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inquiryConditions | Yield |
---|---|
im UV-Licht; |
neopentyl chlorosulfite
neopentyl chloride
Conditions | Yield |
---|---|
In acetone at 322℃; Rate constant; Mechanism; other solvents; other temp.; | |
With quinoline hydrochloride | |
In acetone at 48.9℃; |
Conditions | Yield |
---|---|
With chlorine In benzene at 20℃; Product distribution; Irradiation; with various initial Cl2 concentrations; | |
With chlorine | |
With sodium hypochlorite; (5,10,15,20-tetramesitylporphyrinato)manganese(III) chloride; tetrabutyl-ammonium chloride In dichloromethane; water at 20℃; Inert atmosphere; | |
With sodium hypochlorite; 5,10,15,20-tetramesitylporphyrinatomanganese(III) chloride; tetrabutyl-ammonium chloride In dichloromethane; water at 20℃; Inert atmosphere; Sealed tube; | 31%Chromat. |
dichloro(neopentyloxy)borane
A
2-methyl-2-butylchloride
B
neopentyl chloride
Conditions | Yield |
---|---|
at 150℃; |
triethyl(neopentyloxy)silane
neopentyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; quinoline hydrochloride |
trichloroacetamido-neopentanol
A
2-methyl-but-2-ene
B
2-methyl-2-butylchloride
C
neopentyl chloride
Conditions | Yield |
---|---|
at 150℃; das Hydrochlorid reagiert; |
Conditions | Yield |
---|---|
With bromine; chlorine In trichlorofluoromethane at 10℃; for 0.00266667h; Irradiation; Yield given; |
Conditions | Yield |
---|---|
With acetyl hypochlorite; chlorine In dichloromethane at -78℃; for 3h; Irradiation; |
2,2-dimethylpropane
A
neopentyl chloride
B
1,3-dichloro-2,2-dimethylpropane
C
1,1-dichloro-2,2-dimethylpropane
Conditions | Yield |
---|---|
With chlorine In 1,1,2-Trichloro-1,2,2-trifluoroethane at 23℃; Mechanism; Product distribution; Irradiation; var. neopentane conc., solvents, solvents mixtures, and in vapour phase; other alkanes; |
Conditions | Yield |
---|---|
With chloride In gas Thermodynamic data; ΔH0Rx; |
N,N-Dicloro-tert-octylamine
A
2,4,4-trimethyl-1-pentene
B
2,4,4-trimethylpent-2-ene
C
neopentyl chloride
D
isobutene
Conditions | Yield |
---|---|
In dichloromethane at 270℃; Product distribution; Mechanism; var. concentrations, var. reaction temperatures, var. reactors; |
Neopentyloxy-triphenyl-phosphonium-chlorid
A
neopentyl chloride
B
Triphenylphosphine oxide
Conditions | Yield |
---|---|
In acetonitrile Mechanism; Rate constant; decomposition; |
benzyl chloride
dineopentyl phenyl phosphite
A
neopentyl chloride
B
diphenyl benzylphosphonate
C
Benzyl-phosphonic acid 2,2-dimethyl-propyl ester phenyl ester
Conditions | Yield |
---|---|
In neat (no solvent) at 20 - 100℃; for 8976h; | A 19.3 % Chromat. B n/a C n/a |
dineopentyl phenyl phosphite
neopentyl chloride
Conditions | Yield |
---|---|
With benzyl chloride In neat (no solvent) at 20 - 100℃; for 8976h; | 19.3 % Chromat. |
2,2-dichloro-2-neopentoxy-1,3,2-benzodioxaphosphole
A
o-phenylene chlorophosphate
B
neopentyl chloride
Conditions | Yield |
---|---|
at -50℃; |
2,2-dimethyl-propanol-1
ammonium thiocyanate
triphenylphosphine
A
neopentyl chloride
B
1-isothiocyanato-2,2-dimethylpropane
C
Neopentyl thiocyanate
Conditions | Yield |
---|---|
With tetrachloromethane In acetonitrile for 10h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
neopentyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride | |
With phosphorus pentachloride |
Conditions | Yield |
---|---|
im Licht; |
neopentyl chloride
Conditions | Yield |
---|---|
Chlorieren; |
2-(neopentyloxy)benzo-1,3,2-dioxaphosphole
neopentyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chlorine / various solvent(s) / -100 °C 2: -50 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 50 percent / calcium hypochlorite, 3N HCl 2: 88 percent / 250 °C / 20percent SE-30 on fire-brick View Scheme | |
Multi-step reaction with 2 steps 1: 1.) triethylamine, 2.) glacial acetic acid / 1.) methylene chloride, 25 deg C, 8 h, 2.) 6 h, 3.) water 2: 88 percent / 130 - 150 °C / 0.3 - 0.8 Torr View Scheme |
Chloroiodomethane
tert-Butyl iodide
A
2-methyl-but-2-ene
B
neopentyl chloride
C
2-Methyl-1-butene
Conditions | Yield |
---|---|
With mercury iodide at 20℃; Kinetics; Photolysis; |
neopentyl chloroformate
neopentyl chloride
Conditions | Yield |
---|---|
at 319.84℃; under 51 Torr; Kinetics; Activation energy; Temperature; Pressure; Gas phase; |
Conditions | Yield |
---|---|
Stage #1: neopentyl chloride With lithium In tetrahydrofuran; mineral oil at -45℃; for 0.5h; Inert atmosphere; Stage #2: benzaldehyde In tetrahydrofuran; mineral oil at -45℃; for 0.5h; Inert atmosphere; | 99% |
neopentyl chloride
trimethylstannyl sodium
(neopentyl)trimethylstannane
Conditions | Yield |
---|---|
In tetrahydrofuran 0°C in N2-atmosphere; various yields for various conditions; | 96% |
In further solvent(s) byproducts: NaCl; under argon, equimolar amounts, at 0°C in tetraglyme; GLC; | 92% |
In tetrahydrofuran byproducts: NaCl; under argon, equimolar amounts, at 0°C; GLC; | 62% |
neopentyl chloride
2-amino-4,5-dimethoxybenzaldehyde
Conditions | Yield |
---|---|
In pyridine; benzene for 24h; Ambient temperature; | 82% |
neopentyl chloride
antimony(III) chloride
magnesium
trineopentylstibine
Conditions | Yield |
---|---|
In diethyl ether byproducts: MgCl2; slow addn. of neopentyl chloride to finely divided Mg in Et2O within a He-filled glovebox, heating and stirring (24 h), slow addn. of SbCl3 in Et2O (0°C), refluxing (16-18 h); removing Et2O (vac.), extg. (pentane, 4 times), sublimation (70°C, 0.005 Torr); elem. anal.; | 80% |
neopentyl chloride
dimethylsilicon dichloride
chloro(2,2-dimethylpropyl)(dimethyl)silane
Conditions | Yield |
---|---|
Stage #1: neopentyl chloride With lithium In benzene Reflux; Stage #2: dimethylsilicon dichloride In diethyl ether; benzene at 20℃; for 19h; | 79% |
(i) Li, diethyl ether, (ii) /BRN= 605287/; Multistep reaction; |
neopentyl chloride
A
perfluoroisobutylene
B
3,3,3-trifluoro-2,2-bis-trifluoromethyl-propionyl fluoride
C
1-Chloro-F-2-methylpropane
D
perfluoroneopentyl chloride
Conditions | Yield |
---|---|
With fluorine for 3h; Irradiation; aerosol; Yield given; | A n/a B n/a C n/a D 74% |
With fluorine for 3h; Irradiation; aerosol; Yields of byproduct given; | A n/a B n/a C n/a D 74% |
di(pyridin-2-yl)amine
neopentyl chloride
N-(2,2-dimethylpropyl)-N-(2-pyridyl)pyridin-2-amine
Conditions | Yield |
---|---|
Stage #1: di(pyridin-2-yl)amine With potassium hydride In N,N-dimethyl-formamide at 0℃; for 1.5h; Inert atmosphere; Stage #2: neopentyl chloride In N,N-dimethyl-formamide at 70 - 75℃; for 48h; Inert atmosphere; | 74% |
Stage #1: di(pyridin-2-yl)amine With potassium hydride In N,N-dimethyl-formamide at 0℃; for 1.5h; Inert atmosphere; Stage #2: neopentyl chloride In N,N-dimethyl-formamide at 0 - 75℃; for 48h; Inert atmosphere; | 74% |
4-hydroxy-3-methoxybenzoic acid methyl ester
neopentyl chloride
methyl 3-methoxy-4-(neopentyloxy)benzamide
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 72h; Inert atmosphere; Reflux; | 72% |
2-cyclohex-1-enyl-pyridine
neopentyl chloride
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; neopentylmagnesium bromide; cobalt(II) bromide; 1,3-diisopropyl-1H-benzo[d]imidazol-3-ium bromide In tetrahydrofuran at 60℃; for 12h; Schlenk technique; | 72% |
Conditions | Yield |
---|---|
With iron(II) triflate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; lithium hexamethyldisilazane at 140℃; for 12h; regioselective reaction; | 66% |
neopentyl chloride
neopetyl dichlorophosphine
Conditions | Yield |
---|---|
Stage #1: neopentyl chloride With magnesium In diethyl ether; ethylene dibromide Reflux; Inert atmosphere; Stage #2: With cadmium(II) chloride In diethyl ether; ethylene dibromide at 0℃; for 2h; Inert atmosphere; Stage #3: With phosphorus trichloride In diethyl ether; ethylene dibromide at 0 - 20℃; for 3.5h; Inert atmosphere; | 60% |
Conditions | Yield |
---|---|
Stage #1: neopentyl chloride With anthracene; magnesium; methyl iodide In tetrahydrofuran at 70℃; for 12.5h; Inert atmosphere; Stage #2: phenyltin trichloride In tetrahydrofuran for 8h; Reflux; Inert atmosphere; | 60% |
neopentyl chloride
3,3-dimethylbutanoic acid chloride
dineopentyl ketone
Conditions | Yield |
---|---|
Stage #1: neopentyl chloride With magnesium In tetrahydrofuran Stage #2: 3,3-dimethylbutanoic acid chloride In tetrahydrofuran at -78 - 20℃; | 58% |
(i) Mg, BrCH2CH2Br, Et2O, (ii) /BRN= 1740421/; Multistep reaction; | |
(i) Mg, Et2O, (ii) /BRN= 1740421/, Cu2Cl2; Multistep reaction; |
Conditions | Yield |
---|---|
With Mg In tetrahydrofuran (Ar); addn. dropwise of Grignard soln. prepared from Me3CCH2Cl and Mg inTHF to suspn. of Ph3BiCl in THF; stirring for 2 h at 0°C and 18 h at room temp.; removal of THF under vac., extn. with petroleum ether, removal of solvent; as oil; | 56.6% |
neopentyl chloride
4-methoxyphenyl magnesium bromide
1-(2,2-dimethylpropyl)-4-methoxybenzene
Conditions | Yield |
---|---|
With iron(III) chloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride In tetrahydrofuran at 0 - 40℃; for 1.66667h; | 54% |
2,3-dimethyl-2,3-butane diol
neopentyl chloride
2,2'-bis(1,3,2-benzodioxaborole)
Conditions | Yield |
---|---|
Stage #1: neopentyl chloride; 2,2'-bis(1,3,2-benzodioxaborole) With 2-chloro-1,3,2-benzodioxaborole; N-(2,2,2-trifluoroethoxy)phthalimide In acetonitrile at 25℃; Irradiation; Stage #2: 2,3-dimethyl-2,3-butane diol With triethylamine In acetonitrile regioselective reaction; | 50% |
neopentyl chloride
rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane
A
C18H24Si
B
rac-methylphenyl(neopentyl)(piperidinomethyl)silane
C
1,2-dimethyl-1,1,2,2-tetraphenyldisilane
Conditions | Yield |
---|---|
Stage #1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium In tetrahydrofuran at 0℃; for 6h; Inert atmosphere; Stage #2: neopentyl chloride In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | A n/a B 39% C n/a |
4-methyleneoxetan-2-one
neopentyl chloride
5,5-dimethyl-3-methylenehexanoic acid
Conditions | Yield |
---|---|
With magnesium; nickel dichloride In tetrahydrofuran 1.) 0 deg C, 45 min; 2.) -75 deg C, 1 h; | 31% |
neopentyl chloride
bis(pinacol)diborane
Conditions | Yield |
---|---|
With potassium tert-butylate; tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 80℃; for 24h; | 25% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium carbonate In N,N-dimethyl-formamide at 20℃; for 24h; | 20% |
octane
neopentyl chloride
propyl sodium
A
2,2-dimethylhexane
B
propene
C
propane
D
1,1-dimethylcyclopropane
octane
neopentyl chloride
propyl sodium
A
2,2-dimethylhexane
B
1,1-dimethylcyclopropane
Conditions | Yield |
---|---|
at 50 - 107℃; |
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