DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryCyclopentadecanone Basic information Product Name: Cyclopentadecanone Synonyms: CYCLOPENTADECANONE;CYCLOPENTADECONE;EXALTONE;Normuscon;NORMUSCONE;OXOCYCLOPENTADECAN
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Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Conditions | Yield |
---|---|
With Amberlyst A26 resin bound bis(azido)iodate(I) In acetonitrile at 20℃; for 18h; Irradiation; Inert atmosphere; | 100% |
With iodine; [bis(pyridine)iodine]+ tetrafluoroborate; caesium carbonate In acetonitrile at 60℃; for 7h; | 92% |
With chromium(VI) oxide; sulfuric acid; benzene |
2-Oxocyclopentadecancarbonsaeure-methylester
cyclopentadecanone
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water for 3h; Heating; | 100% |
cyclopentadecanone oxime
cyclopentadecanone
Conditions | Yield |
---|---|
With 2,2'-dipyridyldiselenide; trimethylphosphane In tetrahydrofuran; toluene at 20℃; for 0.5h; Product distribution; Further Variations:; Reagents; Solvents; | 100% |
With diphenyldisulfane; triethylphosphine In tetrahydrofuran for 0.333333h; Ambient temperature; | 92% |
Stage #1: cyclopentadecanone oxime With diphenyldisulfane; trimethylphosphane In tetrahydrofuran at 20℃; Stage #2: With water In tetrahydrofuran Further stages.; | |
With gold(III) tribromide; dimethylglyoxal In ethanol; water at 20℃; for 15h; pH=7; | 100 %Spectr. |
(2E)-cyclopentadec-2-en-1-one
cyclopentadecanone
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal | 100% |
cyclopentadec-4-yn-1-one
cyclopentadecanone
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen In ethanol at 20℃; under 3750.38 Torr; for 8h; Temperature; Autoclave; | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol | 98% |
cyclopentadec-2-en-1-one
cyclopentadecanone
Conditions | Yield |
---|---|
With enone reductase from Sporidiobolus salmonicolor TPU 2001; NADH In aq. phosphate buffer at 30℃; for 1h; pH=7; Kinetics; Enzymatic reaction; | 97.5% |
cyclopentadecanone
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate | 95% |
trans-cyclopentadec-5-enone
cyclopentadecanone
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol | 91% |
cyclopentadecanone
Conditions | Yield |
---|---|
With hydrogen; palladium In ethanol | 88% |
cyclopentadecanone
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water for 15h; Heating; | 86% |
N'-cyclopentadecylidene-4-methylbenzenesulfonohydrazide
cyclopentadecanone
Conditions | Yield |
---|---|
Envirocat EPZG In water; acetone at 80℃; for 3h; | 86% |
5-Iodo-cyclopentadecanone
cyclopentadecanone
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene Irradiation; | 80% |
N-Cyclopentadecylidene-N'-methyl-hydrazine
A
cyclopentadecanone
Conditions | Yield |
---|---|
With iodine monofluoride In chloroform | A 5% B 80% |
cyclopentadecanone
Conditions | Yield |
---|---|
With sodium tetrahydroborate; dihydrogen peroxide; potassium carbonate In methanol for 20h; Ambient temperature; | 80% |
dimethyl hexadecanedioate
cyclopentadecanone
Conditions | Yield |
---|---|
TiO2 + 2 % K2O In tetrahydrofuran at 350℃; Gas phase; | 78% |
With potassium tert-butylate In decalin at 190℃; for 48h; | 6% |
With N-ethyl-N-phenylamine; sodium- anschl. mit wss. H2SO4; |
5-Hydroxy-cyclopentadecanon
cyclopentadecanone
Conditions | Yield |
---|---|
78% |
Conditions | Yield |
---|---|
With hydrogenchloride; zinc In 1,4-dioxane; water at 95 - 100℃; for 17h; | 77% |
With hydrogenchloride; ethanol; zinc | |
With hydrogen; 5%-palladium/activated carbon In toluene at 250℃; under 7500.75 Torr; for 1 - 5h; | 62 - 93 %Chromat. |
Cyclopentadecanone hydrazone
A
cyclopentadecanone
Conditions | Yield |
---|---|
With iodine monofluoride In chloroform at 25℃; | A 50% B 40% |
1,2,10,11-tetraoxocyclotricosane-3,6,9,12,23-pentaone
cyclopentadecanone
Conditions | Yield |
---|---|
thermal decomposition; | 40% |
cyclopentadecanone
Conditions | Yield |
---|---|
Stage #1: methyl cis-16-oxabicyclo[13.1.0]hexadecane-1-carboxylate With methanol; water; sodium hydroxide for 5h; Reflux; Stage #2: With hydrogenchloride; methanol; water for 1h; Reflux; | 33% |
diethyl hexadecanedioate
A
cyclopentadecanone
B
cyclotriacontane-1,16-dione
Conditions | Yield |
---|---|
With potassium tert-butylate; xylene |
Conditions | Yield |
---|---|
With metal oxide | |
at 300 - 500℃; Erhitzen von Salzen unter vermindertem Druck; | |
Thermische Zersetzung des Thoriumsalzes, des Cersalzes oder anderer Salze; |
1,16-hexadecanedioyl dichloride
A
cyclopentadecanone
B
cyclotriacontane-1,16-dione
Conditions | Yield |
---|---|
With diethyl ether; triethylamine 3-std. Kochen des Reaktionsprodukts mit aethanol. KOH; | |
With etheric solution; triethylamine Erhitzen des Reaktionsprodukts mit aethanol. KOH; |
hexadecanedioic acid-anhydride
cyclopentadecanone
Conditions | Yield |
---|---|
With metal oxide | |
at 300 - 500℃; Erhitzen von Salzen unter vermindertem Druck; | |
With metal oxide | |
at 300 - 500℃; Erhitzen von Salzen unter vermindertem Druck; |
diethyl ether
1,16-hexadecanedioyl dichloride
triethylamine
A
cyclopentadecanone
B
cyclotriacontane-1,16-dione
Conditions | Yield |
---|---|
beim Kochen des Reaktionsprodukts mit alkoh. KOH; |
tetradeca-1,13-diene
Dichloromethyl methyl ether
A
cyclopentadecanone
B
2-nonylcyclohexanone
Conditions | Yield |
---|---|
With 9-borabicyclo[3.3.1]nonane dimer; dimethylsulfide borane complex Product distribution; |
bicyclo[10.3.0]pentadec-1(12)-en-13-one
cyclopentadecanone
2-Brom-1-cyclopentadecen-1-carbonsaeuremethylester
cyclopentadecanone
Conditions | Yield |
---|---|
With sodium hydroxide; sodium methylate 1.) methanol, reflux, 5 h, 2.) methanol, water, reflux, 7 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: 1-Bromonaphthalene With iodine; magnesium In diethyl ether Grignard reaction; Stage #2: cyclopentadecanone In diethyl ether Grignard reaction; | 100% |
cyclopentadecanone
1-chloroethyl p-tolyl sulfoxide
1-[1-chloro-1-(p-tolylsulfinyl)ethyl]-1-cyclopentadecanol
Conditions | Yield |
---|---|
at -70℃; | 100% |
Stage #1: 1-chloroethyl p-tolyl sulfoxide With lithium diisopropyl amide In tetrahydrofuran at -70℃; Stage #2: cyclopentadecanone In tetrahydrofuran at -70℃; | |
Stage #1: 1-chloroethyl p-tolyl sulfoxide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.25h; Stage #2: cyclopentadecanone In tetrahydrofuran at -78℃; for 0.25h; |
cyclopentadecanone
5-fluorouridine
5-fluoro-1-[(3a'R,4'R,6'R,6a'R)-3a',4',6',6a'-tetrahydro-6'-(hydroxymethyl)spiro[cyclopentadecane-1,2'-furo[3,4-d][1,3]dioxol]-4'-yl]pyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
With hydrogenchloride; orthoformic acid triethyl ester In 1,4-dioxane; N,N-dimethyl-formamide at 20℃; for 24h; | 100% |
With orthoformic acid triethyl ester In N,N-dimethyl-formamide Acidic conditions; |
cyclopentadecanone
1,1-dichlorocyclopentadecane
Conditions | Yield |
---|---|
With phosphorus pentachloride In benzene at 0 - 20℃; for 28h; | 99% |
cyclopentadecanone
(S)-1-amino-2-(methoxymethyl)pyrrolidine
Conditions | Yield |
---|---|
at 70℃; for 20h; Condensation; | 99% |
cyclopentadecanone
Conditions | Yield |
---|---|
With water-d2; palladium on activated charcoal at 250℃; for 10h; | 99% |
With water-d2; palladium on activated charcoal at 250℃; for 10h; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In cyclohexane | 98% |
With toluene-4-sulfonic acid In toluene for 16h; Reflux; |
cyclopentadecanone
(1,1-dimethylethyl)diphenylsilyl cyanide
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 72h; | 97% |
cyclopentadecanone
chloromethyl p-tolyl sulfoxide
1-[Chloro-(toluene-4-sulfinyl)-methyl]-cyclopentadecanol
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; | 97% |
With lithium diisopropyl amide at -78℃; | 97% |
With lithium diisopropyl amide 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 10 min.; Yield given. Multistep reaction; |
cyclopentadecanone
sodium methylate
methyl cyclotetradec-1-ene-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: cyclopentadecanone With bromine In diethyl ether; toluene at 20 - 25℃; for 0.5h; Stage #2: sodium methylate In toluene at 20 - 25℃; for 0.5h; | 97% |
cyclopentadecanone
2,2-dimethoxyethylamine
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; Inert atmosphere; Schlenk technique; | 97% |
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 24h; Inert atmosphere; | 93% |
cyclopentadecanone
chloromethyl p-tolyl sulfoxide
3'-(p-tolylsulfinyl)spiro[cyclopentadecane-1,2'-oxirane]
Conditions | Yield |
---|---|
Stage #1: chloromethyl p-tolyl sulfoxide With lithium diisopropyl amide In tetrahydrofuran at -78℃; Stage #2: cyclopentadecanone In tetrahydrofuran at -78℃; Stage #3: With potassium tert-butylate In tetrahydrofuran; tert-butyl alcohol at 0℃; | 94% |
Conditions | Yield |
---|---|
With sodium dodecyl-sulfate; Selectfluor In water at 80℃; Micellar solution; regioselective reaction; | A n/a B 92% |
cyclopentadecanone
anthranilic acid amide
Conditions | Yield |
---|---|
With iodine; zirconium(IV) oxide In neat (no solvent) at 25℃; for 2h; Autoclave; Milling; Green chemistry; | 91% |
cyclopentadecanone
8-hydroxycyclopentadecanone
Conditions | Yield |
---|---|
With ferredoxin reductase; [2Fe–2S] ferredoxin; cytochrome P450 enzyme CYP101B1 In aq. buffer pH=7.4; Kinetics; Enzymatic reaction; | 90% |
In ethanol (microbiological transformation); |
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical
cyclopentadecanone
Conditions | Yield |
---|---|
Stage #1: cyclopentadecanone With lithium chloride; lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.75h; Inert atmosphere; Stage #2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical With ferrocenium hexafluorophosphate at -78℃; for 0.833333h; | 90% |
cyclopentadecanone
(2E)-cyclopentadec-2-en-1-one
Conditions | Yield |
---|---|
Stage #1: cyclopentadecanone With chloro-trimethyl-silane; lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; Stage #2: palladium diacetate In acetonitrile for 2h; | 89% |
Multi-step reaction with 2 steps 1: tetrahydrofuran / 24 h / 20 °C 2: hydrogen peroxide / tetrahydrofuran; H2O / 1 h View Scheme | |
Multi-step reaction with 3 steps 1: diethyl ether / 2 h / Ambient temperature 2: SO2Cl2 / hexane; diethyl ether 3: 92 percent / aq. NaHCO3 / CH2Cl2 / 4 h View Scheme |
cyclopentadecanone
(phenylthio)methyllithium
1-(phenylthiomethyl)cyclopentadecanol
Conditions | Yield |
---|---|
88% | |
85% |
cyclopentadecanone
p-methoxy-phenylazide
1-(4-methoxyphenyl)-1,4,5,6,7,8,9,10,11,12,13,14,15,16-tetradecahydro-1H-cyclopentadeca[d][1,2,3]triazole
Conditions | Yield |
---|---|
With L-proline In dichloromethane at 80℃; Sealed tube; | 87% |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; for 108h; | 86% |
Stage #1: cyclopentadecanone With N-hydroxyphthalimide; 1,1-Diphenylmethanol; 2,2'-azobis(isobutyronitrile); oxygen In acetonitrile at 75℃; under 760.051 Torr; for 22h; Baeyer-Villiger oxidation; Stage #2: With 1,1,1,3',3',3'-hexafluoro-propanol; toluene-4-sulfonic acid at 60℃; Baeyer-Villiger oxidation; Inert atmosphere; | 70% |
With potassium peroxomonosulphate; sulfuric acid; Petroleum ether at 50 - 65℃; |
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