Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiry1 high purity 2 able to provide COA/HNMR/HPLC 3 High quality 4 low price 5 Best service Appearance:white powder Storage:Refrigerator, Under Inert Atmosphere Package:bag/bottle/drum Application:pharmaceutical intermediate Transportation:common
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
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inquiry3,5-Dimethoxyaniline Basic information Product Name: 3,5-Dimethoxyaniline Synonyms: BENZENAMINE, 3,5-DIMETHOXY-;3,5-DIMETHOXYANILINE;3,5-DIMETHOXYPHENYLAMINE;5-AMINORESORCINOL DIMETHYL E
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:10272-07-8
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inquiryProduct Name: 3,5-Dimethoxyaniline Synonyms: BENZENAMINE, 3,5-DIMETHOXY-;3,5-DIMETHOXYANILINE;3,5-DIMETHOXYPHENYLAMINE;5-AMINORESORCINOL DIMETHYL ESTER;5-AMINORESORCINOL DIMETHYL ETHER;AKOS 91392;3,5-di
Appearance:White crystal or Colorless liquid Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
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inquiry3,5-Dimethoxyaniline CAS:10272-07-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:10272-07-8
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Cas:10272-07-8
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:10272-07-8
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Our Advantages Production: Advanced chemical equipment with years of experience Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Specif
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
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Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:10272-07-8
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Cas:10272-07-8
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inquiry1-azido-3,5-dimethoxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With sodium tetrahydroborate; palladium In water for 1.5h; Inert atmosphere; | 99% |
With sodium sulfide; water for 0.5h; Reflux; | 96% |
With ammonium hydroxide at 90℃; for 0.5h; | 90% |
With triethylamine; tris[tert-butyl]phosphonium tetrafluoroborate In tetrahydrofuran; water at 20℃; for 15h; Staudinger Azide Reduction; | 94 %Spectr. |
N-(3,5-dimethoxyphenyl)-2,2,2-trifluoroacetamide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With water; potassium carbonate In methanol for 20h; Ambient temperature; | 94% |
2-Trimethylsilanyl-ethanesulfonic acid (3,5-dimethoxy-phenyl)-amide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With cesium fluoride In N,N-dimethyl-formamide at 95℃; for 40h; | 93% |
1-chloro-3,5-dimethoxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With ammonium hydroxide; potassium phosphate In dimethyl sulfoxide at 80℃; UV-irradiation; | 93% |
With ammonium hydroxide; potassium phosphate; copper(l) iodide; N1,N2-bis(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide In water; dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere; | 88% |
With ammonium hydroxide; potassium phosphate; copper(l) iodide; N1,N2-bis(5-methyl-[1,1'-biphenyl]-2-yl)oxalamide In dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; Schlenk technique; | 88% |
N-(3,5-dimethoxy-phenyl)-acetamide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: N-(3,5-dimethoxy-phenyl)-acetamide With Schwartz's reagent In tetrahydrofuran at 20℃; for 0.05h; Inert atmosphere; Stage #2: With water In tetrahydrofuran Inert atmosphere; chemoselective reaction; | 86% |
With alkaline solution |
3,5-dimethoxyphenylboronic acid
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With sodium hydroxide; hydroxylamine-O-sulfonic acid In acetonitrile at 20℃; for 16h; | 82% |
1-bromo-3,5-dimethoxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3,5-dimethoxybenzene With magnesium In tetrahydrofuran Inert atmosphere; Stage #2: With C10H17NO In tetrahydrofuran; toluene at -78℃; for 2h; Inert atmosphere; Stage #3: With ammonium chloride In tetrahydrofuran; water; toluene Inert atmosphere; | 78% |
With ammonium hydroxide; copper(l) iodide; N,N'-bis(3,5-dimethoxyphenyl)cyclopentane-1,1-dicarboxamide; caesium carbonate In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; Sealed tube; | 68% |
With ammonia; sodium; ferric nitrate |
1-iodo-3,5-dimethoxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With ammonium hydroxide; copper(l) iodide; N,N'-bis(3,5-dimethoxyphenyl)cyclopentane-1,1-dicarboxamide; caesium carbonate In dimethyl sulfoxide at 20℃; for 24h; Inert atmosphere; Sealed tube; | 75% |
3,5-dimethoxyphenol
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 3,5-dimethoxyphenol With Nonafluorobutanesulfonyl fluoride; tris(trimethylsilyl)amine; potassium hexamethylsilazane In tetrahydrofuran at 60℃; for 5h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water at 20℃; for 0.0833333h; pH=3 - 4; Reagent/catalyst; Solvent; | 75% |
3,5-dimethoxybenzoic acid
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 3,5-dimethoxybenzoic acid With diphenylphosphoranyl azide; triethylamine In toluene at 80℃; Stage #2: With sodium hydroxide In tetrahydrofuran; toluene at 20℃; for 2h; | 43% |
Stage #1: 3,5-dimethoxybenzoic acid With diphenylphosphoranyl azide; triethylamine In toluene at 80℃; Stage #2: With sodium hydroxide In tetrahydrofuran for 2h; | 43% |
N-hydroxy-3,5-dimethoxybenzamide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: N-hydroxy-3,5-dimethoxybenzamide With acetic anhydride; potassium carbonate In dimethyl sulfoxide at 50℃; for 2h; Lossen Rearrangement; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide at 0℃; | 3% |
Stage #1: N-hydroxy-3,5-dimethoxybenzamide With potassium carbonate In dimethyl sulfoxide at 90℃; for 3h; Lossen Rearrangement; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide at 20℃; for 0.0833333h; |
1-Bromo-2,4-dimethoxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With ammonia; sodium amide in fluessiges NH3; |
1,3-dimethoxy-5-nitrobenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With hydrogenchloride; tin | |
With hydrogenchloride; tin; tin(ll) chloride at 40℃; Reagens 5: Essigsaeure; | |
With ethanol; nickel Hydrogenation; | |
With hydrogen; palladium on activated charcoal In ethyl acetate |
3,5-dimethoxybenzamide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With sodium hypobromide at -15℃; | |
Yield given; | |
With sodium hypochlorite; sodium hydroxide at 80℃; for 5h; | 4.1 g |
ethyl 3,5-dimethoxybenzoate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme |
3,5-Dihydroxybenzoic acid
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 84 percent / sodium hydroxide / heating View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium carbonate / acetone / 55 °C 2.1: triethylamine; diphenylphosphoranyl azide / toluene / 80 °C 2.2: 2 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium carbonate / acetone / 55 °C 2.1: triethylamine; diphenylphosphoranyl azide / toluene / 80 °C 2.2: 2 h View Scheme |
azido(3,5-dimethoxyphenyl)methanone
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: CH2Cl2 / 60 h / Heating 2: 94 percent / H2O, K2CO3 / methanol / 20 h / Ambient temperature View Scheme |
3,5-dimethoxy-benzoic acid hydrazide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme |
3,5-dimethoxybenzoyl chloride
3,5-Dimethoxyaniline
3,5-dimethoxyphenyl isocyanate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 8.7 g / sodium hydroxide (20percent) / 60 °C View Scheme | |
With benzoic acid; sodium hydroxide In tetrahydrofuran at 20℃; for 0.5h; Curtius Rearrangement; |
3,5-dihydroxyphenylamine
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous dioxane 2: aqueous NaOH 3: aq.-ethanolic alkaline solution View Scheme |
N-(3,5-dihydroxyphenyl)acetamide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous NaOH 2: aq.-ethanolic alkaline solution View Scheme |
methyl 3,5-dimethoxybenzoate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: liquid ammonia 2: aqueous sodium hypobromite / -15 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C 2: triethylamine; diphenyl phosphoryl azide / 80 °C 3: sodium hydroxide; benzoic acid / tetrahydrofuran / 0.5 h / 20 °C View Scheme |
3,5-dimethoxyphenol
2,3-dimethoxyphenol
diethylazodicarboxylate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With triphenylphosphine In tetrahydrofuran |
1-carbomethoxy-3,5-dihydroxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: potassium carbonate / acetonitrile / 20 °C 2: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C 3: triethylamine; diphenyl phosphoryl azide / 80 °C 4: sodium hydroxide; benzoic acid / tetrahydrofuran / 0.5 h / 20 °C View Scheme |
1-chloro-3,5-dimethoxybenzene
A
bis(3,5-dimethoxyphenyl)amine
B
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 50℃; for 24h; Inert atmosphere; Overall yield = 81 %; |
Conditions | Yield |
---|---|
With phosphoric acid; ammonia In ethylene glycol at 145℃; for 5h; | A 95 %Spectr. B 84 %Spectr. |
di-tert-butyl dicarbonate
3,5-Dimethoxyaniline
(3,5-dimethoxyphenyl)-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; Inert atmosphere; | 100% |
Stage #1: 3.5-dimethoxyaniline With triethylamine In dichloromethane at 20℃; Stage #2: di-tert-butyl dicarbonate In dichloromethane at 20℃; | 99% |
at 90℃; for 3h; | 98% |
methyl chloroformate
3,5-Dimethoxyaniline
methyl N-(3,5-dimethoxyphenyl)carbamate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; | 100% |
With pyridine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; | 94% |
In toluene for 2h; Acylation; Heating; | 81% |
4-((6,7-dimethoxyquinolin-4-yl)oxy)aniline
bis(trichloromethyl) carbonate
sodium hydrogencarbonate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With triethylamine In toluene | 100% |
3,5-Dimethoxyaniline
Methacryloyl chloride
N-(3,5-dimethoxyphenyl)-2-methylacrylamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 100% |
In dichloromethane at 0 - 20℃; | |
In dichloromethane at 0 - 20℃; | |
In dichloromethane at 0 - 20℃; | |
With dmap; triethylamine In dichloromethane at 0 - 20℃; |
2-Bromoacetyl bromide
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 1.25h; Inert atmosphere; | 100% |
at -77℃; |
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In tetrahydrofuran at 20℃; Inert atmosphere; | 99.9% |
1,1,1-trifluoro-4-phenylbut-3-yn-2-one
3,5-Dimethoxyaniline
(Z)-4-(3,5-Dimethoxy-phenylamino)-1,1,1-trifluoro-4-phenyl-but-3-en-2-one
Conditions | Yield |
---|---|
In methanol Ambient temperature; | 99% |
2-bromo-4'-fluoroacetophenone
3,5-Dimethoxyaniline
2-[(3,5-dimethoxyphenyl)amino]-1-(4-fluorophenyl)ethanone
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In neat (no solvent) at 20℃; for 2h; | 99% |
With sodium hydrogencarbonate In ethanol for 4h; Heating; |
(Z)-ethyl 3-(methylamino)-3-phenylacrylate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In dichloromethane for 30h; Heating; | 99% |
2-formylphenyl triflate
3,5-Dimethoxyaniline
1,3-dimethoxyacridine
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; XPhos In toluene at 105℃; for 13h; Mechanism; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With acetic acid; zinc at 20 - 60℃; for 2.5h; | 99% |
2-bromo-5-chlorobenzaldehyde
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 3.5-dimethoxyaniline With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In toluene at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-bromo-5-chlorobenzaldehyde In toluene at 80℃; for 12h; Inert atmosphere; | 99% |
2-bromo-5-nitrobenzaldehyde
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 3.5-dimethoxyaniline With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In toluene at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-bromo-5-nitrobenzaldehyde In toluene at 80℃; for 12h; Inert atmosphere; | 99% |
2-bromo-6-fluorobenzaldehyde
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 3.5-dimethoxyaniline With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In toluene at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-bromo-6-fluorobenzaldehyde In toluene at 80℃; for 12h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3.5-dimethoxyaniline With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In toluene at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: ortho-bromobenzaldehyde In toluene at 80℃; for 12h; Reagent/catalyst; Solvent; Inert atmosphere; | 99% |
Stage #1: 3.5-dimethoxyaniline With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate In toluene at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: ortho-bromobenzaldehyde In toluene at 80℃; for 12h; Reagent/catalyst; | 99% |
1-bromo-3,5-dimethoxybenzene
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); sodium t-butanolate In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; Schlenk technique; | 99% |
With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); sodium t-butanolate In tetrahydrofuran at 60℃; for 19h; Inert atmosphere; | 81% |
With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); sodium t-butanolate In tetrahydrofuran at 60℃; Inert atmosphere; | 75% |
3,5-dimethoxyaniline hydrochloride
4,4'-dimethoxybenzoin
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
at 130 - 140℃; for 1h; | 99% |
ethyl 6-iodo-4-oxo-3,4-dihydroquinazoline-2-carboxylate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
Stage #1: 3.5-dimethoxyaniline With trimethylaluminum In n-heptane; 1,2-dichloro-ethane at 0 - 20℃; for 0.5h; Stage #2: ethyl 6-iodo-4-oxo-3,4-dihydroquinazoline-2-carboxylate In n-heptane; 1,2-dichloro-ethane for 2h; Reflux; | 99% |
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In water; toluene for 4h; Reflux; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In isopropyl alcohol at 20 - 90℃; for 16h; Inert atmosphere; | 98.4% |
acetic anhydride
3,5-Dimethoxyaniline
N-(3,5-dimethoxy-phenyl)-acetamide
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; | 98% |
In toluene at 20℃; for 15h; Time; Inert atmosphere; | 98% |
In toluene at 25℃; for 20h; | 97% |
indan-1,2,3-trione hydrate
3,5-Dimethoxyaniline
Conditions | Yield |
---|---|
In acetic acid for 16h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With titanium(IV) isopropylate; MS 4 Angstroem; palladium diacetate; triphenylphosphine In benzene at 80℃; for 3h; Alkylation; N-allylation; | 98% |
para-bromotoluene
3,5-Dimethoxyaniline
N-(4-tolyl)-3,5-dimethoxyaniline
Conditions | Yield |
---|---|
With C60H86O4P2Pd2(2+)*2BF4(1-); sodium t-butanolate In 1,4-dioxane at 80℃; for 1h; | 98% |
With sodium t-butanolate; 1,1'-bis(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)palladium In toluene at 90℃; for 5h; |
3,5-Dimethoxyaniline
trifluoroacetic anhydride
N-(3,5-dimethoxyphenyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; | 98% |
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h; | 98% |
With triethylamine In toluene at 15 - 20℃; for 1.5h; Temperature; Solvent; | 85.4% |
With triethylamine In toluene at 18 - 25℃; for 2h; | |
With triethylamine In dichloromethane at 20℃; for 2.5h; Cooling with ice; |
ethyl trifluoroacetate,
3,5-Dimethoxyaniline
N-(3,5-dimethoxyphenyl)-2,2,2-trifluoroacetamide
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran for 48h; Heating / reflux; | 98% |
With dmap In tetrahydrofuran for 48h; Reflux; | 98% |
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