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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Pentadecan-15-olide

Cas:106-02-5

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory price Cosmetic PENTADECALACTONE 106-02-5 Manufacturer

Cas:106-02-5

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

Cyclopentadecanolide

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Cyclopentadecanolide

Cas:106-02-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so

Cyclopentadecanolide-

Cas:106-02-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

106-02-5 Cyclopentadecanolide

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 106-02-5 with best quality

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hot Sell Factory Supply Raw Material Cyclopentadecanolide CAS NO.106-02-5

Cas:106-02-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

Cyclopentadecanolide CAS106-02-5

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $7.0 / 9.0

Type:Trading Company

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:White to off-white powder Storage:room temperature Package:25kg/drum Application:Pentadecanolide is a monomer used to make PGA-co-pentadecalactone polymers to be used in the development of directly compressed prolonged release tablets of

cyclopentadecanolide factory price

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Cyclopentadecanolide 106-02-5

Cas:106-02-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Cyclopentadecanolide

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $72.0 / 84.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

Cyclopentadecanolide CAS:106-02-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm

Cyclopentadecanolide CAS:106-02-5

Cas:106-02-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Cyclopentadecanolide

Cas:106-02-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Cyclopentadecanolide

Cas:106-02-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Cyclopentadecanolide

Cas:106-02-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Cyclopentadecanolide

Cas:106-02-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hefei Zhaobo Technology Co., Ltd.

Our Advantages Production: Advanced chemical equipment with years of experience Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Specif

Pentadecan-15-olide CAS 106-02-5

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $75.0 / 150.0

Type:Trading Company

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Cyclopentadecanolide

Cas:106-02-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Cyclopentadecanolide CAS NO.106-02-5

Cas:106-02-5

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Cyclopentadecanolide

Cas:106-02-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Cyclopentadecanolide CAS NO.106-02-5

Cas:106-02-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

Oxacyclohexadecan-2-One

Cas:106-02-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Cyclopentadecanolide CAS NO.106-02-5

Cas:106-02-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Cyclopentadecanolide CAS NO.106-02-5

Cas:106-02-5

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Cyclopentadecanolide CAS NO.106-02-5

Cas:106-02-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Shandong Jiling Chemical Co., Ltd

factory Storage:Shading, sealed and preserved. Package:Grams, Kilograms Application:An organic synthetic intermediate used Transportation:According to customer request Port:Qingdao

Cyclopentadecanolide

Cas:106-02-5

Min.Order:0

Negotiable

Type:Other

inquiry

Hubei Vanz Pharm Co.,Ltd

ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai

Cyclopentadecanolide

Cas:106-02-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

cyclopentadecanolide

Cas:106-02-5

Min.Order:0

Negotiable

Type:Other

inquiry

Lonwin Chemical Group Limited

Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is

Hot Sale Cyclopentadecanolide 106-02-5

Cas:106-02-5

Min.Order:100 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

inquiry

Synthetic route

15-pentadecyn-2-olide

15-pentadecyn-2-olide

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With hydrogen; platinum(IV) oxide100%
15-hydroxylpentadecanoic acid
4617-33-8

15-hydroxylpentadecanoic acid

A

pentadecanolide
106-02-5

pentadecanolide

B

1,17-dioxa-cyclodotriacontane-2,18-dione
659-76-7

1,17-dioxa-cyclodotriacontane-2,18-dione

Conditions
ConditionsYield
With p-nitrobenzoic anhydride; scandium tris(trifluoromethanesulfonate) In tetrahydrofuran; acetonitrile Heating; Yields of byproduct given;A 99%
B n/a
With dmap; 2-methyl-6-nitrobenzoic anhydride In dichloromethane at 20℃; for 15h;A 92%
B 1%
With dmap; di-2-thienyl carbonate; hafnium(IV) trifluoromethanesulfonate In toluene; acetonitrile at 100℃; for 5h;A 92%
B n/a
(E)-6-pentadecen-15-olide
63294-84-8

(E)-6-pentadecen-15-olide

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With hydrogen; palladium-barium carbonate under 1520 Torr; for 3h; Ambient temperature;99%
(E/Z)-oxacyclohexadec-11-en-2-one
76293-72-6, 76293-73-7, 4941-77-9

(E/Z)-oxacyclohexadec-11-en-2-one

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In ethyl acetate at 20℃; under 760.051 Torr; for 16h; Solvent; Concentration; Schlenk technique; Glovebox;99%
With hydrogen; palladium on activated charcoal under 760 Torr;94%
With hydrogen; palladium on activated charcoal94%
With hydrogen; platinum(IV) oxide under 760 Torr;
With 5%-palladium/activated carbon; hydrogen In methanol at 25℃; for 24h;89.2 %Chromat.
E-Pentadec-2-ene-15-olide
87227-39-2

E-Pentadec-2-ene-15-olide

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal99%
With hydrogen; palladium on activated charcoal In ethyl acetate at 20℃; under 760 Torr; for 3h;98%
With hydrogen; palladium on activated charcoal In ethanol; ethyl acetate for 48h; Ambient temperature;48 mg
15-hydroxylpentadecanoic acid
4617-33-8

15-hydroxylpentadecanoic acid

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With dmap; polymer bound carbodiimide; 4-(dimethylamino)pyridine hydrochloride In tetrahydrofuran; chloroform Cyclization; lactonisation; Heating;97%
With dmap; 4-(dimethylamino)pyridine hydrochloride; dicyclohexyl-carbodiimide In tetrahydrofuran; chloroform Heating;95%
With dmap; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In tetrahydrofuran; chloroform for 18h; Reflux; Inert atmosphere;95%
(Z)-Oxacyclohexadec-6-en-2-one
195320-68-4

(Z)-Oxacyclohexadec-6-en-2-one

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal under 760 Torr;95%
With hydrogen; palladium on activated charcoal95%
trimethylsilyl 15-(trimethylsiloxy)pentadecanoate
93472-40-3

trimethylsilyl 15-(trimethylsiloxy)pentadecanoate

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
dipropylboryl triflate In toluene Heating;94%
15-hydroxypentadecanoic acid butyl ester

15-hydroxypentadecanoic acid butyl ester

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With titanium(IV) isopropylate at 70 - 250℃; under 3.75038 Torr; for 0.333333h; Reagent/catalyst; Inert atmosphere;92.9%
12-iodo-15-pentadecanolide
118072-05-2

12-iodo-15-pentadecanolide

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene Irradiation;92%
With 2,2'-azobis(isobutyronitrile); iodine; tri-n-butyl-tin hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene 1.) THF, reflux, 40 min, 2.) THF, ether; Multistep reaction;
(14-Carboxy-tetradecyl)-diphenyl-sulfonium; perchlorate

(14-Carboxy-tetradecyl)-diphenyl-sulfonium; perchlorate

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With potassium carbonate In acetone for 12h; Heating;92%
With potassium carbonate In acetone for 48h; Heating; Yield given;
1-(N,4-dimethylphenylsulfonylamino)vinyl 15-hydroxypentadecanoate

1-(N,4-dimethylphenylsulfonylamino)vinyl 15-hydroxypentadecanoate

A

pentadecanolide
106-02-5

pentadecanolide

B

N-methyl-N-tosylacetamide
16697-83-9

N-methyl-N-tosylacetamide

Conditions
ConditionsYield
With camphor-10-sulfonic acid In dichloromethane at 20℃; for 4h;A 92%
B n/a
1-(N,4-dimethylphenylsulfonylamino)vinyl 15-hydroxypentadecanoate

1-(N,4-dimethylphenylsulfonylamino)vinyl 15-hydroxypentadecanoate

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With toluene-4-sulfonic acid In dichloromethane at 20℃;92%
15-(tert-butyldimethylsilyloxy)-pentadecanoic acid
77744-43-5

15-(tert-butyldimethylsilyloxy)-pentadecanoic acid

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With tetrabutylammonium tetrafluoroborate; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In chloroform for 18h; Reflux; Inert atmosphere;91%
Multi-step reaction with 4 steps
1.1: n-BuLi / diethyl ether / 0 °C
1.2: (COCl)2; DMF / diethyl ether
2.1: Et3N / CH2Cl2 / 0 - 20 °C
3.1: 96 percent / 3HF*Et3N / acetonitrile / 20 °C
4.1: 58 percent / Cu(OTf)2 / tetrahydrofuran / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: n-BuLi / diethyl ether / 0 °C
1.2: (COCl)2; DMF / diethyl ether
2.1: Et3N / CH2Cl2 / 0 - 20 °C
3.1: 57 percent / 3HF*Et3N / acetonitrile / 20 °C
4.1: 83 percent / Cu(OTf)2 / tetrahydrofuran / 20 °C
View Scheme
12-oxo-15-pentadecanolide
38223-29-9

12-oxo-15-pentadecanolide

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With hydrogenchloride; zinc In acetic anhydride at 0 - 5℃; for 1h;90%
With hydrogenchloride; zinc In toluene at 0℃;84%
With sodium cyanoborohydride; toluene-4-sulfonic acid; toluene-4-sulfonic acid hydrazide 1.) DMF, sulfolane, 15 min., 2.) cyclohexane, reflux, 4 h;50%
Multi-step reaction with 2 steps
1: methanol / 0.67 h / Heating
2: <<(C6H5)3P>Cu>BH4 / CHCl3 / 4 h / Heating
View Scheme
15-Hydroxy-pentadecanoic acid (Z)-2-dimethylcarbamoyl-1-methyl-vinyl ester
89611-22-3

15-Hydroxy-pentadecanoic acid (Z)-2-dimethylcarbamoyl-1-methyl-vinyl ester

A

pentadecanolide
106-02-5

pentadecanolide

B

N,N-Dimethylacetoacetamid
2044-64-6

N,N-Dimethylacetoacetamid

Conditions
ConditionsYield
With magnesium bromide In tetrahydrofuran at 55℃; other solvents, temperatures and reagent;A 90%
B n/a
13-Benzenesulfonyl-oxacyclohexadecan-2-one
81238-39-3

13-Benzenesulfonyl-oxacyclohexadecan-2-one

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With disodium hydrogenphosphate; sodium amalgam In methanol; 1,2-dimethoxyethane at -25℃; for 3h;90%
Acrylic acid 12-iodo-dodecyl ester
109182-98-1

Acrylic acid 12-iodo-dodecyl ester

A

pentadecanolide
106-02-5

pentadecanolide

B

1,17-dioxa-cyclodotriacontane-2,18-dione
659-76-7

1,17-dioxa-cyclodotriacontane-2,18-dione

Conditions
ConditionsYield
With sodium cyanoborohydride In methanol for 3h; Ambient temperature; Irradiation;A 90%
B 7 % Chromat.
trimethylsilyl 15-(trimethylsiloxy)pentadecanoate
93472-40-3

trimethylsilyl 15-(trimethylsiloxy)pentadecanoate

A

pentadecanolide
106-02-5

pentadecanolide

B

1,17-dioxa-cyclodotriacontane-2,18-dione
659-76-7

1,17-dioxa-cyclodotriacontane-2,18-dione

Conditions
ConditionsYield
With 4-(trifluoromethyl)benzoic anhydride; silver perchlorate; titanium tetrachloride In dichloromethane for 3h; Ambient temperature;A 89%
B 4%
With 4-(trifluoromethyl)benzoic anhydride; silver perchlorate; titanium tetrachloride In dichloromethane; toluene at 20℃; for 33h;A 89%
B 2%
Z-oxacyclohexadec-3-en-2-one
173790-14-2

Z-oxacyclohexadec-3-en-2-one

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With samarium diiodide; 2,4-dichlorophenoxyacetic acid dimethylamine; tert-butyl alcohol In tetrahydrofuran for 0.5h; Ambient temperature;88%
methyl 15-hydroxypentadecanoate
76529-42-5

methyl 15-hydroxypentadecanoate

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With Lipase B immobilized on acrylic resin from Candida antarctica In cyclohexane; water at 40℃; for 2h; Enzymatic reaction;88%
Multi-step reaction with 4 steps
1: Imidazole / dimethylformamide
2: 5.0 M NaOH / tetrahydrofuran; methanol; H2O / 7 h
3: 1.) DCC, DMAP; 2.) CH3COOH / 1.) THF, -25 deg C, 4 days; 2.) H2O, room temp., 8 h
4: 45 percent Chromat. / t-BuOK / benzene; tetrahydrofuran
View Scheme
Multi-step reaction with 4 steps
1: Imidazole / dimethylformamide
2: 5.0 M NaOH / tetrahydrofuran; methanol; H2O / 7 h
3: 1.) DCC, DMAP; 2.) CH3COOH / 1.) THF, -25 deg C, 4 days; 2.) H2O, room temp., 8 h
4: 74 percent / t-BuOK, molecular sieves / benzene; tetrahydrofuran / Heating; also without molecuar sieves and reflux
View Scheme
Multi-step reaction with 4 steps
1: Imidazole / dimethylformamide
2: 5.0 M NaOH / tetrahydrofuran; methanol; H2O / 7 h
3: 1.) 1-<3-(Dimethylamino)propyl>-3-ethylcarboximide hydrochloride, DMAP; 2.) CH3COOH / 1.) DMF, 1 day; 2.) H2O, 12 h
4: 81 percent / t-BuOK, molecular sieves / benzene; tetrahydrofuran / Heating; also without molecuar sieves and reflux
View Scheme
Multi-step reaction with 4 steps
1: Imidazole / dimethylformamide
2: 5.0 M NaOH / tetrahydrofuran; methanol; H2O / 7 h
3: 1.) DCC, DMAP; 2.) CH3COOH / 1.) THF, -25 deg C, 5 days; 2.) THF-H2O, room temp., 20 h
4: 43 percent Chromat. / t-BuOK, 19-crown-6 / benzene; tetrahydrofuran
View Scheme
cyclopentadecanone
502-72-7

cyclopentadecanone

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; for 108h;86%
Stage #1: cyclopentadecanone With N-hydroxyphthalimide; 1,1-Diphenylmethanol; 2,2'-azobis(isobutyronitrile); oxygen In acetonitrile at 75℃; under 760.051 Torr; for 22h; Baeyer-Villiger oxidation;
Stage #2: With 1,1,1,3',3',3'-hexafluoro-propanol; toluene-4-sulfonic acid at 60℃; Baeyer-Villiger oxidation; Inert atmosphere;
70%
With potassium peroxomonosulphate; sulfuric acid; Petroleum ether at 50 - 65℃;
15-bromo-pentadecanoic acid
56523-59-2

15-bromo-pentadecanoic acid

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With tetraoctylammonium (2-pyrrolidonide) In N,N-dimethyl-formamide for 24h; Ambient temperature;84%
With potassium carbonate In dimethyl sulfoxide at 75℃; for 4h;78%
With potassium carbonate; butanone
15-hydroxylpentadecanoic acid
4617-33-8

15-hydroxylpentadecanoic acid

2-chloro-1-methyl-pyridinium iodide
14338-32-0

2-chloro-1-methyl-pyridinium iodide

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With triethylamine In acetonitrile84%
With tributyl-amine In acetonitrile74%
With triethylamine In toluene63%.
15-hydroxy-pentadecanoic acid 6-methyl-pyridin-2-yl ester
874583-99-0

15-hydroxy-pentadecanoic acid 6-methyl-pyridin-2-yl ester

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With copper(II) bis(trifluoromethanesulfonate) In tetrahydrofuran at 20℃;83%
15-Hydroxy-pentadecanethioic acid S-[(2R,3aR,19aS)-1-(tetradecahydro-4,7,10,13,16,19-hexaoxa-cyclopentacyclooctadecen-2-yl)methyl] ester
77744-39-9

15-Hydroxy-pentadecanethioic acid S-[(2R,3aR,19aS)-1-(tetradecahydro-4,7,10,13,16,19-hexaoxa-cyclopentacyclooctadecen-2-yl)methyl] ester

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With molecular sieve; potassium tert-butylate In tetrahydrofuran; benzene Heating;81%
With molecular sieve; potassium tert-butylate In tetrahydrofuran; benzene Product distribution; Heating; also without molecuar sieves and reflux;81%
N-nitro-15-pentadecanelactam
122695-16-3

N-nitro-15-pentadecanelactam

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
In tetrachloromethane for 12h; Heating;80%
methyl 15-hydroxypentadecanoate
76529-42-5

methyl 15-hydroxypentadecanoate

A

pentadecanolide
106-02-5

pentadecanolide

B

1,17-dioxa-cyclodotriacontane-2,18-dione
659-76-7

1,17-dioxa-cyclodotriacontane-2,18-dione

Conditions
ConditionsYield
In benzene at 40℃; for 72h; Lipase P;A 78%
B n/a
With Lipase P In benzene at 40℃; for 72h; Product distribution;
15-hydroxylpentadecanoic acid
4617-33-8

15-hydroxylpentadecanoic acid

2-chloro-1-ethyl-3-methylpyridinium tetrafluoroborate

2-chloro-1-ethyl-3-methylpyridinium tetrafluoroborate

pentadecanolide
106-02-5

pentadecanolide

Conditions
ConditionsYield
With triethylamine In acetonitrile78%
methanol
67-56-1

methanol

pentadecanolide
106-02-5

pentadecanolide

methyl 15-hydroxypentadecanoate
76529-42-5

methyl 15-hydroxypentadecanoate

Conditions
ConditionsYield
With sulfuric acid Reflux;100%
With sulfuric acid Reflux;100%
With toluene-4-sulfonic acid for 24h; Esterification; Ring cleavage; Heating;99%
pentadecanolide
106-02-5

pentadecanolide

15-hydroxylpentadecanoic acid
4617-33-8

15-hydroxylpentadecanoic acid

Conditions
ConditionsYield
With (Z)-9-octadecen-1-amine; lipase PS from Pseudomonas cepacia; water In Hexadecane at 40℃; for 0.5h; Miniemulsion system; Enzymatic reaction;100%
With sodium hydroxide In tetrahydrofuran; methanol; water100%
With potassium hydroxide In methanol; water for 5.5h; Heating;99%
pentadecanolide
106-02-5

pentadecanolide

15-iodo-pentadecanoic acid
71736-22-6

15-iodo-pentadecanoic acid

Conditions
ConditionsYield
With hydrogen iodide In acetic acid for 3h; Ring cleavage; iodination; Heating;100%
With aluminium(III) iodide In acetonitrile at 80℃; for 18h;99%
With hydrogen iodide In acetic acid for 6h; Heating;93%
pentadecanolide
106-02-5

pentadecanolide

potassium 15-hydroxypentadecanoate
871570-58-0

potassium 15-hydroxypentadecanoate

Conditions
ConditionsYield
With ethanol; potassium hydroxide for 2h; Reflux;100%
With potassium hydroxide In ethanol for 2h; Reflux;100%
With potassium hydroxide In ethanol for 2h; Reflux;100%
With potassium hydroxide In methanol
pentadecanolide
106-02-5

pentadecanolide

sodium methylate
124-41-4

sodium methylate

methyl 15-hydroxypentadecanoate
76529-42-5

methyl 15-hydroxypentadecanoate

Conditions
ConditionsYield
In methanol at 20℃; for 16h; Inert atmosphere; Darkness;99%
In methanol at 20℃;80%
pentadecanolide
106-02-5

pentadecanolide

1,15-pentadecanediol
14722-40-8

1,15-pentadecanediol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 72h;98.6%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 4h; Inert atmosphere;97%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 4h; Inert atmosphere;96%
pentadecanolide
106-02-5

pentadecanolide

15-bromo-pentadecanoic acid
56523-59-2

15-bromo-pentadecanoic acid

Conditions
ConditionsYield
With sulfuric acid; hydrogen bromide for 84h; Heating;98%
With hydrogen bromide; acetic acid at 60℃; for 16h; Product distribution / selectivity; Autoclave; Inert atmosphere;91%
With sulfuric acid; hydrogen bromide for 20h; Heating;84%
methanol
67-56-1

methanol

pentadecanolide
106-02-5

pentadecanolide

sodium methylate
124-41-4

sodium methylate

methyl 15-hydroxypentadecanoate
76529-42-5

methyl 15-hydroxypentadecanoate

Conditions
ConditionsYield
for 3h; Heating / reflux;98%
pentadecanolide
106-02-5

pentadecanolide

methylmagnesium bromide
75-16-1

methylmagnesium bromide

15-methylhexadecan-1,15-diol
728935-75-9

15-methylhexadecan-1,15-diol

Conditions
ConditionsYield
Stage #1: pentadecanolide; methylmagnesium bromide In tetrahydrofuran at -78 - 20℃; for 16h; Inert atmosphere;
Stage #2: With acetic acid In tetrahydrofuran; water Cooling with ice;
98%
indole
120-72-9

indole

pentadecanolide
106-02-5

pentadecanolide

ω-(3-indolyl)pentadecanoic acid
74022-43-8

ω-(3-indolyl)pentadecanoic acid

Conditions
ConditionsYield
With sodium hydroxide at 250℃; for 18h; Product distribution; autoclave, other base, other temperature;95%
pentadecanolide
106-02-5

pentadecanolide

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

Phosphoric acid (E)-(oxacyclohexadec-2-en-2-yl) ester diphenyl ester

Phosphoric acid (E)-(oxacyclohexadec-2-en-2-yl) ester diphenyl ester

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 0.5h;91%
pentadecanolide
106-02-5

pentadecanolide

n-Octylamine
111-86-4

n-Octylamine

N-octyl-15-hydroxypentadecanoylamine
1220909-19-2

N-octyl-15-hydroxypentadecanoylamine

Conditions
ConditionsYield
With lipase PS from Pseudomonas cepacia; water In Hexadecane at 40℃; for 192h; Miniemulsion system; Enzymatic reaction;91%
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