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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryShanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
Conditions | Yield |
---|---|
With 2-(trimethylsilyl)prop-2-enylzinc chloride; bis(acetylacetonate)nickel(II) In diethyl ether 1.) -15 deg C, 0.5 h, 2.) r.t., 18 h; | 100% |
With titanium(IV) tetraethanolate | 94% |
With [Mg0833Al0.167(OH)2](C(00)O3)84*0.64H2O In acetonitrile at 239.84℃; Reagent/catalyst; Aldol Condensation; Inert atmosphere; | 13.4% |
(+/-)-2-pentanol
cyclohexanone
A
2-cyclohexylidenecyclohexanone
C
cyclohexanol
Conditions | Yield |
---|---|
With magnesium oxide for 6h; Reactivity; Temperature; Reagent/catalyst; Time; Meerwein-Ponndorf-Verley reduction; Inert atmosphere; Heating; | A n/a B n/a C 79% |
cyclohexanone
4-aza-9-diazo-9H-fluorene
A
2-cyclohexylidenecyclohexanone
B
2'-oxospiro<4-azafluorene-9',1-cyclopropane>
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 0℃; for 3h; Product distribution; or cyclopentanone; | A 0.4 g B 73% |
With boron trifluoride diethyl etherate at 0℃; for 3h; | A 0.4 g B 73% |
cyclohexanone
(dichloroalumino)(trichlorotitanio)methane
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
In toluene at 25℃; for 3h; | 60% |
cyclohexanone
cyclohexylamine
A
2-cyclohexylidenecyclohexanone
B
cyclohexanone-2-propionitrile
Conditions | Yield |
---|---|
With acetic acid; acrylonitrile; hydroquinone for 16h; Heating; | A 15% B 42% |
cyclohexanone
acrylonitrile
A
2-cyclohexylidenecyclohexanone
B
cyclohexanone-2-propionitrile
Conditions | Yield |
---|---|
With cyclohexylamine; acetic acid; hydroquinone for 16h; Heating; | A 15% B 42% |
cyclohexanone
A
2-(1-cyclohexenyl)cyclohexanone
B
2-cyclohexylidenecyclohexanone
C
2-cyclohexylidene-6-(1-cyclohexen-1-yl)cyclohexan-1-one
D
2(R*),6(S*)-di(1-cyclohexen-1-yl)cyclohexanone
Conditions | Yield |
---|---|
With potassium hydroxide In toluene at 190℃; for 6.5h; Further byproducts given; | A n/a B n/a C n/a D 33% |
cyclohexanone
1,1,1,3,3,3-hexamethyl-disilazane
A
2-cyclohexylidenecyclohexanone
B
1-(Trimethylsilyloxy)cyclohexene
C
N-Cyclohexenylcyclohexanimine
Conditions | Yield |
---|---|
dicobalt octacarbonyl at 110℃; for 6h; | A n/a B n/a C 32% |
cyclohexanone
acetonitrile
A
2-cyclohexylidenecyclohexanone
B
2-cyclohexylideneacetonitrile
Conditions | Yield |
---|---|
With [Mg0751Al0.249(OH)2](C(01)O3)25*0.71H2O at 239.84℃; Inert atmosphere; | A 11.2% B 8.4% |
cyclohexanone
tert-butyldimethylsilyl chloride
A
2-cyclohexylidenecyclohexanone
B
tert-butyl(cyclohex-1-en-1-yloxy)dimethylsilane
Conditions | Yield |
---|---|
Stage #1: cyclohexanone; tert-butyldimethylsilyl chloride With triethylamine for 1h; Inert atmosphere; Stage #2: With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 3h; Inert atmosphere; | A n/a B 11% |
1-iodo-3,4-dimethoxybenzene
A
2-cyclohexylidenecyclohexanone
B
1-(3,4-dimethoxyphenyl)cyclohexan-1-ol
Conditions | Yield |
---|---|
With diethyl ether; phenyllithium anschl. mit Cyclohexanon; |
2-(1'-chlorocyclohexyl)cyclohexanone
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With sodium methylate |
1-acetoxy-6-bromo-cyclohexene
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With iodine; butyraldehyde; zinc In tetrahydrofuran |
1'-hydroxy-bicyclohexyl-2-one
A
2-(1-cyclohexenyl)cyclohexanone
B
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With potassium hydroxide In butan-1-ol at 30℃; Equilibrium constant; |
1'-Brom<1,1'-bicyclohexyl>-2-on
A
2-(1-cyclohexenyl)cyclohexanone
B
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With triethylamine In ethanol; water at 80℃; for 1h; Yield given. Yields of byproduct given; |
dimethyl N-(ethoxycarbonylmethyl)iminodithiocarbonate
cyclohexanone
A
2-cyclohexylidenecyclohexanone
B
S-methyl N-thiocarbamate
C
ethyl N-carbamate
Conditions | Yield |
---|---|
With potassium tert-butylate 1) THF, -78 deg C, 0,5 h, 2) THF, 0 deg C, 0,5 h; Yield given. Multistep reaction. Yields of byproduct given; | |
With sodium hydride 1) THF, -78 deg C, 0,5 h, 2) THF, -78 deg C, 0,5 h; 20 deg C, 1,5 h; Yield given. Multistep reaction. Yields of byproduct given; |
cyclohexanone
A
hexahydro-2H-oxepin-2-one
B
Adipic acid
C
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With Rh(CO)16; oxygen |
cyclohexanone
A
2-(1-cyclohexenyl)cyclohexanone
B
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With aluminum oxide; iron(III) oxide In decalin at 210℃; under 4500.4 Torr; Rate constant; different activity of Al2O3 and Fe2O3; | |
With 2,2-diphenyl-1-picrylhydrazyl; t-butylnitrite In tetrachloromethane at 79.9℃; for 1h; Rate constant; Mechanism; Product distribution; var. solvents; | |
In tetrachloromethane at 79.9℃; Yield given; |
cyclohexanone
A
2-cyclohexylidenecyclohexanone
B
bis(trimethylsilyl)methane
Conditions | Yield |
---|---|
With bis(trimethylsilyl)dilithiomethane In tetrahydrofuran at -80℃; Yields of byproduct given; |
Conditions | Yield |
---|---|
With PPA |
Conditions | Yield |
---|---|
With sodium hydroxide; potassium carbonate 1) heating, 2) drying; Yield given. Multistep reaction; |
1-oxa-4-azaspiro[4.5]decane
A
cyclohexyl(2-(hydroxy)ethyl)amine
B
2-cyclohexylidenecyclohexanone
C
1-(2-hydroxyethyl)-4,5,6,7-tetrahydro-1H-indole
Conditions | Yield |
---|---|
With PPA for 10h; Heating; | A 1.4 g B 3.04 g C 1.72 g |
sulfuric acid
1,1'-bicyclohexenyl peroxide
2-cyclohexylidenecyclohexanone
cyclohexanone
A
2-(1-cyclohexenyl)cyclohexanone
B
2-cyclohexylidenecyclohexanone
C
2,2-(Dimethylpropyliden)cyclohexan
D
1-neopentylcyclohexanol
Conditions | Yield |
---|---|
at -20℃; for 1h; |
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With diethyl ether; sodium methylate |
A
2-cyclohexylidenecyclohexanone
B
1-(3,4-dimethoxyphenyl)cyclohexan-1-ol
Conditions | Yield |
---|---|
With cyclohexanone |
cyclohexanone
A
2-(1-cyclohexenyl)cyclohexanone
B
2-cyclohexylidenecyclohexanone
C
2,6-dicyclohexylidenecyclohexanone
D
2(R*),6(S*)-di(1-cyclohexen-1-yl)cyclohexanone
Conditions | Yield |
---|---|
With potassium hydroxide; air at 137℃; for 1.33333h; Product distribution; Further Variations:; Temperatures; time dependence; aldol condensation; |
Conditions | Yield |
---|---|
[ReH4(η2-H2)(Cyttp)]OTf at 60℃; for 15h; Product distribution; Further Variations:; Catalysts; Solvents; Temperatures; |
cyclohexanone
A
hexahydro-2H-oxepin-2-one
B
2-cyclohexylidenecyclohexanone
Conditions | Yield |
---|---|
With oxone; silica gel In carbon dioxide at 40℃; under 187515 Torr; Baeyer-Villiger oxidation; |
2-cyclohexylidenecyclohexanone
methyl iodide
2-methyl-2-(cyclohexen-1'-yl)-cyclohexanone
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol for 6h; Ambient temperature; | 85% |
guanazole
2-cyclohexylidenecyclohexanone
2'-amino-5',6',7',8'-tetrahydro-4'H-spiro[cyclohexane-1,9'-[1,2,4]triazolo[5,1-b]quinazoline]
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 2h; Reflux; | 82% |
In N,N-dimethyl-formamide Heating; | 61% |
5-amino-1,2,3-triazole-4-carboxamide
2-cyclohexylidenecyclohexanone
5,6,7,8-tetrahydro-4H-spiro{[1,2,3]triazolo[5,1-b]quinazoline-9,1'-cyclohexane}-3-carboxamide
Conditions | Yield |
---|---|
In methanol at 120℃; for 0.333333h; Microwave irradiation; | 81% |
2-cyclohexylidenecyclohexanone
3-SMe-1,2,4-triazin-5(4H)-one
3-(methylthio)-7,8,9,10,12,13,14,15,15a,15b-decahydro-1H-benzo[c][1,2,4]triazino[1,6-a]azecine-1,6(2H)-dione
Conditions | Yield |
---|---|
With trifluoroacetic acid In N,N-dimethyl-formamide at 20℃; for 120h; | 70% |
Conditions | Yield |
---|---|
67.7% |
2-cyclohexylidenecyclohexanone
3-p-tolyl-7,8,9,10,12,13,14,15,15a,15b-decahydro-1Hbenzo[c][1,2,4]triazino[1,6-a]azecine-1,6(2H)-dione
Conditions | Yield |
---|---|
With trifluoroacetic acid In N,N-dimethyl-formamide at 20℃; for 120h; | 67% |
3(5)-amino-1,2,4-triazole
2-cyclohexylidenecyclohexanone
5',6',7',8'-tetrahydro-4'H-spiro[cyclohexane-1,9'-[1,2,4]-triazolo[5,1-b]quinazoline]
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide Heating; | 66% |
2-cyclohexylidenecyclohexanone
1-(2-methoxyvinyl)benzene
A
Adipic acid
B
benzaldehyde
Conditions | Yield |
---|---|
With ozone In diethyl ether at -70℃; | A 8% B 65% |
2-cyclohexylidenecyclohexanone
3-phenyl-1H-1,2,4-triazol-5-amine
2'-phenyl-5',6',7',8'-tetrahydro-4'H-spiro[cyclohexane-1,9'-[1,2,4]triazolo[5,1-b]quinazoline]
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 2h; Reflux; | 60% |
(5-amino-1H-1,2,4-triazol-3-yl)(morpholino)methanone
2-cyclohexylidenecyclohexanone
2'-(morpholin-4-ylcarbonyl)-5',6',7',8'-tetrahydro-4'H-spiro[cyclohexane-1,9'-[1,2,4]triazolo[5,1-b]quinazoline]
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 2h; Reflux; | 58% |
3-phenyl-1,2,4-triazin-5(2H)-one
2-cyclohexylidenecyclohexanone
3-phenyl-7,8,9,10,12,13,14,15,15a,15b-decahydro-1Hbenzo[c][1,2,4]triazino[1,6-a]azecine-1,6(2H)-dione
Conditions | Yield |
---|---|
With trifluoroacetic acid In N,N-dimethyl-formamide at 20℃; for 120h; | 58% |
2-cyclohexylidenecyclohexanone
3-amino-1,2,4-triazole
5',6',7',8'-tetrahydro-4'H-spiro[cyclohexane-1,9'-[1,2,4]-triazolo[5,1-b]quinazoline]
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 2h; Reflux; | 56% |
2-cyclohexylidenecyclohexanone
3-benzyl-1,2,4-triazin-5(4H)one
3-benzyl-7,8,9,10,12,13,14,15,15a,15b-decahydro-1Hbenzo[c][1,2,4]triazino[1,6-a]azecine-1,6(2H)-dione
Conditions | Yield |
---|---|
With trifluoroacetic acid In N,N-dimethyl-formamide at 20℃; for 120h; | 52% |
4-Phenyl-1,2,4-triazolidine-3,5-dione
2-cyclohexylidenecyclohexanone
1-(2-Oxo-bicyclohexyl-1'-en-1-yl)-4-phenyl-[1,2,4]triazolidine-3,5-dione
Conditions | Yield |
---|---|
In ethyl acetate at 3℃; | 50% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 0.5h; Heating; | 49% |
2-cyclohexylidenecyclohexanone
Phenyl vinyl sulfoxide
B
2-cyclohex-1-enyl-2-(2-phenylsulphinylethyl)cyclohexanone
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol 1.) 30 m, reflux, 2.) reflux, overnight; | A n/a B 37% |
2-cyclohexylidenecyclohexanone
malononitrile
9-amino-10-cyano-1,2,3,4,5,6,7,8-octahydrophenanthrene
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid In toluene for 5h; Heating; | 28.5% |
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