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Cas:104-12-1
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiry4-Chlorophenyl isocyanate Basic information Product Name: 4-Chlorophenyl isocyanate Synonyms: 1-chloro-4-isocyanato-benzen;1-Chloro-4-isocyanatobenzene;1-Chloro-4-isocyanato-benzene;4-ch
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Cas:104-12-1
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Cas:104-12-1
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam
Cas:104-12-1
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inquiryName: 4-Chlorophenyl isocyanate Synonyms: 4-Chloroisocyanatobenzene; P-Chlorophenyl isocyanate; 1-chloro-4-isocyanatobenzene; 1-chloro-4-nitrosobenzene; 4-Chloronitrosobenzene; 1-Chloro-4-nitrosobenzene; 4-Chloro-1-nitrosobenzene; NSC 202930; p-Chlo
Cas:104-12-1
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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inquiryAppearance:Clear colorless liquid to white solid Storage:ln stock Package:25kg/Barrel;250kg/Barrel Application:Used in organic synthesis, mainly used as intermediates for medicine, pesticides, etc. Transportation:Express/Sea/Air Port:Any port in Chi
Cas:104-12-1
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Cas:104-12-1
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inquiry4-Chlorophenyl isocyanate CAS: 104-12-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:104-12-1
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inquiry4-Chlorophenyl isocyanateAppearance:Colorless to pale yellow Storage:Store in dry, dark and ventilated Package:according to customers' requirements Application:Pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or b
Product name: Chlorophenyl Isocyanate CAS No.:104-12-1 Molecule Formula:C6H4ClNO Molecule Weight:141.56 Purity: 99.0% Package: 200kg/drum Description:Colorless or light yellow liquid Manufacture Standards:Enterprise Standard TEST
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Min.Order:1 Kilogram
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inquiry4-Chlorophenyl isocyanate Basic information Product Name: 4-Chlorophenyl isocyanate Synonyms: 1-chloro-4-isocyanato-benzen;1-Chloro-4-isocyanatobenzene;1-Chloro-4-isocyanato-benzene;4-chloroisocyanatobenzene;4-Chloro-iso-cyanatobenzene;4-Chlor
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Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquirycarbon dioxide
N-p-chlorophenyltriphenylphosphinimine
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In benzene for 2h; Heating; | 97% |
bis(trichloromethyl) carbonate
4-chloro-aniline
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In ethyl acetate at 0 - 5℃; for 3h; Solvent; Cooling with ice; Reflux; | 92% |
In 1,2-dichloro-ethane at 70 - 83℃; | 89.4% |
Stage #1: bis(trichloromethyl) carbonate; 4-chloro-aniline In dichloromethane at 20℃; for 0.5h; Stage #2: With triethylamine In dichloromethane at -35 - 20℃; for 2h; | 84% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 3h; | 77.1% |
A
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
at 550℃; under 0.002 Torr; | A 8% B 77% |
4-chlorobenzoyl azide
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In toluene for 1.5h; Heating; | 75% |
In toluene at 100℃; for 1h; Reflux; | |
Curtius Rearrangement; |
1-methoxy-2-methylprop-1-ene
4-chloro-N-(dimethyl-λ4-sulfanylidene)benzamide
A
4,4-dimethyl-5-methoxy-2-(4-chlorophenyl)-2-oxazoline
B
p-chlorphenylisocyanate
C
4-chlorobenzamide
Conditions | Yield |
---|---|
In benzene at 35℃; for 1h; Mechanism; Product distribution; Irradiation; other temperatures, other solvents, other concentration of reactant; | A 49% B n/a C n/a |
Conditions | Yield |
---|---|
With di(rhodium)tetracarbonyl dichloride; pyridine hydrochloride In chlorobenzene at 185℃; under 38000 Torr; for 1h; | 49% |
bis(tetrahydrofurane)oxovanadium(IV) dichloride; (Bu4N) In 1,2-dichloro-benzene at 120℃; under 750.06 Torr; | 18% |
bis(tetrahydrofurane)oxovanadium(IV) dichloride; (Bu4N) In 1,2-dichloro-benzene at 120℃; under 750.06 Torr; Rate constant; | 18% |
With pyridine; di(rhodium)tetracarbonyl dichloride; pyridine hydrochloride In chlorobenzene at 205℃; under 50 Torr; for 0.666667h; Yield given; |
2-((4-chlorophenyl)-amino)-2-oxoacetic acid
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; silver nitrate; copper(II) sulfate In dichloromethane; water at 40℃; for 3h; | 46% |
With ammonium peroxydisulfate; copper diacetate; silver nitrate In dichloromethane; water at 40℃; for 3h; | 46% |
1-methoxy-2-methylprop-1-ene
3-(4-chlorophenyl)-1,4,2-dioxazol-5-one
A
4,4-dimethyl-5-methoxy-2-(4-chlorophenyl)-2-oxazoline
B
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In dichloromethane Irradiation; | A 9% B 42% |
3-(4-chlorophenyl)-1,4,2-dioxazol-5-one
A
4,4-dimethyl-5-methoxy-2-(4-chlorophenyl)-2-oxazoline
B
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With 1-methoxy-2-methylprop-1-ene In dichloromethane Irradiation; | A 9% B 42% |
A
(Z)-2-butenenitrile
B
crotononitrile
C
(p-chlorophenyl)iminoacetonitrile
D
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
at 720℃; under 0.0015 Torr; regioselective reaction; | A n/a B n/a C 30% D n/a |
Conditions | Yield |
---|---|
With chlorine; 1,1,2,2-tetrachloroethane Erwaermen des Reaktionsprodukts auf 90grad; |
phosgene
4-Ethoxyaniline
A
p-chlorphenylisocyanate
B
4-ethoxyphenyl isocyanate
Conditions | Yield |
---|---|
With 1-Chloronaphthalene at 240℃; |
4-chloro-N-(2,2-diphenylvinylidene)aniline
A
benzophenone
B
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With oxygen; copper dichloride In N,N-dimethyl-formamide; benzene at 28℃; Mechanism; Rate constant; k=6.1E-2 min-3; |
Conditions | Yield |
---|---|
at 180 - 220℃; Thermodynamic data; ΔH; heat of dissociation; |
Conditions | Yield |
---|---|
In 1,4-dioxane Heating; | |
With pyrographite In ethyl acetate Heating; |
3-Methyl-pyrazole-1-carboxylic acid (4-chloro-phenyl)-amide
A
3-Methylpyrazole
B
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With dibutylamine In tetrachloromethane at 40℃; Rate constant; | |
In 1,4-dioxane at 40℃; Rate constant; var. aprotic solvents; |
O-cyclododecyl-N-(4-chlorophenyl)selenocarbamate
A
cis-cyclododecene
B
(E)-Cyclododecen
C
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform-d1 at 80℃; for 4h; Product distribution; rates of olefin at various temperature and time; |
N-(4-chlorophenyl)selenocarbamate of cholestanol
A
5α-cholest-3-ene
B
cholest-2-ene
C
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform-d1 at 80℃; for 4h; Product distribution; rates of olefin formation at various temperature and time; |
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With copper dichloride In tetrahydrofuran for 0.5h; |
N-(4-chlorobenzoyl)-9,10-dihydro-9,10-dimethyl-9,10-epoxyiminoanthracene
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With triphenylphosphine In benzene Heating; | 92 % Chromat. |
(4-chlorophenyl)carbamic chloride
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; toluene for 0.25h; |
chlorine
phenyl isocyanate
bis(diphenyl)urea
A
2,4-dichlorophenyl isocyanate
B
p-chlorphenylisocyanate
C
2,4,6-trichlorophenyl isocyanate
Conditions | Yield |
---|---|
at 120 - 130℃; |
Conditions | Yield |
---|---|
With montmorillonite K-10 In 1,2-dichloro-benzene at 183℃; for 5h; | 99 % Chromat. |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide at 56.84℃; for 4.5h; Photolysis; |
Conditions | Yield |
---|---|
With sodium azide In toluene for 1h; Heating; | |
Multi-step reaction with 2 steps 1: sodium azide / acetone / 0.5 h / 0 °C 2: toluene / 1 h / 100 °C / Reflux View Scheme | |
Stage #1: 4-chloro-benzoyl chloride With sodium azide In water; acetone at 0℃; Curtius Rearrangement; Stage #2: In toluene for 2h; Curtius Rearrangement; Reflux; Inert atmosphere; | 400 mg |
A
p-chlorphenylisocyanate
B
(Benzoylmethylene)triphenylphosphorane
Conditions | Yield |
---|---|
at 385.25 - 424.85℃; Kinetics; |
cyclohexane-1,2-epoxide
p-chlorphenylisocyanate
3-(4-Chloro-phenyl)-hexahydro-benzooxazol-2-one
Conditions | Yield |
---|---|
Ph4SbI-Bu3SnI In benzene at 80℃; for 2h; | 100% |
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In benzene | 100% |
p-chlorphenylisocyanate
6,7-dimethoxy-4-(1-piperazinyl)quinazoline
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; | 100% |
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 4.5h; | 100% |
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate at 80℃; for 16h; | 100% |
2-(adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one
p-chlorphenylisocyanate
N-(4-chlorophenyl)-4,4-dimethyl-3-oxo-2-(adamantan-2-yl)-1,2-diazetidine-1-carboxamide
Conditions | Yield |
---|---|
With triethylamine; dmap In dichloromethane at 20℃; for 1.5h; | 100% |
2-fluoro-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenylamine
p-chlorphenylisocyanate
1-[2-fluoro-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-3-(4-chlorophenyl)-urea
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 23h; Inert atmosphere; | 100% |
p-chlorphenylisocyanate
1-t-Butoxycarbonylpiperazine
tert-butyl 4-(4-chlorophenylcarbamoyl)piperazine-1-carboxylic acid ester
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 3h; | 99.9% |
In dichloromethane at 0 - 20℃; for 1h; | 89% |
In chloroform at 20℃; | |
In dichloromethane at 20℃; for 2h; |
C19H17NO3S
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 25℃; for 0.166667h; diastereoselective reaction; | 99.5% |
Conditions | Yield |
---|---|
In chlorobenzene | 99% |
In toluene at 80℃; for 1h; | 96% |
In water; toluene for 2h; Heating; | 90% |
p-chlorphenylisocyanate
diethylamine
N,N-diethyl-N'-(4-chlorophenyl)urea
Conditions | Yield |
---|---|
With [{Ph2P(Se)NCH2CH2NPPh2(Se)}Ti(NMe2)2] In toluene at 25℃; for 1h; Schlenk technique; Inert atmosphere; Glovebox; | 99% |
With [κ2-{(Ph2P-(=Se))}2NCH2(C5H4N)ZnCl2] In toluene at 25℃; Schlenk technique; Inert atmosphere; | 96% |
In benzene for 0.5h; | 69% |
In ethanol |
p-chlorphenylisocyanate
1,3,5-tris-(4-chloro-phenyl)-[1,3,5]triazinane-2,4,6-trione
Conditions | Yield |
---|---|
With [(CH2)2N[(CH2)3N[(CH2)3NHC(O)]2]2]2-azidophosphine dendrimer at 20℃; for 5h; | 99% |
With 1,3-diisopropyl-3,4,5,6-tetrahydropyrimidin-1-ium-2-carboxylate In tetrahydrofuran at 75℃; for 1h; | 99% |
With C47H79N4Si3Y In tetrahydrofuran at 23℃; for 12h; Glovebox; Schlenk technique; Inert atmosphere; | 99% |
[(2S,3R)-3-(4-Nitro-phenyl)-aziridin-2-yl]-phenyl-methanone
p-chlorphenylisocyanate
1-(4-Chlorphenylcarbamoyl)-2-(4-nitrophenyl)-3-benzoylaziridin
Conditions | Yield |
---|---|
In diethyl ether for 0.333333h; Heating; | 99% |
6-(methylamino)hexanoic acid
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
With sodium hydroxide Ambient temperature; | 99% |
Conditions | Yield |
---|---|
In tetrahydrofuran for 1h; Ambient temperature; | 99% |
2-isopropylidenehydrazino-2,6-dioxo-4,4-dimethylcyclohexyl thioketone
p-chlorphenylisocyanate
5-(4,4-Dimethyl-2,6-dioxo-cyclohexylidene)-2,2-dimethyl-[1,3,4]thiadiazolidine-3-carboxylic acid (4-chloro-phenyl)-amide
Conditions | Yield |
---|---|
In chloroform for 15h; Ambient temperature; | 99% |
p-chlorphenylisocyanate
D-glucosamine hydrochloride
2-<3-(4-chlorophenylureido)>-2-deoxy-α-D-glucopyranose
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In 1,4-dioxane; water for 0.5h; Ambient temperature; | 99% |
p-chlorphenylisocyanate
N-benzylaminomethyl-dimethylphosphine oxide
Conditions | Yield |
---|---|
In dichloromethane | 99% |
6-amino-4H-1-benzopyran-4-one
p-chlorphenylisocyanate
1-(4-chloro-phenyl)-3-(4-oxo-4H-chromen-6-yl)-urea
Conditions | Yield |
---|---|
In toluene at 80℃; for 18h; Heating / reflux; | 99% |
In toluene at 80℃; for 18h; Heating / reflux; | 99% |
p-chlorphenylisocyanate
C5(CH3)5(P(CH3)3)2RuSi(C6H5)2N(ClC6H4)CO(1+)*B(C6F5)4(1-)=[C5(CH3)5(P(CH3)3)2RuSi(C6H5)2N(ClC6H4)CO]B(C6F5)4
Conditions | Yield |
---|---|
In dichloromethane-d2 inert atmosphere; not isolated; | 99% |
5-amino-1,3-dihydro-2H-indol-2-one
p-chlorphenylisocyanate
1-(4-chlorophenyl)-3-(2-oxo-2,3-dihydro-1H-indol-5-yl)-urea
Conditions | Yield |
---|---|
In methanol; dichloromethane at 10 - 20℃; | 99% |
p-chlorphenylisocyanate
diphenylphosphane
N-(4-chlorophenyl)-1,1-diphenylphosphanecarboxamide
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 3h; Schlenk technique; Inert atmosphere; | 99% |
With Zr(tBu-ONNMe2O)Bn2; trityl tetrakis(pentafluorophenyl)borate In chlorobenzene at 60℃; for 24h; Schlenk technique; | 90% |
Stage #1: diphenylphosphane With α-Ln(α-deprotonated dimethylbenzylamine)3 In tetrahydrofuran Schlenk technique; Stage #2: p-chlorphenylisocyanate In tetrahydrofuran at 20℃; for 6h; Schlenk technique; | 83% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 99% |
In dichloromethane for 2h; Reflux; | 72% |
In chloroform at 60℃; for 16h; | 63% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Inert atmosphere; | 99% |
4-amino-3,4-dihydro-2,2-dimethyl-6-ethylsulfonylamino-2H-1-benzopyran
p-chlorphenylisocyanate
N-4-chlorophenyl-N'-(6-ethylsulfonylamino-3,4-dihydro-2,2-dimethyl-2H-1-benzopyran-4-yl)urea
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; Reflux; | 99% |
pyrrolidine
p-chlorphenylisocyanate
N-(4-chlorophenyl)-1-pyrrolidinecarboxamide
Conditions | Yield |
---|---|
With [{Ph2P(Se)NCH2CH2NPPh2(Se)}Ti(NMe2)2] In toluene at 25℃; for 1h; Schlenk technique; Inert atmosphere; Glovebox; | 99% |
With [κ2-{(Ph2P-(=Se))}2NCH2(C5H4N)ZnCl2] In toluene at 25℃; Schlenk technique; Inert atmosphere; | 93% |
With 1,6-anhydro-3,4-dideoxy-β-D-glycero-hexopyranos-2-ulose at 0 - 20℃; for 1h; | 86% |
at 20℃; for 2h; Molecular sieve; Inert atmosphere; |
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; | 99% |
p-chlorphenylisocyanate
N-propanoyl-1,3-thiazolidine-2-thione
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; | 99% |
p-chlorphenylisocyanate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 5h; | 99% |
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