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Cas:4393-09-3
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inquiryName: 2,3-Dimethoxybenzylamine Synonyms: (2,3-dimethoxyphenyl)methanamine CAS: 4393-09-3 MF: C9H13NO2 Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum Application:Orga
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inquiry2,3-Dimethoxybenzylamine CAS:4393-09-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents
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2,3-DimethoxybenzylamineAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Min.Order:10 Milligram
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inquiry2,3-Dimethoxybenzylamine Basic information Product Name: 2,3-Dimethoxybenzylamine Synonyms: (2,3-Dimethoxyphenyl)methanamine;RARECHEM AL BW 0151;2,3-DIMETHOXYBENZYL
Cas:4393-09-3
Min.Order:10 Gram
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Type:Trading Company
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2,3-Dimethoxybenzylamine supplierAppearance:White to almost white crystaline Storage:Keep away of light,cool place Package:25kg/drum;200kg/drum Application:Pharma Intermediate Transportation:Sea/air/courier
At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App
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inquiryConditions | Yield |
---|---|
With sodium amalgam; acetic acid at 40 - 50℃; | |
With lithium aluminium tetrahydride |
Conditions | Yield |
---|---|
With sodium hydroxide; hydrogen; sodium chloride; platinum(IV) oxide 1.) ethanol, chloroform, 40 psi, 3 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethyoxybenzaldehyde In trimethyl orthoformate at 25℃; Stage #2: With lithium borohydride In tetrahydrofuran at 65℃; for 5h; Stage #3: With trifluoroacetic acid In dichloromethane at 25℃; for 5h; |
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 25℃; for 5h; ((9-(amino)xanthen-2-yl)oxy)butanoic acid handle, p-methylbenzhydrylamine resin (H2N-XAL-MBHA resin); |
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
Stage #1: C9H10NO2Pol With lithium borohydride In tetrahydrofuran at 65℃; for 5h; Stage #2: With trifluoroacetic acid In dichloromethane at 25℃; for 5h; |
boc-β-methoxyalanine dicyclohexylamine
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
In ethyl acetate | 100% |
2,3-dimethoxybenzyl amine
Fmoc-Pro-OH
2-(2,3-dimethoxy-benzylcarbamoyl)-pyrrolidine-1-carboxylic acid 9H-fluoren-9-ylmethyl ester
Conditions | Yield |
---|---|
Stage #1: Fmoc-Pro-OH With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 0.333333h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile at 20℃; | 99% |
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
With iodine; potassium carbonate In N,N-dimethyl-formamide for 18h; Heating; | 99% |
8-(2,3-dimethoxy-benzoylamino)-octanoic acid
2,3-dimethoxybenzyl amine
N-[7-(2,3-dimethoxy-benzylcarbamoyl)-heptyl]-2,3-dimethoxy-benzamide
Conditions | Yield |
---|---|
Stage #1: 8-(2,3-dimethoxy-benzoylamino)-octanoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile for 0.5h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile | 96% |
2,3-dimethoxybenzyl amine
Fmoc-Asn-OH
[2-carbamoyl-1-(2,3-dimethoxy-benzylcarbamoyl)-ethyl]-carbamic acid 9H-fluoren-9-ylmethyl ester
Conditions | Yield |
---|---|
Stage #1: Fmoc-Asn-OH With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 0.333333h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile at 20℃; | 95% |
Conditions | Yield |
---|---|
With iodine; potassium carbonate In N,N-dimethyl-formamide for 18h; Heating; | 95% |
(R)-6-oxo-1,2-dithia-5-azacyclodecane-4-carboxylic acid
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
Stage #1: (R)-6-oxo-1,2-dithia-5-azacyclodecane-4-carboxylic acid With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole In tetrahydrofuran at 20℃; for 0.5h; Stage #2: 2,3-dimethoxybenzyl amine In tetrahydrofuran at 20℃; for 18h; Further stages.; | 94% |
2,3-dimethoxybenzyl amine
acetic anhydride
N-(2,3-dimethoxybenzyl)acetamide
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 12h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With iodine; potassium carbonate In N,N-dimethyl-formamide for 18h; Heating; | 93% |
Conditions | Yield |
---|---|
In dichloromethane | 90% |
2,3-dimethoxybenzyl amine
Fmoc-(tBu)Asp-OH
N-(2,3-dimethoxy-benzyl)-3-(9H-fluoren-9-ylmethoxycarbonylamino)-succinamic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: Fmoc-(tBu)Asp-OH With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide for 2h; Stage #2: 2,3-dimethoxybenzyl amine In dichloromethane; N,N-dimethyl-formamide | 90% |
Conditions | Yield |
---|---|
With iodine; potassium carbonate In N,N-dimethyl-formamide for 18h; Heating; | 90% |
BOC-glycine
2,3-dimethoxybenzyl amine
N-t-butoxycarbonylglycine(2,3-dimethoxybenzyl)amide
Conditions | Yield |
---|---|
Stage #1: BOC-glycine With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide for 1h; Stage #2: 2,3-dimethoxybenzyl amine In dichloromethane; N,N-dimethyl-formamide | 88% |
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
Stage #1: Fmoc-His(Mtt)-OH With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 0.333333h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile at 20℃; | 87% |
2,3-dimethoxybenzyl amine
N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine
[3-carbamoyl-1-(2,3-dimethoxy-benzylcarbamoyl)-propyl]-carbamic acid 9H-fluoren-9-ylmethyl ester
Conditions | Yield |
---|---|
Stage #1: N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 0.333333h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile at 20℃; | 87% |
Conditions | Yield |
---|---|
Inert atmosphere; | 84% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 24h; |
2,3-dimethoxybenzyl amine
methyl 5-(N,N-dimethylamino)-2,4-pentadienoate
Conditions | Yield |
---|---|
In tetrahydrofuran for 85h; Heating; | 83% |
Conditions | Yield |
---|---|
Stage #1: Hippuric Acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide for 1h; Stage #2: 2,3-dimethoxybenzyl amine In dichloromethane; N,N-dimethyl-formamide | 82% |
2,3-dimethoxybenzyl amine
N-(9-fluorenylmethoxycarbonyl)-O-methyl-L-tyrosine
[1-(2,3-dimethoxy-benzylcarbamoyl)-2-(4-methoxy-phenyl)-ethyl]-carbamic acid 9H-fluoren-9-ylmethyl ester
Conditions | Yield |
---|---|
Stage #1: N-(9-fluorenylmethoxycarbonyl)-O-methyl-L-tyrosine With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 0.333333h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile at 20℃; | 82% |
Conditions | Yield |
---|---|
With potassium carbonate; dimethyl sulfoxide at 80℃; for 2h; | 82% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethoxybenzyl amine With triethylamine In tetrahydrofuran at 0℃; for 0.25h; Stage #2: cyanomethyl bromide In tetrahydrofuran at 0 - 20℃; for 16h; | 82% |
2,3-dimethoxybenzyl amine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide for 48h; | 81% |
2,3-dimethoxybenzyl amine
2-bromo-1-o-tolylethanone
Conditions | Yield |
---|---|
With iodine; potassium carbonate In N,N-dimethyl-formamide for 18h; Heating; | 80% |
8-chloro-2,2-dimethyl-5-pyrrolidin-1-yl-1,4-dihydro-2H-pyrano[4'',3":4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine
2,3-dimethoxybenzyl amine
N-(2,3-dimethoxybenzyl)-5-(pyrrolidin-1-yl)-2,2-dimethyl-1,4-dihydro-2H-pyrano[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine-8-amine
Conditions | Yield |
---|---|
In ethanol for 24h; Heating / reflux; | 79% |
2,3-dimethoxybenzyl amine
N-2,3-Dimethoxybenzoyl-glycine
Conditions | Yield |
---|---|
Stage #1: N-2,3-Dimethoxybenzoyl-glycine With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide In 1,4-dioxane at 20℃; for 16h; Stage #2: 2,3-dimethoxybenzyl amine With sodium hydrogencarbonate In water for 20h; | 77% |
Conditions | Yield |
---|---|
Stage #1: azelaic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile for 0.25h; Stage #2: 2,3-dimethoxybenzyl amine In acetonitrile for 2h; | 77% |
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In chloroform for 48h; Reflux; | 76% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 10h; | 75% |
Conditions | Yield |
---|---|
With iodine; potassium carbonate In N,N-dimethyl-formamide for 18h; Heating; | 75% |
Conditions | Yield |
---|---|
Stage #1: N-dodecanoylglycine With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide for 1h; Stage #2: 2,3-dimethoxybenzyl amine In dichloromethane; N,N-dimethyl-formamide | 74% |
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