Appearance:Colorless liquid Storage:well sealed in dry cool place Package:40KG/200KG/plastic coated metal pail/ISOTANK Application:used for medical &pesticide intermediate Transportation:BY SEA Port:Tianjin, Shanghai
Cas:1070-83-3
Min.Order:1 Metric Ton
FOB Price: $90.0 / 100.0
Type:Trading Company
inquiryDayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryProduct description: Product name 3,3-Dimethylbutyric acid CAS number 1070-83-3 Assay ≥99% Appearance Yellowish to colorless transparent liquid Capacity 200mt/year Application
Cas:1070-83-3
Min.Order:100 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquirytert-Butylacetic acid Synonyms 3,3-Dimethylbutyric acid; Butylaceticacid; 3,3-Dimethylbutyric acid; 3,3-dimethylbutanoic acid; 3,3-dimethylbutanoate; 3,3,3-TRIMETHYLPROPIONIC ACID CAS RN. 1070-83-3
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $2.0 / 3.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:1070-83-3
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryTIANFUCHEM--1070-83-3--3,3-Dimethylbutyric acid in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business re
Cas:1070-83-3
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1070-83-3
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:1070-83-3
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Name: 3,3-Dimethylbutyric acid Molecular Formula: C6H12O2 Molecular Weight: 116.16 CAS: 1070-83-3 Structural Formula: Appearance:Colorless clear liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/dr
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Other
inquiryAppearance:Light yellow to colorless transparent liquid Storage:R.T Package:25kg/drum Application:Pharmaceutical intermediate Transportation:Express/Sea/Air Port:Any port in China
Cas:1070-83-3
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:1070-83-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $90.0 / 95.0
Type:Trading Company
inquiry3,3-Dimethylbutyric acid CAS:1070-83-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:1070-83-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:1070-83-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:1070-83-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:1070-83-3
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:1070-83-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:1070-83-3
Min.Order:100 Gram
Negotiable
Type:Other
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:1070-83-3
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:1070-83-3
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryProduct name: 3,3-Dimethyl Butyric Acid CAS No.: 1070-83-3 Molecule Formula:C6H11O2 Molecule Weight:115.15 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING
Cas:1070-83-3
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, in
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $666.0 / 777.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:1070-83-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:1070-83-3
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:1070-83-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:1070-83-3
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryConditions | Yield |
---|---|
With dihydrogen peroxide; 7-(trifluoromethyl)-1,10-ethyleneisoalloxazinium chloride In water; acetonitrile at 85℃; for 18h; | 98% |
With oxygen; copper(II) acetate monohydrate; cobalt(II) diacetate tetrahydrate In water at 20℃; under 760.051 Torr; for 3h; | 95% |
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; for 3h; Schlenk technique; | 83% |
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; under 760.051 Torr; for 3h; Catalytic behavior; Solvent; Schlenk technique; | 83% |
With dihydrogen peroxide; benzeneseleninic acid In tetrahydrofuran for 2h; Heating; | 76 % Chromat. |
Conditions | Yield |
---|---|
With sulfuric acid at 2℃; for 0.75h; | 90% |
With sulfuric acid; boron trifluoride | |
(i) H2SO4, BF3, (ii) aq. H2SO4; Multistep reaction; | |
With sulfuric acid at 0 - 5℃; for 1.25h; |
3,3-dimethyl-1-butynyl tosylate
tert-Butylacetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In acetonitrile for 24h; Heating; | 90% |
With hydrogenchloride In acetonitrile for 24h; Mechanism; Heating; other alkynyl tosylate; | 90% |
Conditions | Yield |
---|---|
With potassium hydroxide; oxygen In 1,2-dimethoxyethane at 20℃; for 14h; | 85% |
With alkaline KMNO4 at 4℃; |
Conditions | Yield |
---|---|
With boron trifluoride In sulfuric acid 1.) 5-15 deg C, 3 h, 2.) 10 deg C, 0.5 h; | 81% |
With sulfuric acid at 6℃; for 2h; | 77% |
(i) H2SO4, BF3, (ii) aq. H2SO4; Multistep reaction; |
neo-hexylboronic acid
tert-Butylacetic acid
Conditions | Yield |
---|---|
With chromium(VI) oxide In dichloromethane; acetic acid at 25℃; for 12h; | 80% |
tert-Butylacetic acid
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran; methanol at 20℃; for 4h; | 68% |
Conditions | Yield |
---|---|
With sulfuric acid at 5℃; for 0.5h; | 55% |
3,3-dimethylbutanol
A
3,3-dimethylbutyrylaldehyde
B
tert-Butylacetic acid
Conditions | Yield |
---|---|
With copper(II) oxide at 300℃; Gas phase; | A n/a B 30% |
4,4-dimethyl-pentan-2-one
A
tert-Butylacetic acid
B
acetic acid
C
Trimethylacetic acid
Conditions | Yield |
---|---|
With oxygen; H5PV2Mo10O40(1,11) In acetonitrile at 60℃; under 750.06 Torr; for 24h; | A 20% B 16% C 20% |
Conditions | Yield |
---|---|
bei der Ozonspaltung; |
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
With alkaline Ca(OCl)2 | |
With sodium hypobromide | |
With sodium hypobromide |
Conditions | Yield |
---|---|
With potassium permanganate |
1,1,1-trichloro-3,3-dimethyl-butane
tert-Butylacetic acid
Conditions | Yield |
---|---|
With water at 275℃; |
1,1-dichloro-3,3-dimethyl-1-butene
tert-Butylacetic acid
Conditions | Yield |
---|---|
With water at 275℃; |
ethyl t-butylcyanoacetate
tert-Butylacetic acid
Conditions | Yield |
---|---|
With hydrogen bromide |
Conditions | Yield |
---|---|
With potassium hydroxide | |
Multi-step reaction with 2 steps 1: alcoholic KOH View Scheme |
4-t-amylphenol
A
tert-Butylacetic acid
B
3,3-dimethyl-2-oxopentanoic acid
Conditions | Yield |
---|---|
With potassium permanganate Oxydation; |
1,1-dimethylpropylmagnesium chloride
methylammonium carbonate
tert-Butylacetic acid
Conditions | Yield |
---|---|
Multistep reaction; |
Conditions | Yield |
---|---|
(i) Li, Et2O, (ii) /BRN= 1900390/, (iii) aq. HCl; Multistep reaction; |
1,1-Dichloroethylene
2,6-di-tert-butyl-4-methoxymethylene-phenol
tert-Butylacetic acid
Conditions | Yield |
---|---|
With sulfuric acid at 5℃; |
1,2,3-trichloro-5,5-dimethyl-hex-2-ene
tert-Butylacetic acid
Conditions | Yield |
---|---|
With potassium hydroxide; potassium permanganate |
N-(3,3-Dimethyl-1-tosyl-1-butenyl)-formamid
tert-Butylacetic acid
Conditions | Yield |
---|---|
With hydrogenchloride |
carbon dioxide
2,2-dimethylpropylmagnesium chloride
tert-Butylacetic acid
Conditions | Yield |
---|---|
With diethyl ether | |
(i) MnCl2, THF, (ii) /BRN= 1900390/; Multistep reaction; |
Conditions | Yield |
---|---|
(i) H2SO4, BF3, (ii) aq. H2SO4; Multistep reaction; |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; | |
Multi-step reaction with 3 steps 1: HBr 2: potassium acetate / und man verseift das erhaltene Acetat durch Erhitzen mit gepulvertem Kali auf 200grad View Scheme |
(E)-1-(diethoxymethylsilyl)-3,3-dimethyl-1-butene
tert-Butylacetic acid
Conditions | Yield |
---|---|
With potassium hydrogen bifluoride; dihydrogen peroxide In acetic anhydride; N,N-dimethyl-formamide for 20h; Ambient temperature; Yield given; |
tert-Butylacetic acid
(S)-3-(benzyloxy)-2-isocyano-N-methoxy-N-methylpropanamide
Boc-L-phenylalaninal
C33H47N3O8
Conditions | Yield |
---|---|
In dichloromethane Passerini reaction; | 100% |
tert-Butylacetic acid
Conditions | Yield |
---|---|
Stage #1: tert-Butylacetic acid With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 0℃; for 0.25h; Stage #2: (2R)-2-amino-N-(1-cyanocyclopropyl)-3-[4-(2-pyridyl)piperazin-1-yl]sulfonyl-propanamide With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
Heating; | 98% |
With sulfuric acid | |
(i) SOCl2, (ii) /BRN= 1098229/; Multistep reaction; | |
With sulfuric acid at 75℃; for 2h; Yield given; |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 25℃; for 18h; | 98% |
oxalyl dichloride
Methyl (+/-)-3-oxo-8-[3-(1-oxo-pyridin-2-yl)amino-1-propyloxy]-2-(4-trifluoromethylbenzyl)-2,3,4.5-tetrahydro-1H-2-benzazepine-4-acetate
tert-Butylacetic acid
methyl (+/-)-3-oxo-8-[3-[N-(1-oxo-pyridin-2-yl)-N-(tert-butylacetyl)amino]-1-propyloxy]-2-(4-trifluoromethylbenzyl)-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; N,N-dimethyl-formamide | 97% |
Conditions | Yield |
---|---|
With hydrogen; silica gel; palladium at 330℃; | 96% |
Conditions | Yield |
---|---|
With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane at 25℃; for 14h; Acylation; | 96% |
With dicyclohexyl-carbodiimide In tetrahydrofuran for 12h; | 49% |
With 1,2-dichloro-ethane In dichloromethane for 3h; |
Conditions | Yield |
---|---|
In toluene mixt. 3,3-dimethylbutanoic acid (6 equiv.) and zinc oxide (4 equiv.) and toluene heated with stirring for 3 h (water removed); product filtered, solvent removed from filtrate, purified by recrystn.;elem. anal.; | 96% |
Conditions | Yield |
---|---|
In acetonitrile at 100℃; for 72h; Inert atmosphere; High pressure; | 96% |
In toluene Ti-isopropoxide added dropwise to soln. of (CH3)3CCH2COOH in toluene, mixt. stirred for 12 h; crystn. on slow evapn. under Ar for 2-3 d; elem. anal.; | 24.2% |
tetrahydrofuran
tert-Butylacetic acid
ethyl 2-(2-bromophenyl)-2-diazoacetate
Conditions | Yield |
---|---|
With potassium carbonate at 80℃; for 12h; Inert atmosphere; Schlenk technique; | 96% |
tert-Butylacetic acid
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; water | 95% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 24h; | 95% |
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 24h; | 95% |
tert-Butylacetic acid
2,4-bis(tert-butyl)acetoacetic acid
Conditions | Yield |
---|---|
Stage #1: tert-Butylacetic acid With trifluorormethanesulfonic acid; trifluoroacetic anhydride at 60 - 65℃; Stage #2: With water Cooling; | 94% |
Multi-step reaction with 3 steps 1: (i) LDA, (ii) /BRN= 1209232/ 2: 230 - 240 °C 3: aq. HCl View Scheme | |
Multi-step reaction with 2 steps 1: trifluorormethanesulfonic acid / 2.5 h / 65 °C 2: water / 0.5 h / Cooling with ice View Scheme |
tert-Butylacetic acid
4-methoxycarbonyl aniline
4-(3,3-dimethylbutanamido)benzoic acid
Conditions | Yield |
---|---|
Stage #1: tert-Butylacetic acid; 4-methoxycarbonyl aniline With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 24h; Stage #2: With ethanol; water; lithium hydroxide In tetrahydrofuran at 65℃; for 3h; | 94% |
tert-Butylacetic acid
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose
1,2;5,6-di-O-(1-methylethylidene)-α-D-glucofuranosyl 3,3-dimethyl butanoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; | 93% |
tert-Butylacetic acid
Conditions | Yield |
---|---|
Stage #1: tert-Butylacetic acid With dmap; diisopropyl-carbodiimide In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; Stage #2: (2S,4R)-allyl 4-(2-((1R,3R)-3-((tert-butoxycarbonyl)(methyl)amino)-1-hydroxy-4-methylpentyl)thiazole-4-carboxamido)-2-methyl-5-phenylpentanoate In dichloromethane Inert atmosphere; | 93% |
tert-Butylacetic acid
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride
(S)-benzyl 1-(3,3-dimethylbutanoyl)pyrrolidine-2-carboxylate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature; | 92% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 74% |
tert-Butylacetic acid
O-diphenylmethyl 2,2,2-trichloroacetimidate
benzhydryl 3,3-dimethylbutanoate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 18h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; phenylsilane; 1,2-bis-(diphenylphosphino)ethane In dibutyl ether at 60℃; for 18h; Schlenk technique; Inert atmosphere; | 92% |
tert-Butylacetic acid
(2S,4R)-benzyl 4-hydroxypyrrolidine-2-carboxylate hydrochloride
Conditions | Yield |
---|---|
Stage #1: tert-Butylacetic acid; (2S,4R)-benzyl 4-hydroxypyrrolidine-2-carboxylate hydrochloride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 0.5h; | 91% |
chlorosulfuric acid chloromethyl ester
tert-Butylacetic acid
chloromethyl 3,3-dimethylbutanoate
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate In dichloromethane; water at 0 - 20℃; for 16h; | 91% |
tert-Butylacetic acid
Conditions | Yield |
---|---|
In toluene dry inert atm.; equimolar ratio, stirring (12 h); concn., evapn., crystn., drying; elem. anal.; | 90.9% |
tert-Butylacetic acid
1,3-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-β-D-galactopyranosyl)-glycerol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 90% |
tert-Butylacetic acid
2,3,4,5,6-pentafluorophenol
3,3-dimethylbutyric acid pentafluorophenyl ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In 1,4-dioxane for 12h; | 90% |
tert-Butylacetic acid
Conditions | Yield |
---|---|
In water; acetone | 90% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; trifluoroacetic anhydride In dichloromethane at 20℃; for 24h; | 90% |
In dichloromethane at 20℃; for 3h; |
tert-Butylacetic acid
Conditions | Yield |
---|---|
With dmap; copper diacetate In acetonitrile at 80℃; for 3h; Schlenk technique; Sealed tube; | 90% |
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