2: With formic acid; 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate In N,N-dimethyl-formamide at 85℃; for 2h; Further stages.; | 86% |
trimethyl-(1-naphthalen-1-yl-ethoxy)-silane
1'-naphthacetophenone
Conditions | Yield |
---|---|
With γ-picolinium chlorochromate In dichloromethane at 20℃; for 6h; | 85% |
Conditions | Yield |
---|---|
With 1,3-bis-(diphenylphosphino)propane; palladium diacetate; p-benzoquinone In N,N-dimethyl-formamide at 130℃; for 0.0833333h; oxidative Heck reaction; regiospecific reaction; | 85% |
Conditions | Yield |
---|---|
In tetrahydrofuran; diethyl ether; hexane at 20℃; for 15h; Solvent; Schlenk technique; Inert atmosphere; chemoselective reaction; | 85% |
1-(naphthalen-1-yl)-2-phenoxyethan-1-one
1'-naphthacetophenone
Conditions | Yield |
---|---|
With 2,6-bis[1-(2,6-dimethylphenylimino)ethyl]pyridine cobalt(II)dichloride; bis(pinacol)diborane; sodium t-butanolate In tetrahydrofuran; methanol at 65℃; for 3h; Schlenk technique; Inert atmosphere; | 84% |
carbon monoxide
1-naphthyl triflate
tetramethylstannane
1'-naphthacetophenone
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; 4 A molecular sieve; lithium chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In N,N-dimethyl-formamide at 90℃; under 2660 Torr; for 1.5h; | 83% |
Conditions | Yield |
---|---|
With LiCl; CO; dichloro{1,1'-bis(diphenylphosphino)ferrocene}palladium(II) In N,N-dimethyl-formamide High Pressure; the triflate and the stannane in DMF contg. the Pd catalyst and LiCl heated at 90°C under high pressure CO for 1,5 h; cooled to room temp., dild. with ether, filtered, filtrate washed with water and satd. NaCl soln., dried, concd., chromd. (flash column, hexanes/EtOAc); | 83% |
carbon monoxide
1-Iodonaphthalene
trimethyl indium
1'-naphthacetophenone
Conditions | Yield |
---|---|
With mesoporous material MCM-41-immobilized palladium(II)-schiff base complex In tetrahydrofuran at 68℃; under 760.051 Torr; for 3h; Inert atmosphere; | 83% |
1-acetyl-1,4-dihydro-1,4-epoxynaphthalene
1'-naphthacetophenone
Conditions | Yield |
---|---|
With triphenyl phosphite; perrhenic acid anhydride In toluene at 100℃; for 18h; Inert atmosphere; | 83% |
4,4,5,5-tetramethyl-2-(1-(naphthalen-1-yl)ethyl)-1,3,2-dioxaborolane
1'-naphthacetophenone
Conditions | Yield |
---|---|
With 2-(2-methoxyphenylamino)-4-(2-methoxyphenylimino)pent-2-ene; copper diacetate In pyridine; acetic acid; acetonitrile at 60℃; for 16h; chemoselective reaction; | 82% |
Conditions | Yield |
---|---|
With tert.-butylnitrite; N-hydroxyphthalimide In acetonitrile at 80℃; for 24h; Schlenk technique; | 80% |
With tert.-butylhydroperoxide; 1-n-butyl-3-methylimidazolim bromide In water at 20℃; for 12h; | 80% |
With FeH6Mo6O24(3-)*3H3N*3H(1+)*7H2O; tetrabutylammomium bromide; dihydrogen peroxide In 1,4-dioxane at 70℃; for 24h; | 78% |
1'-naphthacetophenone
1-(1-naphthyl)ethanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol for 2h; | 100% |
Stage #1: 1'-naphthacetophenone With sodium tetrahydroborate In ethanol Stage #2: With hydrogenchloride In ethanol | 100% |
Stage #1: 1'-naphthacetophenone With Trimethyl borate; dimethylsulfide borane complex; (-)-3-amino-6,6-dimethyl-2-hydroxy-bicyclo[3.1.1]heptane In tetrahydrofuran at 20℃; Stage #2: With methanol In tetrahydrofuran | 98% |
1'-naphthacetophenone
(S)-1-(1-Naphthyl)ethanol
Conditions | Yield |
---|---|
With [(R,R,R)-Ru(BINAP-PO3H2)(DPEN)Cl2] on magnetite nanoparticle; potassium tert-butylate; hydrogen In isopropyl alcohol at 20℃; under 36200.4 Torr; for 20h; | 100% |
With potassium hydroxide; (R,R)-1,2-diphenylethylenediamine; hydrogen; [RuCl2((R)-3,3'-dm-binap)(dmf)n] In isopropyl alcohol at 20℃; under 6080 Torr; | 99% |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C53H73FeN2O2PS; hydrogen; lithium tert-butoxide In isopropyl alcohol at 60℃; under 22801.5 Torr; for 12h; Autoclave; enantioselective reaction; | 99% |
1'-naphthacetophenone
Triethoxyvinylsilane
2'-<2-(triethoxysilyl)ethyl>-1'-acetonaphthone
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; sodium formate; triphenylphosphine In toluene at 140℃; for 0.3h; | 100% |
With carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II) In toluene for 6h; Heating; | 67% |
With bis(1,5-cyclooctadiene)iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; C38H28P2 In 1,3-dioxane at 130℃; for 24h; Reagent/catalyst; regioselective reaction; | 45% |
1'-naphthacetophenone
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
2-(naphthalen-1-yl)pent-4-en-2-ol
Conditions | Yield |
---|---|
With indium iodide In tetrahydrofuran at 40℃; for 24h; | 100% |
With methanol; indium (III) tris(hexamethyldisilyl) amide In toluene at 20℃; for 6h; Inert atmosphere; | 100% |
With (PPh3)3CuF In tetrahydrofuran at 20℃; for 3h; | 98% |
With indium In water at 30℃; for 24h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With sodium at 0 - 20℃; for 3h; Claisen Condensation; | 100% |
1'-naphthacetophenone
(R)-1-(naphth-1-yl)ethanol
Conditions | Yield |
---|---|
With potassium hydroxide; hydrogen; (R)-3,3'-dimethyl-[1,1'-binaphthalene]-2,2'-diamine; [RuCl2((R)-3,3'-dm-binap)(dmf)n]; (S,S)-1,2-diphenyl-1,2-diaminoethane In isopropyl alcohol at 20℃; under 6080 Torr; for 4h; | 99% |
With [Fe(II)(N-isocyano-N-isopropylpropan-2-amine)2((5S,8S,14aS,18aS)-5,8-diphenyl-5,6,7,8,13,14,14a,15,16,17,18,18a,19,20-tetradecahydrotribenzo[b,f,l][1,4]diaza[8,11]diphosphacyclotetradecine)](BF4)2; isopropyl alcohol; sodium t-butanolate at 75℃; for 1.5h; Glovebox; enantioselective reaction; | 99.3% |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (SC,SC,RFC)-1-(diphenylphosphino)-2-[1-N-((4S)-4-tert-butyl-2-oxazolinyl-2-ylmethyl)ethyl]ferrocene; hydrogen; potassium carbonate In isopropyl alcohol at 25℃; under 15201 Torr; for 2h; Glovebox; Autoclave; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 20℃; Claisen Schmidt condensation; Cooling with ice; | 99.2% |
Conditions | Yield |
---|---|
With potassium fluoride; 4-chloromethoxybenzene; palladium diacetate In tetrahydrofuran; water at 20℃; for 1h; Inert atmosphere; chemoselective reaction; | 99% |
With polymethylhydrosiloxane; iron(III) chloride hexahydrate In 1,2-dichloro-ethane at 120℃; for 1h; Microwave irradiation; | 98% |
With triethylsilane; indium(III) bromide In chloroform at 60℃; for 1h; Inert atmosphere; | 95% |
1'-naphthacetophenone
2-bromoaceto-1-naphthone
Conditions | Yield |
---|---|
With pyridinium hydrobromide perbromide In tetrahydrofuran; chloroform at 20℃; for 18h; | 99% |
With bromine In 1,4-dioxane at 20℃; for 0.833333h; | 93% |
With pyridinium hydrobromide perbromide In tetrahydrofuran; chloroform at 20℃; | 93.5% |
1'-naphthacetophenone
chloromethyl p-tolyl sulfoxide
Conditions | Yield |
---|---|
With n-butyllithium; diisopropylamine In tetrahydrofuran at -65℃; for 0.416667h; | 99% |
1'-naphthacetophenone
A
(S)-1-(1-Naphthyl)ethanol
B
(R)-1-(naphth-1-yl)ethanol
Conditions | Yield |
---|---|
With dimethylsulfide borane complex; (S)-2-(anilinodiphenylmethyl)pyrrolidine In tetrahydrofuran at 20℃; for 2h; enantioselective reaction; | A n/a B 99% |
With dimethylsulfide borane complex In tetrahydrofuran at 20℃; for 2h; enantioselective reaction; | A n/a B 99% |
With (mer-[(S,S)-1,5-dimethyl-2,4-bis(4-phenyl-1,3-oxazolin-2-yl)benzene(1-)]Ru(CO)Cl)2(ZnCl2); hydrogen; sodium methylate In isopropyl alcohol at 40℃; under 22801.5 Torr; for 24h; Inert atmosphere; Autoclave; optical yield given as %ee; enantioselective reaction; | A 96% B n/a |
Conditions | Yield |
---|---|
With C84H110N10Zn2 In neat (no solvent) at 20℃; for 12h; Sealed tube; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
chloro(1,5-cyclooctadiene)rhodium(I) dimer; asymmetric tetraphenyl-tetraoxa-phosphazulene derivative In toluene at 0℃; for 24h; enantioselective hydrosilylation; | |
With silver tetrafluoroborate; (S)-[RhBr(nbd)(oxazolinyl-carbene)] In dichloromethane at -60℃; for 10h; |
Conditions | Yield |
---|---|
With C29H46LaN3Si2 at 15℃; for 2h; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
With zinc(II) iodide In acetonitrile for 48h; Addition; | 97% |
With antimony(III) chloride at 20℃; for 0.25h; Neat (no solvent); | 95% |
1'-naphthacetophenone
C6H4C4H3COC(2)H3
Conditions | Yield |
---|---|
With water-d2 In Dimethoxymethane | 99% |
With water-d2; sodium hydroxide |
1'-naphthacetophenone
O-(tert-butyl)hydroxylamine hydrochloride
1-acetylnaphthalene O-tert-butyl oxime
Conditions | Yield |
---|---|
With sodium acetate In ethanol at 20℃; for 27h; | 99% |
1'-naphthacetophenone
ethyl acetoacetate
malononitrile
6-amino-2,4-dihydro-3,4-dimethyl-4-(naphthalen-1-yl)pyrano[2,3-c]pyrazole-5-carbonitrile
Conditions | Yield |
---|---|
With hydrazine hydrate; heptakis(6-amino-6-deoxy)-β-cyclodextrin at 20℃; for 0.0166667h; Neat (no solvent); | 99% |
Conditions | Yield |
---|---|
With [Cp*Co(vinyltrimethylsilane)2] In benzene-d6 at 20℃; for 14h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With C84H110N10Zn2 In neat (no solvent) at 20℃; for 6h; Sealed tube; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
With C14H24N4Si(1+)*I(1-) In benzene-d6 at 90℃; for 6h; Catalytic behavior; Inert atmosphere; Schlenk technique; regioselective reaction; | 86% |
With bis-(phosphoranyl)methanido aluminum hydride In benzene-d6 at 110℃; for 6h; Inert atmosphere; | 54% |
With C27H44AlN3 at 20℃; for 4h; Inert atmosphere; Glovebox; |
Conditions | Yield |
---|---|
With C114H137F6N3O8P2S2 In diethyl ether at -20℃; Mukaiyama Aldol Addition; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: 1'-naphthacetophenone With bis(trifluoromethanesulfonyl)amide In diethyl ether at -78 - 23℃; Mukaiyama Aldol Addition; Schlenk technique; Inert atmosphere; Stage #2: ketene t-butyldimethylsilyl methyl acetal In diethyl ether at -20℃; for 0.5h; Mukaiyama Aldol Addition; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; C38H28P2 In 1,3-dioxane at 130℃; for 24h; Reagent/catalyst; regioselective reaction; | 99% |
1'-naphthacetophenone
toluene-4-sulfonic acid hydrazide
4-methyl-N'-(1-(naphthalen-1-yl)ethylidene)benzenesulfonohydrazide
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water for 24h; Reflux; | 98% |
In methanol at 20℃; | 89% |
With hydrogenchloride In ethanol for 1h; Heating; | 77% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 50 - 60℃; Sonication; Green chemistry; | 98% |
Conditions | Yield |
---|---|
With methanol; O-benzenesulfonyl-acetohydroxamic acid ethyl ester; toluene-4-sulfonic acid at 23℃; for 24h; Inert atmosphere; | 98% |
With O-benzenesulfonyl-acetohydroxamic acid ethyl ester; toluene-4-sulfonic acid In ethanol at 20℃; for 24h; | 62% |
1'-naphthacetophenone
methyl magnesium iodide
2-(naphthalen-1-yl)propan-2-ol
Conditions | Yield |
---|---|
In diethyl ether for 2h; Ambient temperature; | 97.7% |
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