Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accre
Cas:96-47-9
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiry2-Methyltetrahydrofuran CAS No: 96-47-9 Molecular Structure: Specifications: Item Details
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inquiryTIANFUCHEM--96-47-9--2-Methyltetrahydrofuran factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry2-Methyltetrahydrofuran Basic information Product Name: 2-Methyltetrahydrofuran Synonyms: 2-Methyltetrahydrofuran,For Grignard reaction,anhydrous, stabilized;2-Methyltetrahydrofuran,99+%,Extra Dry,Stabilized;2-Methyltetrahydrofuran,99+%,Extra D
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inquiryProduct Name 2-Methyltetrahydrofuran Synonyms 2-Methylfuranidine;2-Methyloxolane;Furan, 2-methyl-tetrahydro-;Tetrahydrofuran, 2-methyl-;Tetrahydrosylvan;TETRAHYDROSILVAN;
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
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inquiryProduct Detail Minimum Order Qty. 10 Gram
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inquiryHebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several
Cas:96-47-9
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inquiryProduct Name 2-Methyl tetrahydrofuran CAS No 96-47-9 Structure Molecular formula C5H1
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiry2-Methyltetrahydrofuran / METHFAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Intermedia
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
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inquiryProduct Name: 2-Methyltetrahydrofuran Synonyms: 2-Methyltetrahydrofuran,For Grignard reaction,anhydrous, stabilized;2-Methyltetrahydrofuran,99+%,Extra Dry,Stabilized;2-Methyltetrahydrofuran,99+%,Extra Dry over Molecular Sieve,Stabilized;2-Methy
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inquiryProduct name: 2-Methyltetrahydrofuran CAS No.: 96-47-9 Molecule Formula:C5H10O Molecule Weight:86.13 Purity: 99.0% Package: 200kg/drum Description:Colorless clear liquid Manufacture Standards:Enterprise Standard
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inquiryStock products, own laboratoryAppearance:Colorless to light yellow liquid Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryShanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is
Cas:96-47-9
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
excellent quality and reliable supplierAppearance:COA mentioned Storage:COA mentioned Package:Standard or custom package Application:pharmaceutical raw materails Transportation:sea/air /courier Port:China main port
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1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and
1. Factory steady offer directly; 2. More than 10 years of production and process improved experience; 3. Professional hazard chemical Logistics; 4. Reliable quality assurance 5. Punctual delivery time Appearance:Clear colorless Liquid Sto
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inquiryHenan Wising Chem specialize in sourcing the chemicals in China. We are associated with many trusted manufacturers each having different area of expertise required for meeting the needs of our local as well as overseas buyers . We have access t
Cas:96-47-9
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inquiryAppearance: colorless liquid Purity: 99.5% Water: 0.05%max Packing: 170kg per drum. Production Capacity: 1400kg per day. Payment terms: TT after BL date; L/C; 20%TT in advance and balance against copy of BL. Lead time: 3-10days after th
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inquiryConditions | Yield |
---|---|
With 3% Pd/C; hydrogen In isopropyl alcohol at 219.84℃; under 25858.1 Torr; for 5h; Inert atmosphere; | 100% |
With palladium-aluminum at 150℃; Hydrogenation; | |
With osmium at 80℃; Hydrogenation; |
Conditions | Yield |
---|---|
With hydrogen In isopropyl alcohol under 30003 Torr; for 5h; Reagent/catalyst; Autoclave; | 99% |
Trichlorbutylstannan for 0.24h; | 96% |
Nafion-H at 135℃; for 5h; | 90% |
Conditions | Yield |
---|---|
With hydrogen In hexane at 180℃; for 4h; Temperature; Reagent/catalyst; Solvent; Autoclave; | 98% |
Multi-step reaction with 2 steps 1: hydrogen / 1,4-dioxane / 2 h / 190 °C / 30003 Torr / Autoclave 2: hydrogen / 1,4-dioxane / 5 h / 190 °C / 30003 Torr / Autoclave View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen / 1,4-dioxane / 2 h / 190 °C / 30003 Torr / Autoclave 2: hydrogen / 1,4-dioxane / 5 h / 190 °C / 30003 Torr / Autoclave View Scheme |
Conditions | Yield |
---|---|
With palladium on silica; copper phyllosilicate; hydrogen at 180℃; Reagent/catalyst; Inert atmosphere; | 97.1% |
Stage #1: furfural With hydrogen at 200℃; under 760.051 Torr; Flow reactor; Stage #2: With hydrogen at 120℃; under 760.051 Torr; Temperature; Flow reactor; | 96.3% |
With hydrogen; 5% palladium over charcoal; copper chromite catalyst E 403-TU at 175℃; under 760.051 Torr; Product distribution / selectivity; In the presence of quartz glass rings (as an evaporation zone); |
Conditions | Yield |
---|---|
With tris(2,4-pentanedionato)ruthenium(III); N-butyl-N'-(4-sulfobutyl)-imidazolium p-toluenesulfonate; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] at 160℃; under 75007.5 Torr; for 18h; Inert atmosphere; Autoclave; Ionic liquid; | 95% |
Multi-step reaction with 2 steps 1: sodium; alcohol 2: hydrochloric acid; alcohol / 150 °C / im Druckrohr View Scheme | |
Multi-step reaction with 2 steps 1: sodium; xylene 2: HI / auf dem Wasserbad und folgenden Reduzieren mit Zinkstaub und Eisessig View Scheme |
Conditions | Yield |
---|---|
With bromopentacarbonylmanganese(I); phenylsilane In toluene at 100℃; for 24h; Catalytic behavior; Time; Temperature; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 95% |
With Cu/SiO2 at 220℃; under 22502.3 Torr; Temperature; | 93% |
With ammonium hexafluorophosphate; Λ(+)-tris(pentane-2,5-dionato)ruthenium; N-butyl-N'-(4-sulfobutyl)-imidazolium p-toluenesulfonate; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] at 160℃; under 75007.5 Torr; for 18h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With N-iodo-succinimide In chlorobenzene for 2h; Irradiation; | A 94% B 1% C n/a |
With N-iodo-succinimide In chlorobenzene for 2h; Product distribution; Irradiation; var. irradiat. times, temps. and light cond.; | A 94% B 1% C n/a |
(C4H9)3SnOCH(CH3)CH2CH2CH2Cl
A
2-methyltetrahydrofuran
B
tributyltin chloride
Conditions | Yield |
---|---|
decompn. of the crude compound at 120°C (0.5 h); | A 93% B n/a |
decompn. of the crude compound at 120°C (0.5 h); | A 93% B n/a |
Conditions | Yield |
---|---|
With Nd magnetically supported catalyst In dichloromethane at 83℃; for 24h; Schlenk technique; Inert atmosphere; | 91% |
With aluminium(III) triflate In nitromethane at 101℃; for 1h; | 87% |
With ytterbium(III) triflate at 120℃; Inert atmosphere; Ionic liquid; | 78% |
Conditions | Yield |
---|---|
With hydrogen In para-xylene at 180℃; under 30003 Torr; for 48h; Glovebox; Sealed tube; chemoselective reaction; | 90% |
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; iodine Irradiation; | 89% |
furfural
A
2-methyltetrahydrofuran
B
2-methylfuran
C
(+/-)-2-pentanol
D
2-Pentanone
Conditions | Yield |
---|---|
With hydrogen; Cu-based catalyst at 212℃; Product distribution; Further Variations:; Temperatures; reaction in vapour phase, fixed bed reactor; | A 3.3% B 88.6% C 4.8% D 2.7% |
Conditions | Yield |
---|---|
With 30% Cu/SiO2 In methanol at 190℃; under 60006 Torr; for 10h; Reagent/catalyst; Solvent; Temperature; Autoclave; | A 16.3% B 82.9% |
Conditions | Yield |
---|---|
With carbon dioxide; 5% Pd(II)/C(eggshell); hydrogen at 300℃; under 112511 Torr; Supercritical conditions; | A 82% B 6% |
N-(4-Pentenyl-1-oxy)pyridine-2(1H)-thione
2-methyltetrahydrofuran
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene at 80℃; for 0.333333h; Product distribution; Mechanism; | 80% |
Conditions | Yield |
---|---|
With hydrogen In water at 130℃; for 4h; Reagent/catalyst; Solvent; Autoclave; | A 17% B 80% |
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 20% B 79% |
With hydrogen In water at 130℃; for 24h; Reagent/catalyst; Autoclave; | A 77% B 12% |
Conditions | Yield |
---|---|
With triethylsilane; trifluorormethanesulfonic acid In dichloromethane-d2 at 20℃; for 24h; NMR tube; | 80% |
With hydrogen In neat (no solvent) at 90℃; under 15001.5 Torr; for 5h; | > 99 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: furfural With hydrogen at 200℃; under 760.051 Torr; Flow reactor; Stage #2: With hydrogen at 100℃; under 760.051 Torr; Temperature; Flow reactor; | A 79.3% B 20% |
With hydrogen In isopropyl alcohol at 229.84℃; under 30003 Torr; for 2h; | A 10% B 57% |
With carbon dioxide; palladium on activated charcoal; hydrogen In water at 80℃; for 0.333333h; |
Conditions | Yield |
---|---|
Stage #1: furfural With hydrogen at 160℃; under 760.051 Torr; Flow reactor; Stage #2: With hydrogen at 130℃; under 760.051 Torr; Flow reactor; | A 13.7% B 78.2% |
With hydrogen In 1,4-dioxane; isopropyl alcohol at 200℃; under 48754.9 Torr; for 6h; Reagent/catalyst; | A 36% B 45% |
Multi-step reaction with 2 steps 1: isopropyl alcohol; 10% Pd/C / 7.5 h / 150 °C / Inert atmosphere 2: isopropyl alcohol; 10% Pd/C / 7.5 h / 180 °C / Inert atmosphere View Scheme |
5-ketohexanoic acid
A
2-methyltetrahydrofuran
B
5-methyl-dihydro-furan-2-one
Conditions | Yield |
---|---|
With hydrogen In isopropyl alcohol at 250℃; under 52505.3 Torr; for 24h; Temperature; Reagent/catalyst; | A 75% B 8% |
With hydrogen In isopropyl alcohol at 250℃; under 52505.3 Torr; for 5h; Temperature; Reagent/catalyst; | A 22.7% B 64.5% |
phenylthio-4-pentenol
A
2-methyltetrahydrofuran
B
n-Pent-4-enyl alcohol
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In various solvent(s) at 80℃; for 0.5h; Rate constant; Mechanism; Bu3Sn. effect in SH2 displacement of alkoxy radicals from sulphur, exo cyclization; | A 73% B 26% |
furfural
A
2-methyltetrahydrofuran
B
Tetrahydrofurfuryl alcohol
C
(2-furyl)methyl alcohol
Conditions | Yield |
---|---|
Stage #1: furfural With hydrogen at 160℃; under 760.051 Torr; Flow reactor; Stage #2: With hydrogen at 120℃; under 760.051 Torr; Flow reactor; | A 13.1% B 70% C 9.1% |
With Ni3Sn2; hydrogen In isopropyl alcohol at 20 - 179.84℃; for 12h; Autoclave; | A 5 %Chromat. B 5 %Chromat. C 91 %Chromat. |
With hydrogen In isopropyl alcohol at 50℃; under 3750.38 Torr; Autoclave; |
levulinic acid
A
2-methyltetrahydrofuran
B
pentan-1-ol
C
5-methyl-dihydro-furan-2-one
Conditions | Yield |
---|---|
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 68% B 7% C 11% |
With hydrogen; CuO0.95Co0.05/SiO2 In 1,4-dioxane at 265℃; under 18751.9 Torr; | |
With hydrogen; CuO(80)SiO2(20) In 1,4-dioxane at 265℃; under 19135 Torr; Product distribution / selectivity; Inert atmosphere; |
levulinic acid
A
2-methyltetrahydrofuran
B
1,4-Pentanediol
C
(+/-)-2-pentanol
D
5-methyl-dihydro-furan-2-one
Conditions | Yield |
---|---|
With hydrogen In water at 150℃; for 4h; Reagent/catalyst; Autoclave; | A 67% B n/a C 9% D 14% |
Conditions | Yield |
---|---|
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 64% B 6% |
With hydrogen In 1,4-dioxane at 330℃; Product distribution / selectivity; | |
With hydrogen In 1,4-dioxane at 265℃; under 15001.5 Torr; Product distribution / selectivity; | |
With hydrogen; CuO(80)SiO2(20) In 1,4-dioxane at 290℃; under 19135 Torr; Product distribution / selectivity; Inert atmosphere; | |
With hydrogen; CuO(80)SiO2(20) In 1,4-dioxane at 265℃; under 15001.5 Torr; Product distribution / selectivity; Inert atmosphere; |
levulinic acid
A
2-methyltetrahydrofuran
B
(+/-)-2-pentanol
C
pentan-1-ol
Conditions | Yield |
---|---|
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 63% B 18% C 10% |
Conditions | Yield |
---|---|
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 60% B 18% |
Multi-step reaction with 2 steps 1: ruthenium-carbon composite; hydrogen / 1,4-dioxane / 5 h / 30003 Torr / Autoclave 2: ruthenium-carbon composite; hydrogen / isopropyl alcohol / 5 h / 30003 Torr / Autoclave View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen / water / 100 °C / 30003 Torr / Flow reactor; Green chemistry 2: hydrogen / water / 70 °C / 30003 Torr / Flow reactor; Green chemistry View Scheme |
levulinic acid
A
2-methyltetrahydrofuran
B
1,4-Pentanediol
C
(+/-)-2-pentanol
D
pentan-1-ol
Conditions | Yield |
---|---|
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 60% B 10% C 23% D 6% |
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; | A 25% B 27% C 34% D 7% |
With hydrogen In water at 150℃; under 37503.8 Torr; for 4h; Autoclave; |
(2-furyl)methyl alcohol
A
2-methyltetrahydrofuran
B
Tetrahydrofurfuryl alcohol
C
2-methylfuran
Conditions | Yield |
---|---|
With hydrogen In methanol at 25℃; for 1h; Reagent/catalyst; Sealed tube; Green chemistry; | A 8% B 52% C 25% |
With Ni/Al2O3; hydrogen at 180℃; under 7500.75 Torr; Reagent/catalyst; Flow reactor; |
(2-furyl)methyl alcohol
A
2-methyltetrahydrofuran
B
Tetrahydrofurfuryl alcohol
Conditions | Yield |
---|---|
With hydrogen In methanol at 25℃; under 750.075 Torr; for 1h; Reagent/catalyst; Sealed tube; Green chemistry; | A 25% B 52% |
With water; hydrogen at 199.84℃; under 60006 Torr; for 3h; Autoclave; | |
With hydrogen In ethanol at 60℃; under 2250.23 Torr; for 2h; | |
With hydrogen at 200℃; under 760.051 Torr; Flow reactor; | A 5.3 %Chromat. B 94.5 %Chromat. |
2-methyltetrahydrofuran
rac-5-iodopentan-2-ol
Conditions | Yield |
---|---|
With aluminium trichloride; sodium iodide In acetonitrile at 0℃; for 2h; regioselective ring opening of var. 2 subst. tetrahydrofurans; | 100% |
With aluminium trichloride; sodium iodide In acetonitrile at 0℃; for 2h; | 100% |
With aluminum (III) chloride; sodium iodide In acetonitrile at 0 - 20℃; for 5h; Inert atmosphere; Schlenk technique; | 58% |
2-methyltetrahydrofuran
aniline
(+/-)-2-methyl-1-phenylpyrrolidine
Conditions | Yield |
---|---|
With carbon dioxide; alumina In toluene at 237℃; under 108011 Torr; Flow reactor; Supercritical conditions; | 100% |
Stage #1: aniline With 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate In 5,5-dimethyl-1,3-cyclohexadiene at 90℃; for 0.25h; Stage #2: 2-methyltetrahydrofuran In 5,5-dimethyl-1,3-cyclohexadiene at 110℃; for 15h; Sealed tube; | 93% |
With trimethylaluminum In toluene at 20 - 110℃; for 16h; | 78% |
2-methyltetrahydrofuran
1,5,9-trimesityldipyrromethene
dibutylmagnesium
Conditions | Yield |
---|---|
Stage #1: 1,5,9-trimesityldipyrromethene; dibutylmagnesium In toluene for 0.25h; Inert atmosphere; Schlenk technique; Glovebox; Stage #2: 2-methyltetrahydrofuran In toluene Inert atmosphere; Schlenk technique; Glovebox; | 100% |
Conditions | Yield |
---|---|
With [(IPr=S)BiCl3]*CHCl3 In dichloromethane at 20℃; for 2h; Reagent/catalyst; regioselective reaction; | 98% |
K[Pt(C2H4)Cl3] In 2-methyltetrahydrofuran for 24h; Ambient temperature; | 70% |
With zinc |
2-methyltetrahydrofuran
1,4-Diiodopentane
Conditions | Yield |
---|---|
With O-phenyl phosphorodichloridate; sodium iodide for 24h; Heating; | 98% |
With N,N-diethyl-1,1,1-trimethylsilanamine; methyl iodide In toluene at 80 - 90℃; for 103h; Ring cleavage; iodination; diiodation; diiodination; | 51% |
2-methyltetrahydrofuran
2,2-Dimethylpropanoyl iodide
4-pivaloyloxy-1-iodopentane
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; Green chemistry; | 98% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With molybdenum(V) chloride In 1,2-dichloro-ethane at 50℃; for 3h; | 96% |
With zinc(II) oxide In neat (no solvent) at 0 - 20℃; Green chemistry; | 94% |
With iron In 1,2-dichloro-ethane at 70℃; for 8h; Time; Schlenk technique; Inert atmosphere; regioselective reaction; | 91% |
2-methyltetrahydrofuran
(S)-2-acetoxypropanoyl chloride
Conditions | Yield |
---|---|
With bismuth(III) chloride In dichloromethane at 20℃; | 96% |
2-methyltetrahydrofuran
acetic anhydride
1,4-diacetoxypentane
Conditions | Yield |
---|---|
With aminosulfonic acid In acetic acid at 60℃; for 4h; | 95% |
With sulfuric acid at 20℃; for 20h; | 70% |
With ytterbium(III) triflate Heating; | 47% |
at 170 - 180℃; | |
at 240℃; |
2-methyltetrahydrofuran
4-methoxy-benzoyl chloride
4-chloropentyl 4-methoxybenzoate
Conditions | Yield |
---|---|
With zinc(II) oxide In neat (no solvent) at 0 - 20℃; for 2.5h; Green chemistry; regioselective reaction; | 95% |
With iron In 1,2-dichloro-ethane at 70℃; Schlenk technique; Inert atmosphere; regioselective reaction; | 93% |
With iron pentacarbonyl Heating; |
Conditions | Yield |
---|---|
With bismuth(III) bromide In dichloromethane at 20℃; for 4h; | 95% |
With palladium diacetate at 100℃; for 2h; Microwave irradiation; | 81.9% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; Green chemistry; | 95% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; Green chemistry; | 95% |
2-methyltetrahydrofuran
ethyl iodoacetate
Propionic acid 4-iodo-1-methyl-butyl ester
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; Green chemistry; | 95% |
2-methyltetrahydrofuran
Acetyl bromide
A
1-acetoxy-4-bromopentane
B
acetic acid-(4-bromo-1-methyl-butyl ester)
Conditions | Yield |
---|---|
With zinc(II) chloride 1.) 21 deg C, 0.5 h, 2.) reflux, 2.5 h; Yields of byproduct given. Title compound not separated from byproducts; | A 93% B n/a |
With zinc(II) chloride 1.) 21 deg C, 0.5 h, 2.) reflux, 2.5 h; Yield given. Title compound not separated from byproducts; | A 93% B n/a |
Conditions | Yield |
---|---|
Stage #1: 1-amino-3-methylbenzene With 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate at 90℃; for 0.25h; Stage #2: 2-methyltetrahydrofuran at 110℃; for 10h; Sealed tube; | 93% |
Conditions | Yield |
---|---|
With bismuth(III) chloride In dichloromethane at 20℃; | 92% |
Conditions | Yield |
---|---|
With iron In 1,2-dichloro-ethane at 70℃; Schlenk technique; Inert atmosphere; regioselective reaction; | 92% |
Conditions | Yield |
---|---|
With zinc(II) oxide In neat (no solvent) at 0 - 20℃; for 2h; Green chemistry; regioselective reaction; | 92% |
With iron In 1,2-dichloro-ethane at 70℃; Schlenk technique; Inert atmosphere; regioselective reaction; | 88% |
2-methyltetrahydrofuran
Conditions | Yield |
---|---|
at -30 - 20℃; for 0.333333h; Darkness; | 92% |
2-methyltetrahydrofuran
3,5-dimethyl-N-ethylaniline
Conditions | Yield |
---|---|
With titanium tetrachloride; 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane; o-xylene at 120℃; for 14h; Sealed tube; | 92% |
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