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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Palmatine Chloride supplier in China

Cas:10605-02-4

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price API 99% Palmatine chloride 10605-02-4 GMP Manufacturer

Cas:10605-02-4

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Palmatine chloride

Cas:10605-02-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Pharmaceutical Palmatine Chloride CAS 10605-02-4 Medical Grade

Cas:10605-02-4

Min.Order:1 Kilogram

FOB Price: $60.0 / 100.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Competitve Price in stockCAS 10605-02-4 with high quality products

Cas:10605-02-4

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Dibenzo[a,g]quinolizinium,5,6-dihydro-2,3,9,10-tetramethoxy-, chloride (1:1) 10605-02-4

Cas:10605-02-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Palmatine chloride CAS:10605-02-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter

Palmatine chloride CAS:10605-02-4

Cas:10605-02-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Dibenzo[a,g]quinolizinium,5,6-dihydro-2,3,9,10-tetramethoxy-, chloride (1:1)

Cas:10605-02-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Taizhou Crene Biotechnology co.ltd

Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

Palmatine chloride 10605-02-4

Cas:10605-02-4

Min.Order:100 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Palmatine chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

Palmatine chloride

Cas:10605-02-4

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Palmatine Chloride

Cas:10605-02-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h

Factory Supply Palmatine chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Other

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Palmatine chloride

Cas:10605-02-4

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Palmatine chloride

Cas:10605-02-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea

IsoliensinineCAS NO.: 10605-02-4

Cas:10605-02-4

Min.Order:1 Kilogram

FOB Price: $4.0

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Palmatinechloride

Cas:10605-02-4

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Palmatine chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

shanghai Tauto Biotech Co., Ltd

The quality is guaranteed. If you find the product is wrong compared with COA, we promise 100% refund or change product. COA and HPLC will be shipped out with goods. You can also inform your analysis method and we will follow your analysis me

E-0294 Palmatine chloride

Cas:10605-02-4

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so

TIANFUCHEM--10605-02-4---Palmatine chloride

Cas:10605-02-4

Min.Order:1 Metric Ton

FOB Price: $500.0

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Palmatine chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Other

inquiry

Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

Isoliensinine CAS 10605-02-4

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Other

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

Palmatine-Hydrochloride

Cas:10605-02-4

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Sinoway Industrial Co., Ltd.

Why is SINOWAY:1) Specialized in pharmaceutical and healthcare industrial since 19872) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days.4) We have warehouse in USA with quickly shipment . Application:API

99% up by HPLC Palmatine chloride 10605-02-4

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Dingyan Chem Co., Ltd

high purity, manufacturer Application:Intermediate

Palmatine hydrochloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec Palmatine (chloride) P74831 20mg

Cas:10605-02-4

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Palmatine chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Palmatine Chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

Palmatine chloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Chengdu Lemeitian Pharmaceutical Technology Co,. Ltd

ADVANTAGE:1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day2. The products are provided with COA, HPLC, NMR, quality assurance, pac

Palmatine hydrochloride

Cas:10605-02-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

2-[2-(6,7-dimethoxyisoquinolin-3-yl)-4,5-dimethoxyphenyl]ethanol

2-[2-(6,7-dimethoxyisoquinolin-3-yl)-4,5-dimethoxyphenyl]ethanol

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
With methanesulfonyl chloride; triethylamine In dichloromethane at 20℃; for 6h;92%
With tetrachloromethane; triphenylphosphine In dichloromethane at 27 - 30℃; for 24h; Inert atmosphere;70%
2-(2-(2-(1,3-dioxolan-2-yl)-3,4-dimethoxyphenyl)acetyl)-4,5-dimethoxyphenethyl pivalate

2-(2-(2-(1,3-dioxolan-2-yl)-3,4-dimethoxyphenyl)acetyl)-4,5-dimethoxyphenethyl pivalate

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Stage #1: 2-(2-(2-(1,3-dioxolan-2-yl)-3,4-dimethoxyphenyl)acetyl)-4,5-dimethoxyphenethyl pivalate With ammonium chloride In ethanol; water at 90 - 110℃; for 56h;
Stage #2: With sodium hydroxide In water for 0.0833333h;
88%
With ammonium chloride In ethanol; water at 90 - 110℃; for 66h; Inert atmosphere;
methyl p-toluene sulfonate
80-48-8

methyl p-toluene sulfonate

2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride

2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Stage #1: methyl p-toluene sulfonate; 2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride With potassium carbonate In acetonitrile at 80℃; for 12h; Green chemistry;
Stage #2: Reagent/catalyst; Solvent; Temperature; Green chemistry;
80%
dimethyl sulfate
77-78-1

dimethyl sulfate

2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride

2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
With potassium carbonate In methanol at 60℃; for 6h;75%
2,3-dihydroxyberberine methanesulfonate

2,3-dihydroxyberberine methanesulfonate

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Stage #1: 2,3-dihydroxyberberine methanesulfonate; carbonic acid dimethyl ester With caesium carbonate In N,N-dimethyl-formamide at 140℃; for 8h;
Stage #2: With hydrogenchloride In water for 0.5h; Solvent; Reagent/catalyst;
73.5%
2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride

2,3-dihydroxy-9,10-dimethoxy-5,6-dihydro-isoquino[3,2-a]isoquinolinylium chloride

methyl iodide
74-88-4

methyl iodide

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
With sodium hydroxide In methanol at 25℃; for 6h;60%
2-{[2-(2-hydroxyethyl)-4,5-dimethoxyphenyl]ethynyl}-4,5-dimethoxybenzaldehyde

2-{[2-(2-hydroxyethyl)-4,5-dimethoxyphenyl]ethynyl}-4,5-dimethoxybenzaldehyde

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: silver nitrate; ammonium acetate / tert-butyl alcohol / 14 h / 27 - 30 °C / Inert atmosphere
2: triphenylphosphine; tetrachloromethane / dichloromethane / 24 h / 27 - 30 °C / Inert atmosphere
View Scheme
2-acetyl-4,5-dimethoxyphenethyl pivalate

2-acetyl-4,5-dimethoxyphenethyl pivalate

2-(6-bromo-2,3-dimethoxyphenyl)-1,3-dioxolane

2-(6-bromo-2,3-dimethoxyphenyl)-1,3-dioxolane

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: caesium carbonate; bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II) / tetrahydrofuran / 18 h / 90 °C / Inert atmosphere
2: ammonium chloride / water; ethanol / 66 h / 90 - 110 °C / Inert atmosphere
View Scheme
berberine chloride
633-65-8

berberine chloride

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: trifluorormethanesulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 0.5 h / 25 °C
1.2: 0 °C
1.3: anion-exchange resin (Cl-)
2.1: potassium carbonate / acetonitrile / 12 h / 80 °C / Green chemistry
2.2: anion-exchange resin (Cl-) / Green chemistry
View Scheme
Multi-step reaction with 2 steps
1.1: trifluorormethanesulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 0.5 h / 25 °C
1.2: 0 °C
1.3: anion-exchange resin (Cl-)
2.1: potassium carbonate / methanol / 6 h / 60 °C
View Scheme
2,3-dimethoxybenzyl amine
4393-09-3

2,3-dimethoxybenzyl amine

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: C14H22O4Rh / water / 24 h / 100 °C / Sealed tube; Green chemistry
2.1: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / 2 h / 100 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 1 h / 20 °C
View Scheme
1-(3,4-dimethoxyphenyl)-2-(dimethyl(oxo)-λ6-sulfanylidene)ethan-1-one

1-(3,4-dimethoxyphenyl)-2-(dimethyl(oxo)-λ6-sulfanylidene)ethan-1-one

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: C14H22O4Rh / water / 24 h / 100 °C / Sealed tube; Green chemistry
2.1: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / 2 h / 100 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3.2: 1 h / 20 °C
View Scheme
3,4-dimethoxybenzoic acid chloride
3535-37-3

3,4-dimethoxybenzoic acid chloride

palmatine chloride
10605-02-4

palmatine chloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Reflux
1.2: 3 h / 0 - 20 °C
2.1: C14H22O4Rh / water / 24 h / 100 °C / Sealed tube; Green chemistry
3.1: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / 2 h / 100 °C
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
4.2: 1 h / 20 °C
View Scheme
chloroform
67-66-3

chloroform

palmatine chloride
10605-02-4

palmatine chloride

8-trichloromethyl-7,8-dihydropalmatine
50932-23-5

8-trichloromethyl-7,8-dihydropalmatine

Conditions
ConditionsYield
With ammonium hydroxide for 24h;100%
With ammonium hydroxide at 20℃; for 24h;74.9%
palmatine chloride
10605-02-4

palmatine chloride

C17H14NO4(1+)*Br(1-)

C17H14NO4(1+)*Br(1-)

Conditions
ConditionsYield
With hydrogen bromide Heating;100%
pyrrole
109-97-7

pyrrole

palmatine chloride
10605-02-4

palmatine chloride

8-(pyrrol-1-yl)-7,8-dihydropalmatine
1106994-66-4

8-(pyrrol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: pyrrole With sodium hydride In tetrahydrofuran Sonication; Inert atmosphere;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; for 5h; Inert atmosphere;
98%
palmatine chloride
10605-02-4

palmatine chloride

Palmatrubine hydrochloride
16705-04-7

Palmatrubine hydrochloride

Conditions
ConditionsYield
at 180℃; Microwave irradiation;95%
Stage #1: palmatine chloride at 195℃; for 0.25h;
Stage #2: With hydrogenchloride In ethanol at 20℃; for 1h;
94%
Stage #1: palmatine chloride at 195 - 210℃;
Stage #2: With hydrogenchloride In ethanol; water
86%
methanol
67-56-1

methanol

palmatine chloride
10605-02-4

palmatine chloride

8-methoxy-7,8-dihydropalmatine
60229-93-8

8-methoxy-7,8-dihydropalmatine

Conditions
ConditionsYield
With sodium methylate for 24h;90%
1H-imidazole
288-32-4

1H-imidazole

palmatine chloride
10605-02-4

palmatine chloride

8-(imidazol-1-yl)-7,8-dihydropalmatine
1106994-78-8

8-(imidazol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: 1H-imidazole With sodium hydride In tetrahydrofuran Sonication; Inert atmosphere;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; for 17.5h; Inert atmosphere;
88%
palmatine chloride
10605-02-4

palmatine chloride

(trifluoromethyl)trimethylsilane
81290-20-2

(trifluoromethyl)trimethylsilane

(±)-8-trifluoromethyldihydropalmatine

(±)-8-trifluoromethyldihydropalmatine

Conditions
ConditionsYield
With cesium fluoride In dichloromethane at 40℃; for 48h;86.1%
palmatine chloride
10605-02-4

palmatine chloride

dihydropalmatine
26067-60-7

dihydropalmatine

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate; potassium carbonate at 20℃; for 3h;81.1%
With sodium tetrahydroborate; potassium carbonate; sodium hydroxide In methanol at 20℃; for 3h;79%
With sodium tetrahydroborate; potassium carbonate; sodium hydroxide In methanol at 20℃; for 3h;79%
With methanol; sodium tetrahydroborate; potassium carbonate Reflux;54%
1,2,4-Triazole
288-88-0

1,2,4-Triazole

palmatine chloride
10605-02-4

palmatine chloride

8-(1,2,4-triazol-1-yl)-7,8-dihydropalmatine
1106994-81-3

8-(1,2,4-triazol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: 1,2,4-Triazole With sodium hydride In tetrahydrofuran Sonication; Inert atmosphere;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; for 17.5h; Inert atmosphere;
74%
5-bromo-1H-indole
10075-50-0

5-bromo-1H-indole

palmatine chloride
10605-02-4

palmatine chloride

8-(5-bromoindol-1-yl)-7,8-dihydropalmatine
1407154-42-0

8-(5-bromoindol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: 5-bromo-1H-indole With sodium hydride In tetrahydrofuran for 0.25h; Inert atmosphere; Sonication;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; Inert atmosphere;
73%
NH-pyrazole
288-13-1

NH-pyrazole

palmatine chloride
10605-02-4

palmatine chloride

8-(pyrazol-1-yl)-7,8-dihydropalmatine
1106994-75-5

8-(pyrazol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: NH-pyrazole With sodium hydride In tetrahydrofuran Sonication; Inert atmosphere;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;
63%
Glyoxal
131543-46-9

Glyoxal

palmatine chloride
10605-02-4

palmatine chloride

C23H22NO4(1+)*Cl(1-)

C23H22NO4(1+)*Cl(1-)

Conditions
ConditionsYield
Stage #1: palmatine chloride With sodium tetrahydroborate; potassium carbonate; sodium hydroxide In methanol at 20℃; for 3h;
Stage #2: Glyoxal With acetic acid In acetonitrile for 6h; Reflux;
Stage #3: With hydrogenchloride In methanol; water at 20℃; for 24h;
62%
sodium methylate
124-41-4

sodium methylate

palmatine chloride
10605-02-4

palmatine chloride

5,6-dihydro-2,3,8,9-10-pentamethoxydibenzoquinolizinium-13-olate
112435-30-0

5,6-dihydro-2,3,8,9-10-pentamethoxydibenzoquinolizinium-13-olate

Conditions
ConditionsYield
With oxygen; rose bengal In methanol at 0℃; for 0.333333h; Irradiation;60%
palmatine chloride
10605-02-4

palmatine chloride

palmatrubine
16176-68-4

palmatrubine

Conditions
ConditionsYield
at 190℃; under 10 - 15 Torr; for 7h;59%
palmatine chloride
10605-02-4

palmatine chloride

4-methoxy-benzylamine
2393-23-9

4-methoxy-benzylamine

2,3,10‐trimethoxy‐9‐p‐methoxybenzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐p‐methoxybenzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 6h;57%
palmatine chloride
10605-02-4

palmatine chloride

acetone
67-64-1

acetone

(±)-8-acetonyldihydropalmatine
38699-74-0

(±)-8-acetonyldihydropalmatine

Conditions
ConditionsYield
With sodium hydroxide In water at 20℃; for 3h;54.9%
With sodium hydroxide In water for 0.5h;
palmatine chloride
10605-02-4

palmatine chloride

para-fluorobenzylamine
140-75-0

para-fluorobenzylamine

2,3,10‐trimethoxy‐9‐p‐fluorobenzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐p‐fluorobenzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 7h;54%
1H-indole-5-carbonitrile
15861-24-2

1H-indole-5-carbonitrile

palmatine chloride
10605-02-4

palmatine chloride

8-(5-cyanoindol-1-yl)-7,8-dihydropalmatine
1407154-43-1

8-(5-cyanoindol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: 1H-indole-5-carbonitrile With sodium hydride In tetrahydrofuran for 0.25h; Inert atmosphere; Sonication;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; Inert atmosphere;
53%
7-Azaindole
271-63-6

7-Azaindole

palmatine chloride
10605-02-4

palmatine chloride

8-(7-azaindol-1-yl)-7,8-dihydropalmatine
1407154-44-2

8-(7-azaindol-1-yl)-7,8-dihydropalmatine

Conditions
ConditionsYield
Stage #1: 7-Azaindole With sodium hydride In tetrahydrofuran for 0.25h; Inert atmosphere; Sonication;
Stage #2: palmatine chloride In tetrahydrofuran at 20℃; Inert atmosphere;
52%
2,4-Dimethoxybenzylamine
20781-20-8

2,4-Dimethoxybenzylamine

palmatine chloride
10605-02-4

palmatine chloride

2,3,10‐trimethoxy‐9‐o,p‐dimethoxybenzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐o,p‐dimethoxybenzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 6h;52%
palmatine chloride
10605-02-4

palmatine chloride

para-methylbenzylamine
104-84-7

para-methylbenzylamine

2,3,10‐trimethoxy‐9‐p‐methylbenzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐p‐methylbenzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 4h;48%
4-Bromobenzylamine
3959-07-7

4-Bromobenzylamine

palmatine chloride
10605-02-4

palmatine chloride

2,3,10‐trimethoxy‐9‐p‐bromobenzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐p‐bromobenzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 7h;44%
palmatine chloride
10605-02-4

palmatine chloride

3-methyl-benzenemethanamine
100-81-2

3-methyl-benzenemethanamine

2,3,10‐trimethoxy‐9‐m‐methylbenzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐m‐methylbenzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 4h;43%
palmatine chloride
10605-02-4

palmatine chloride

benzylamine
100-46-9

benzylamine

2,3,10‐trimethoxy‐9‐benzylaminoprotopalmatine chloride

2,3,10‐trimethoxy‐9‐benzylaminoprotopalmatine chloride

Conditions
ConditionsYield
at 110℃; for 6h;41%

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