Index Name Specifications Appearance Colorless liquid Light component wt % 0.7834% n-pentane wt%
Items Standard Test Result Content ≥95.0% 97.2120% Density of relativity 0.6253~0.6273
Cas:109-66-0
Min.Order:1 Gram
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inquiryISO9001 Good quality Competitive price On time delivery Appearance:colorless liquid Storage:kept in a light-proof,well-colsed,dry and cool place. Package:125kg/drum Application:For high density polyethylene solvent polymerization catalysts
Cas:109-66-0
Min.Order:10 Metric Ton
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Cas:109-66-0
Min.Order:1 Kilogram
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inquiryProduct name Pentane CAS NO. 109-66-0 Other names PETANE;PENTANE;PENTANE-195;PENTANE FRACTION;PETROLEUM SPIRIT 30/40;N-PENTAN;N-
n-Pentane CAS:109-66-0 Specification Alias: pentane B&J brand 4 L; Pentane,99.5%; Pentane mixed isomers; Pentane oil; pentane CAS No.: 109-66-0 EINECS No.: 203-692-4 Molecular formula: C5H12
Cas:109-66-0
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:109-66-0
Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:109-66-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:109-66-0
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryProduct Name:Pentane Synonym:n-Pentane Cas No:109-66-0 Molecular Formula:C5H12 Molecular Weight:72.15 Appearance and character: transparent colorless liquid Purity: 95%~99% Density: 0.626 Melting point: - 130℃ Boiling point: 36℃
Cas:109-66-0
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Product name Pentane CAS 109-66-0 MF C5H12 MW 72.15 Product name PentaneCAS 109-66-0 MF C5H12 MW 72.15mp-130 °Cbp36 °Cd…
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Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:109-66-0
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
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Pentane cas 109-66-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
bulk?production Application:Pharmaceutical intermediates
in stock Application:109-66-0
Cas:109-66-0
Min.Order:0
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inquiryin storeAppearance:Colorless liquid Package:500ml Application:Organic Chemicals
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Min.Order:10 Milligram
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Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryJunyuan Petroleum Group is China's leading manufacturer of n-Hexane, n-Pentane, Isopentane, Pentane Blends, Isohexane, n-Heptane and D solvents, founded in 1999. Junyuan Petroleum Group provides n-Hexane,99%, n-Pentane,99%, Isopentane, 99%, Pe
We have strong R&D center which can support and provide custom synthesis accordingly such as fine chemicals,biotechnique , pharmaceuticals etc.We can provide free sample for our clients to test anf verify the quality of our goods.LongyuChem holds str
Conditions | Yield |
---|---|
With H3Ni4(C5H5)4; hydrogen at 40℃; under 760 Torr; other olefins; var. times; | 100% |
With hydrogen In N,N-dimethyl-formamide at 25℃; under 760.051 Torr; for 10h; | 87% |
With C14H15NZr In toluene at 25℃; Reagent/catalyst; | 11% |
Conditions | Yield |
---|---|
With hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760 Torr; Kinetics; | A 99.5% B n/a |
triethylsilane
1-fluoropentane
A
triethylsilyl fluoride
B
pentane
Conditions | Yield |
---|---|
With C21H16N3P(2+) In dichloromethane at 25℃; for 1.5h; Reagent/catalyst; | A 97% B n/a |
With [(SIMes)PFMe2][B(C6F5)4]2 In dichloromethane-d2 for 1h; Catalytic behavior; Inert atmosphere; |
Conditions | Yield |
---|---|
With hydrogen; (3-ClMe2SiPr)P(Ph)CH2C4H7O2 on silicagel In propan-1-ol at 20℃; under 750.06 Torr; for 0.333333h; Product distribution; var. catalyst; | A 96% B 3% C 1% |
With hydrogen; palladium dichloride In N,N-dimethyl-formamide under 18751.5 Torr; for 0.216667h; Product distribution; Ambient temperature; various time; | A 1.7% B 82.7% C 1.4% |
With hydrogen In hexane at 24.84 - 59.84℃; Kinetics; Autoclave; Inert atmosphere; |
Conditions | Yield |
---|---|
With triethylsilane; C24BF20(1-)*C30H32BF5P(1+) at 100℃; for 48h; Reagent/catalyst; | 95% |
With triethylsilane; 2C24BF20(1-)*C18H17FNP(2+) at 25℃; for 1h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Schlenk technique; Glovebox; | 92% |
With trityl tetrakis(pentafluorophenyl)borate In 1,2-dichloro-benzene at 22℃; for 24h; Product distribution; Further Variations:; Reagents; Solvents; |
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; nickel at 120℃; | A 5% B 94% |
With hydrogen In n-heptane at 199.84℃; under 22502.3 Torr; Kinetics; Autoclave; |
Conditions | Yield |
---|---|
With hydrogen; osmium(VIII) oxide at 120℃; under 37503 Torr; for 15h; or 100 to 180 deg C, different Os-catalysts and -concentrations; Further byproducts given; | 90% |
With hydrogen; osmium(VIII) oxide at 120℃; under 37503 Torr; for 15h; Product distribution; different Os-catalysts and concentration; reaction temperatures; other alkanes, cycloalkanes, benzene, toluene; | 90% |
With platinum on activated charcoal at 300℃; Hydrogenation; |
Conditions | Yield |
---|---|
With triethylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 20h; Reduction; | 88% |
With triethylsilane; tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 20h; Reduction; | 97 % Spectr. |
Conditions | Yield |
---|---|
With hydrogen; silica gel; palladium at 330℃; | 85% |
Conditions | Yield |
---|---|
With hydrogen; 1-n-butyl-3-methylimidazolium hexafluoroantimonate; [Rh(I)(norbornadiene)(PPh3)2]PF6 In acetone at 30℃; under 750.06 Torr; for 2h; | A 83% B 13% |
With hydrogen; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; [Rh(I)(norbornadiene)(PPh3)2]PF6 In acetone at 30℃; under 750.06 Torr; | A 25% B 74% |
With C28H25ClNPTi In toluene at 25℃; Reagent/catalyst; | A 7% B 19% |
With (iPr4antraphos)Ir(C2H4) at 180℃; for 130h; Inert atmosphere; | A 45.5 %Chromat. B 27.9 %Chromat. |
hexanoic acid
A
decane
B
1-penten
C
pentane
D
2-pentene
Conditions | Yield |
---|---|
With potassium hydroxide In water pH=5.4 - 9.4; Concentration; pH-value; Kolbe Electrolysis; Electrochemical reaction; | A 82% B 44% C 30% D 26% |
With potassium hydroxide In water pH=5.8 - 9; Kolbe Electrolysis; Electrochemical reaction; | A 39% B 14% C 5% D 7% |
Conditions | Yield |
---|---|
With hydrogen; nickel(II) oxide; aluminum oxide at 500℃; | 80.5% |
With hydrogen; nickel(II) oxide; aluminum oxide at 500℃; other catalyst; other temp.; | 80.5% |
With ethanol; nickel at 29 - 35℃; under 25742.8 Torr; Hydrogenation; | |
With dihydrogen hexachloroplatinate; ethanol; H2PtCl6-(C9H19)3N-(i-C4H9)2AlH-C2H5OH; hydrogen; diisobutylaluminium hydride In toluene at 20℃; under 300.02 Torr; further reagents; |
n-butyllithium
1-methoxy-2,4,6-trinitrobenzene
A
lithium picrate
B
pentane
Conditions | Yield |
---|---|
In tetrahydrofuran Product distribution; Mechanism; formation of intermediate ς-complex, NMR spectrum of the ς-complex; | A 80% B n/a |
1-Pentyne
A
(Z)-pent-2-ene
B
(E)-pent-2-ene
C
1-penten
D
pentane
Conditions | Yield |
---|---|
With hydrogen; palladium dichloride In N,N-dimethyl-formamide under 18751.5 Torr; for 0.3h; Product distribution; Ambient temperature; various time; | A n/a B n/a C 78.5% D 2.4% |
With [Ru4(μ-H)4(CO)12] In benzene at 25℃; for 23h; Irradiation; | A 10% B 13% C 73% D 4% |
With [Ru4(μ-H)4(CO)12]; hydrogen In benzene at 25℃; under 517.1 Torr; for 24h; Irradiation; | A 13% B 10% C 66% D 11% |
chloroform
ethylmagnesium chloride
A
propane
B
3-ethylpentane
C
pentane
Conditions | Yield |
---|---|
With C31H37ClN3NiO2(1-)*Li(1+) In tetrahydrofuran at 25℃; for 0.333333h; Inert atmosphere; Overall yield = 93.4 %; | A 6% B 9.4% C 78% |
With C31H37ClFeN3O2 In tetrahydrofuran at 25℃; for 0.0833333h; Inert atmosphere; |
2-Pentyne
A
(Z)-pent-2-ene
B
(E)-pent-2-ene
C
1-penten
D
pentane
Conditions | Yield |
---|---|
With [Ru4(μ-H)4(CO)12] In benzene at 25℃; for 23h; Irradiation; | A 75% B 1% C 24% D n/a |
With [Ru4(μ-H)4(CO)12]; hydrogen In benzene at 25℃; under 517.1 Torr; for 24h; Irradiation; | A 19% B 73% C 2% D 6% |
With [Ru4(μ-H)4(CO)12]; hydrogen In benzene at 25℃; for 24h; Irradiation; | A 19% B 73% C 2% D 6% |
With hydrogen; dodecacarbonyltetrarhodium(0) at 80℃; under 760 Torr; for 3h; Product distribution; other alkynes, other carbonyl-rhodium catalyst system; | A 64 % Chromat. B 17 % Chromat. C 2 % Chromat. D 12 % Chromat. |
3,4,5,6-tetrahydro-2H-pyran-2-one
A
1 ,5-pentanediol
B
pentan-1-ol
C
pentane
Conditions | Yield |
---|---|
With hydrogen; (acetylacetonato)dicarbonylrhodium (l); molybdenum hexacarbonyl In 1,4-dioxane at 150℃; under 75007.5 Torr; for 3h; | A 75% B 19% C 6% |
Conditions | Yield |
---|---|
With aluminium trichloride; polyethoxysilane (silicone GKZh-94) In nitromethane Product distribution; | A 72% B 23% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; water; uranium(IV) chloride 1.) diglyme, 2.) diglyme, 6 h; | A 30% B 70% |
Conditions | Yield |
---|---|
With (2-(4-methoxyphenyl)ethene-1,1-diyl)bis(diphenylphosphane); bis(1,5-cyclooctadiene)iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate In 1,4-dioxane; toluene at 160℃; for 72h; Molecular sieve; Glovebox; Sealed tube; regioselective reaction; | A 70% B n/a |
Conditions | Yield |
---|---|
With H2Ru4(CO)12 In benzene at 25℃; for 7h; Product distribution; Quantum yield; Irradiation; further pentenes, other periods of time; | A n/a B n/a C 69% |
With hydrogen; palladium; platinum Mechanism; Product distribution; dependence of product distribution on kind of catalyst; | |
With hydrogen; (CO)12> In dichloromethane at 35℃; under 760 Torr; for 24h; Product distribution; other ruthenium catalysts, other temp., other pressure of H2, various partial pressure of CO, also in the presence of PPh3; | |
With hydrogen; bis(benzonitrile)palladium(II) dichloride In toluene at 25℃; Product distribution; Kinetics; | |
With iron pentacarbonyl; hydrogen Product distribution; Irradiation; var. times; |
sodium tetrahydroborate
1-Bromopentane
tetramethlyammonium chloride
B
pentane
Conditions | Yield |
---|---|
In water; diethylene glycol byproducts: NaBr, H2; NaBH4 in diglyme heated to 105°C, n-amyl bromide added to stirred suspn. over 5 h, suspn. allowed to cool, filtered, solids washed with Et2O, combined solns. evapd. residue dissolved in water and Me4NCl added; ppt. filtered and recrystd. from acetone/water; | A 67% B n/a |
1-methylbuta-1,3-diene
A
(Z)-pent-2-ene
B
(E)-pent-2-ene
C
1-penten
D
pentane
Conditions | Yield |
---|---|
With hydrogen; palladium dichloride In N,N-dimethyl-formamide under 18751.5 Torr; for 0.116667h; Product distribution; Ambient temperature; various time; | A 11.7% B 62.1% C 15.3% D 1.2% |
With hydrogen; complex 1 under 684 Torr; for 6h; Product distribution; Variation of complex catalysts, time.; | |
With hydrogen; Pd-containing polymer In methanol at 20℃; Product distribution; catalytic properties of palladium fixed on poly(m- and p-)hydroxyphenylbenzoxazoleterephthalamides, hydrogenation and isomerization of olefins; | |
With hydrogen; <2> In dichloromethane for 5h; Product distribution; other alkene; |
2-bromopentane
octylmagnesium bromide
A
4-methyldodecane
B
pentane
C
2-pentene
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; cobalt(II) chloride; lithium iodide In tetrahydrofuran at 10℃; for 1h; Inert atmosphere; chemoselective reaction; | A 62% B n/a C n/a |
Conditions | Yield |
---|---|
silica/alumina-supp. -O-W[(C-tBu)(-CH2-tBu)2] at 150℃; under 600 Torr; for 120h; Product distribution; Further Variations:; Catalysts; | A 61.7% B 3.4% C 25.7% D 5.5% |
tetrachloromethane
ethylmagnesium chloride
A
3-ethylpentane
B
pentane
Conditions | Yield |
---|---|
With C31H37ClN3NiO2(1-)*Li(1+) In tetrahydrofuran at 25℃; for 0.333333h; Inert atmosphere; Overall yield = 100 %; | A 42.8% B 57.2% |
dichloromethane
ethylmagnesium chloride
A
propene
B
n-butane
C
pentane
Conditions | Yield |
---|---|
With C31H37ClN3NiO2(1-)*Li(1+) In tetrahydrofuran at 25℃; for 0.333333h; Inert atmosphere; Overall yield = 91 %; | A 14% B 20% C 57% |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; iodine | 100% |
HOC6H3ClCH2N(CH3)C2H4N(CH3)CH2C6H2(C(CH3)3)2OH
pentane
Conditions | Yield |
---|---|
In diethyl ether byproducts: (CH3)3COH; (N2); glovebox; soln. of ligand in ether was added to soln. of Zr complex in ether; stirred at room temp. for 2 h; solvent removed (vac.); washed (pentane); solvent removed (vac.); elem. anal.; | 100% |
HOC6H2Cl2CH2N(CH3)C2H4N(CH3)CH2C6H2(C10H15)(CH3)OH
pentane
Conditions | Yield |
---|---|
In diethyl ether byproducts: (CH3)3COH; (N2); glovebox; soln. of ligand in ether was added to soln. of Zr complex in ether; stirred at room temp. for 2 h; solvent removed (vac.); washed (pentane); solvent removed (vac.); elem. anal.; | 100% |
N,N-bis(3,4-dimethyl-2-hydroxybenzyl)-N',N'-dimethylethylenediamine
C14H6(C4H9)4H2NC3H7O2Ti(OC3H7)2
pentane
Conditions | Yield |
---|---|
In diethyl ether the mixt. in ether was stirred for 2 h at room temp. under N2; volatiles were removed under reduced pressure; elem. anal.; | 99% |
HOC6H2Br2CH2N(CH3)C2H4N(CH3)CH2C6H2(C(CH3)3)2OH
pentane
Conditions | Yield |
---|---|
In diethyl ether byproducts: (CH3)3COH; (N2); glovebox; soln. of ligand in ether was added to soln. of Zr complex in ether; stirred at room temp. for 2 h; solvent removed (vac.); washed (pentane); solvent removed (vac.); elem. anal.; | 99% |
HOC6H2I2CH2N(CH3)C2H4N(CH3)CH2C6H2(C10H15)(CH3)OH
pentane
Conditions | Yield |
---|---|
In diethyl ether byproducts: (CH3)3COH; (N2); glovebox; soln. of ligand in ether was added to soln. of Zr complex in ether; stirred at room temp. for 2 h; solvent removed (vac.); washed (pentane); solvent removed (vac.); elem. anal.; | 99% |
[(dimethyl-bis(4-tert-butyl-2-pyridyl)borate)Pt(CH3)2]Na
water
pentane
[(dimethyl-bis(4-tert-butyl-2-pyridyl)borate)PtH(1-pentene)]
Conditions | Yield |
---|---|
In not given byproducts: NaOH; 3 equiv. H2O, room temp., 5 min; | 99% |
niobium pentachloride
pentane
benzene
A
4,4'-bis[P-(chlorogold(I))diphenylphosphino]biphenyl
Conditions | Yield |
---|---|
In tetrahydrofuran under N2; soln. of Au complex in THF added to solid NbCl5; stirred at room temp. overnight; volatiles removed in vac.; dissolved in benzene; centrifuged; decanted; concd. in vac.; crystd. from benzene-pentane; elem. anal.; | A 99% B 76% |
Conditions | Yield |
---|---|
In pentane (N2) to soln. Cr-Ge complex in pentane TMEDA was added at room temp., stored at 6°C overnight; | 99% |
Conditions | Yield |
---|---|
In pentane (N2) to soln. Mo-Ge complex in pentane TMEDA was added at room temp., stored at 6°C overnight; | 99% |
Conditions | Yield |
---|---|
at -80 - -30℃; for 72h; Inert atmosphere; Schlenk technique; | 99% |
2,2,2-trichloroethyl 2-(4-bromophenyl)-2-diazoacetate
pentane
Conditions | Yield |
---|---|
With Rh2[R-3,5-di(p-tBuC6H4)-triphenylcyclopropanecarboxylate]4 Reagent/catalyst; Reflux; stereoselective reaction; | 99% |
perfluorophenyl azide
trityl tetrafluoroborate
tris-(o-tolyl)phosphine
pentane
Conditions | Yield |
---|---|
Stage #1: perfluorophenyl azide; trityl tetrafluoroborate; tris-(o-tolyl)phosphine In dichloromethane at 20℃; for 12h; Inert atmosphere; Schlenk technique; Glovebox; Stage #2: pentane | 99% |
Conditions | Yield |
---|---|
With hydrogen under 15001.5 Torr; Catalytic behavior; Reagent/catalyst; Temperature; chemoselective reaction; | 98.5% |
With hydrogen at 250℃; under 760.051 Torr; Reagent/catalyst; Temperature; | 73.2% |
With hydrogen; Pd3(PW12O40)2 at 179.9℃; | 39.5% |
Conditions | Yield |
---|---|
In pentane Ar; U compd. and ligand (1:1 molar ratio), stirred for 12 at 20°C; filtered, evapd., elem. anal.; | 98% |
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
pentane
Conditions | Yield |
---|---|
Stage #1: bis[2-(trifluoromethyl)propyl]-2,2'-bipyridine-3,3'-dicarboxylate; C18H8Cl2F12N2O4Pd; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In dichloromethane at 45℃; for 3h; Stage #2: pentane | 98% |
tetrahydrofuran
methylmagnesium chloride
pentane
Mg2(μ-Cl)2(tetrahydrofuran)[Ph(pyrazol-1-yl)B(μ-N(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]2*pentane
Conditions | Yield |
---|---|
In tetrahydrofuran under N2 atm. using Schlenk techniques; stirred soln. of borate ligand in THF was treated at -78°C with soln. of MeMgCl in THF; mixt. allowed to warm to room temp.; stirred overnight; soln. concd. (vac.); layered with pentane; crystals are formed; mother liq. decanted; dried (vac.); | A 97% B n/a |
1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene
pentane
Conditions | Yield |
---|---|
In chloroform byproducts: CH3CN; (Ar); exclusion of direct daylight; soln. of Fe complex (2 equiv.) in CHCl3 was added to Pd complex (1 equiv.); stirred at room temp. for 1 h; poured into pentane; kept at -18°C overnight; filtered; washed (pentane); dried (vac.); elem. anal.; | 97% |
N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine
pentane
Conditions | Yield |
---|---|
Stage #1: N,N'-bis(2-hydroxy-3,5-di tertiarybutylbenzyl)homopiperazine With n-butyllithium In tetrahydrofuran at 20℃; for 72h; Inert atmosphere; Schlenk technique; Stage #2: pentane Inert atmosphere; Schlenk technique; | 97% |
1,4-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)-1,4-diazacycloheptane
pentane
Conditions | Yield |
---|---|
Stage #1: 1,4-bis(3-tert-butyl-5-methyl-2-hydroxybenzyl)-1,4-diazacycloheptane With n-butyllithium In tetrahydrofuran at 20℃; for 72h; Inert atmosphere; Schlenk technique; Stage #2: pentane Inert atmosphere; Schlenk technique; | 97% |
Conditions | Yield |
---|---|
Stage #1: C84H84CeLi3O12 With trityl chloride In tetrahydrofuran at 20℃; for 2h; Stage #2: pentane | 97% |
2-(3-bromopropyl)isoindole-1,3-dione
1-lithio-2-tert-butyldimethylsilyl-1,2-dicarba-closo-dodecaborane(12)
pentane
Conditions | Yield |
---|---|
In diethyl ether; benzene cooled soln. (0°C) of B compd. in benzene-Et2O treated dropwise with benzene-Et2O soln. of C6H4(CO)2N(CH2)3Br (molar ratio 1:1.08); warmed to room temp.; gradually brought to reflux; refluxed for 2 d; solvent removed on rotary evaporator; treated with MeOH; cooled (-10°C) overnight; filtered; solid washed with chilled MeOH; dried in vac.; purified by slow evapn. of pentane-Et2O soln.; elem. anal.; | 95% |
n-propylamino-N,N-bis(2-methylene-4,6-di-tert-butylphenol)
[Ti(OCH(CH3)2)2N(CH3)2C2H4N(OC6H2(CH3)2CH2)2]
pentane
Conditions | Yield |
---|---|
In toluene 2 h at 110°C in toluene in a sealed tube; | 95% |
Conditions | Yield |
---|---|
With H2O2 In chloroform under N2 or in vac.; a soln. of H2O2 (0.238 mmol) was added dropwise to a soln. of Ru-contg. compd. (0.198 mmol) in chloroform; the mixt. was stirred at room temp. for 12 h before it was filtered; the filtrate was evapd. to dryness in vac.; the residue was washed with diethyl ether and crystd. in a chloroform-pentane mixt.; elem. anal.; (31)P NMR spectra monitoring; | 95% |
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