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Cas:10497-05-9
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inquiryProduct description: Product name Tris(trimethylsilyl) phosphate CAS number 10497-05-9 Assay ≥99.5% Appearance Colorless transparent liquid Capacity 500mt/year Application Li
Cas:10497-05-9
Min.Order:100 Gram
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inquiryFactory low price Tris(trimethylsilyl)phosphate Cas 10497-05-9 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediate
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inquirygood quality Appearance:white powder Storage:cold storage Package:meet the demand of customer Application:diagnostic reagent Transportation:by sea or by air Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:10497-05-9
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:10497-05-9
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inquiryDetails hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research
Cas:10497-05-9
Min.Order:20 Kilogram
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Cas:10497-05-9
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inquiryTris(trimethylsilyl)phosphate CAS:10497-05-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
Cas:10497-05-9
Min.Order:1 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:10497-05-9
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:4 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:10497-05-9
Min.Order:10 Gram
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Cas:10497-05-9
Min.Order:1 Gram
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inquiryTianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationships with
Cas:10497-05-9
Min.Order:1 Kilogram
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inquiryProduct name: Tris(Trimethylsilyl)Phosphate CAS No.:10497-05-9 Molecule Formula: C9H27O4PSi3 Molecule Weight:314.53 Purity: 99.0% Package: 25kg/drum Description:Colorless or light yellow liquid Manufacture Standards:Enterprise Standard
Cas:10497-05-9
Min.Order:1 Kilogram
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:10497-05-9
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inquiryTRIS(TRIMETHYLSILYL) PHOSPHATE Basic information Product Name: TRIS(TRIMETHYLSILYL) PHOSPHATE Synonyms: Phosphoric acid, TMS;Phosphoric acid, tristrimethylsilyl;Phosphoric acid, triTMS;Silanol, trimethyl-, phosphate (3:1);Silanol,trimethyl-,ph
Cas:10497-05-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:10497-05-9
Min.Order:0
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Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:10497-05-9
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:10497-05-9
Min.Order:1 bottle
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inquiryIn fluorine chemical, Yuji Tech has been dedicated to R&D of production of ODS alternatives, fluoropolymers and fluorinated fine chemicals for years, and has become an international leading innovation enterprise in fluorine chemical research an
Cas:10497-05-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as: Frac
1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.
hexamethyldisilathiane
A
Tris(trimethylsilyl) phosphate
B
O,O,O-tris(trimethylsilyl) phosphorothioate
Conditions | Yield |
---|---|
With phosphorus pentoxide at 170 - 180℃; for 10h; | A 85% B 98% |
chloro-trimethyl-silane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
In formamide for 1h; Inert atmosphere; Schlenk technique; | 98% |
Hexamethyldisiloxane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
Stage #1: Hexamethyldisiloxane With phosphoric acid at 160 - 170℃; under 4500.45 - 6000.6 Torr; for 5h; Autoclave; Reflux; Stage #2: N-trimethylsilyldihydropyrrole at 100℃; under 760.051 Torr; | 96.52% |
chloro-trimethyl-silane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With potassium dihydrogenphosphate In hexane Reflux; | 96% |
With ammonium dihydrogen phosphate at 78℃; for 3h; Temperature; Reagent/catalyst; Time; | 89.6% |
With phosphoric acid | |
With phosphoric acid Schlenk technique; Inert atmosphere; | |
With phosphoric acid Inert atmosphere; |
Conditions | Yield |
---|---|
With saccharin In acetonitrile for 1h; Heating; | 93% |
N-trimethylsilyl-pyrrolidin-2-one
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With lithium dihydrogenphosphate at 20℃; for 1h; | 86% |
tetrakis(trimethylsiloxy)phosphonium iodide
A
trimethylsilyl iodide
B
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
In benzene Heating; during 5 h the solvent was distilled off, the temp. rose to 110 deg C; | A n/a B 85% |
C22H50O10P2SSi5
A
Tris(trimethylsilyl) phosphate
B
bis(trimethylsilyl) (1,1-dioxido-3Н-2,1-benzoxathiol-3-yl)phosphonate
Conditions | Yield |
---|---|
at 90 - 110℃; under 1 Torr; | A n/a B 52% |
N,O-bis-(trimethylsilyl)-acetamide
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With trichlorophosphate at 120℃; for 1h; | 26% |
tris(trimethylsilyl) phosphite
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With trityl-glycidol at 130 - 150℃; | 24% |
With styrene oxide at 130 - 150℃; |
1,1,1,3,3,3-hexamethyl-disilazane
A
Tris(trimethylsilyl) phosphate
B
Tetrakis(trimethylsilyl) pyrophosphate
C
1,1,3,5,7,7-hexakis(trimethylsilyl) pyrophosphate
Conditions | Yield |
---|---|
With phosphorus pentoxide at 100 - 140℃; for 2h; Further byproducts given; | A 21% B 6% C 3% D 3% |
Methoxytrimethylsilane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With phosphonic Acid; air |
Hexamethyldisiloxane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With phosphorus pentoxide | |
With phosphorus pentoxide durch langsame Destillation; | |
With phosphorus pentoxide In neat (no solvent) very slow distn. of (CH3)3SiOSi(CH3)3 over P2O5;; | |
With P4O10 In neat (no solvent) very slow distn. of (CH3)3SiOSi(CH3)3 over P2O5;; |
phosphoric acid, bis(trimethylsilyl)monomethyl ester
phenylthiotrimethylsilane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With perhydrodibenzo-18-crown-6; potassium thiophenolate In benzene |
phosphoric acid ethyl ester-bis-trimethylsilanyl ester
phenylthiotrimethylsilane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With perhydrodibenzo-18-crown-6; potassium thiophenolate In benzene |
phenylthiotrimethylsilane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With perhydrodibenzo-18-crown-6; potassium thiophenolate In benzene |
trimethylsilyl acetate
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With phosphorus(V) oxybromide at 90℃; for 3h; |
Conditions | Yield |
---|---|
durch langsame Destillation; |
1,1,1,3,3,3-hexamethyl-disilazane
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With ammonium hypophosphite |
bis(trimethylsilyl)phosphonite
allyl-trimethyl-silane
A
bis(trimethylsilyl) phosphonate
B
Tris(trimethylsilyl) phosphate
C
trimethylsilyl [3-(trimethylsilyl)propyl]phosphinate
D
bis(trimethylsilyl) [3-(trimethylsilyl)propyl]phosphonate
E
trimethylsilylhypophosphite
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); water for 7h; Reflux; | A n/a B 0.1 g C 0.45 g D 0.12 g E n/a |
tris(trimethylsilyl) phosphite
A
bis(trimethylsilyl) phosphonate
B
Tris(trimethylsilyl) phosphate
C
Tetrakis(trimethylsilyl) pyrophosphate
D
Trimethylsilyldifluorophosphat
E
bis(trimethylsilyl) phosphorofluoridate
Conditions | Yield |
---|---|
With [1,3]-dioxolan-2-one; lithium hexafluorophosphate; water; Diethyl carbonate In [D3]acetonitrile at 20℃; Glovebox; Inert atmosphere; |
tris(trimethylsilyl) phosphite
A
bis(trimethylsilyl) phosphonate
B
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
With nickel(II) chloride hexahydrate at 160℃; for 42h; Schlenk technique; Inert atmosphere; |
Conditions | Yield |
---|---|
In hexane N2-atmosphere; addn. of soln. of GaMe3 (10% excess) to phosphate ester soln.; concn., crystd. on cooling (-24°C), collection (filtration), drying (vac.); elem. anal.; | 95% |
Tris(trimethylsilyl) phosphate
trimethylsilyl fluoride
Conditions | Yield |
---|---|
With sodium fluoride 150 to 200 deg C; | 91.5% |
Tris(trimethylsilyl) phosphate
(fluoro)bis(cyclopentadienyl)vanadium
tris(pentafluorophenyl)borate
Conditions | Yield |
---|---|
Stage #1: Tris(trimethylsilyl) phosphate; tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 1h; Inert atmosphere; Glovebox; Stage #2: (fluoro)bis(cyclopentadienyl)vanadium In dichloromethane at 20℃; for 24h; Inert atmosphere; Glovebox; | 90% |
Tris(trimethylsilyl) phosphate
trimethylsilylazide
Conditions | Yield |
---|---|
With sodium azide at 150℃; for 0.166667h; | 87% |
Conditions | Yield |
---|---|
With sodium azide at 150℃; for 0.166667h; other substrates, other reagents; | A 87% B n/a |
Conditions | Yield |
---|---|
In hexane N2-atmosphere; addn. of soln. of AlMe3 (10% excess) to phosphate ester soln. at cooling, warming to room temp.; evapn. (vac.); elem. anal.; | 87% |
bis(trimethylsilyl) phosphonate
Tris(trimethylsilyl) phosphate
ethyl N-phenylformimidate
O,O',O'',O'''-tetra(trimethylsilyl) N-anilinomethylenebisphosphonate
Conditions | Yield |
---|---|
With zinc(II) chloride at 150 - 160℃; for 1h; Reflux; | 86% |
18-crown-6 ether
Tris(trimethylsilyl) phosphate
potassium tert-butylate
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 0.166667h; | 85% |
Tris(trimethylsilyl) phosphate
trimethylsilane adduct of trimethylsilylium tetrakis(pentafluorophenyl)borate
Conditions | Yield |
---|---|
In toluene for 1h; Sonication; | 83% |
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
In tetrahydrofuran N2-atmosphere; refluxing for 5 h; elem. anal.; | 82% |
Conditions | Yield |
---|---|
In tetrahydrofuran N2-atmosphere; refluxing for 5 h; evapn., recrystn. (hexane); elem. anal.; | 81% |
Conditions | Yield |
---|---|
In hexane N2-atmosphere; addn. of soln. of AlMe3 (10% excess) to phosphate ester soln. at cooling, warming to room temp.; concn., crystd. on cooling (-24°C), collection (filtration), drying (vac.); elem. anal.; | 74% |
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
In toluene at 20℃; Schlenk technique; Inert atmosphere; | 69% |
Tris(trimethylsilyl) phosphate
titanium tetrachloride
Conditions | Yield |
---|---|
In further solvent(s) boiling gently soln. of OP(OSi(CH3)3)3 (0.51 mmol) and TiCl4 (0.50 mmol) in ClSi(CH3)3; allowing to cool;; pptn.;; | 66% |
In benzene-d6 byproducts: ClSi(CH3)3; briefly heating to boiling in benzene-d6;; not isolated, detected by 1H- and 31P-NMR;; |
Tris(trimethylsilyl) phosphate
Conditions | Yield |
---|---|
In acetonitrile inert atmosphere; crystn. (40-50°C, 4 h, room temp., 2 d); elem. anal.; | 59% |
Tris(trimethylsilyl) phosphate
tert-butylaluminium dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran dropwise addn. of 1 equiv. P-compd. to Al-compd. (stirring), refluxing for 2 h; vol. reduction (vac.), crystn. (-20°C, overnight); elem. anal.; | 56% |
Tris(trimethylsilyl) phosphate
bis(tert-butyl)aluminium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran dropwise addn. of 1 equiv. P-compd. to Al-compd. (stirring), refluxing for 2 h; vol. reduction (vac.), crystn. (-20°C, overnight); elem. anal.; | 56% |
Conditions | Yield |
---|---|
150 to 200 deg C; | 45.5% |
Tris(trimethylsilyl) phosphate
(fluoro)bis(cyclopentadienyl)vanadium
tris(pentafluorophenyl)borate
Conditions | Yield |
---|---|
Stage #1: Tris(trimethylsilyl) phosphate; tris(pentafluorophenyl)borate In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; Glovebox; Stage #2: (fluoro)bis(cyclopentadienyl)vanadium In tetrahydrofuran at 20℃; for 48h; Inert atmosphere; Glovebox; | 43.2% |
tris[μ-[2,6-bis(1-methylethyl)benzenaminato]]trimethyltricycloaluminum
Tris(trimethylsilyl) phosphate
(MeAl)[2,6-(i-Pr)2C6H3N]3(Al[OP(OSiMe3)3])2(O3POSiMe3)
Conditions | Yield |
---|---|
In toluene under N2 atm. OP(OSiMe3)3 was added dropwise to alumazene in toluene andrefluxed for 24 h; react. mixt. was cooled to room temp.; elem. anal.; | 36% |
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