As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:546-68-9
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inquiryTests Specifications Results Appearance Colorless to light yellow liquid Colorless liquid Ti%
Cas:546-68-9
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhigh purity lowest priceOverview Quick Details Classification: Chemical Auxiliary Agent CAS No.: 546-6
Unique advantages for Titanium tetraisopropanolate Cas 546-68-9 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Liquid Storage:Flammables area Package:200kg/drum Application:
Cas:546-68-9
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inquiryService we can provide: 1. mixed container: we can mix different items in one container. 2. quality control: before shipment, we can provide free sample for test. inspection before shipping. 3. packing: we can pack according to your requireme
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:546-68-9
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inquiryTitanium tetraisopropanolate Basic information Reactions Product Name: Titanium tetraisopropanolate Synonyms: tetraisopropoxidetitanium;tetraisopropoxytitanium;tetraisopropyltitanate(flam
TIANFUCHEM-- 546-68-9--High purity Titanium tetraisopropanolate in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stabl
Cas:546-68-9
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inquiryWe are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
Cas:546-68-9
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:546-68-9
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inquiryProduct quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tr
Cas:546-68-9
Min.Order:1 Kilogram
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inquiryTitanium tetraisopropanolate CAS:546-68-9 Specification density: 0.965 g/cm3(20°c) solidifying point: 14°c titanium content: ≥16.55%)that is larger than th
Cas:546-68-9
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inquiryAppearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
Cas:546-68-9
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:546-68-9
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:546-68-9
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:546-68-9
Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Cas:546-68-9
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:546-68-9
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inquiryProduct name: Titanium(IV) Isopropoxide CAS No.:546-68-9 Molecule Formula:C12H28O4Ti Molecule Weight:284.22 Purity: 99.0% Package: 25kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TE
Cas:546-68-9
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting Tetraisopropyl titanate (TA-10;A-1(TPT)),CAS:546-68-9, Please contact us by email freely. We are leading exporter in China. If you really need this car
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inquirySAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
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inquiryOcean inorganic department is a professional supplier and exporter engaging in inorganic chemical materials and metal organic compounds. Over the past years, our company is committed to improving the product quality and developing new products, in
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Appearance:colorless liquid Storage:tightly from light Package:200kg/drum Transportation:SEA Port:Qingdao
Cas:546-68-9
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:546-68-9
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inquiryConditions | Yield |
---|---|
With diethylamine In hexane at 0℃; for 1h; Reagent/catalyst; Inert atmosphere; | 85% |
With NH3 In benzene byproducts: NH4Cl; NH4Cl sepd., Ti(OiPr)4 distilled; elem. anal.; | 70% |
With sodium byproducts: NaCl; isopropanol was placed in flask, Na was added with heating, Ti-salt was introduced; extd. with hexane, centrifuged, solvents were distilled off, vac. distillation; | 59.7% |
With ammonia In benzene under N2; TiCl4 added slowly dropwise with stirring to alc. at 0°C; the resultant mixt. dild. with benzene; dry ammonia passed for 1 h; mixt. heated for 2-3 h on a water bath at 60-65°C; ppt. filtered off; distd. under vac.; | |
With trimethylamine In not given TiCl4 reacted with 2-propanol in the presence of trimethylamine; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: NaCl; Ar; extd. with hexane, NaCl was centrifuged; | 60% |
Conditions | Yield |
---|---|
In not given Electrolysis; Ti anode, Pt cathode, Ar-atmosphere, stirring, 30 V/0.15 A, 16 h; soln. contg. various salts (Bu4NBr, Bu4NBF4, NaBr or other); distn. (50-60°C, 10 mm); elem. anal.; | |
With Bu4NBr In neat (no solvent) byproducts: H2; Electrochem. Process; Ar, at 30 V for 16 h; vac. distn.; elem. anal.; |
Conditions | Yield |
---|---|
In neat (no solvent) Ar-atmosphere; addn. of equimolar amt. of acetaldehyde to Ti-compd. at -15°C, stirring (room temp., 2 h); |
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In dichloromethane-d2 not isolated (NMR investigation of the reaction mixture); |
Conditions | Yield |
---|---|
In neat (no solvent) TiBeAl(OPri)9 disproportionates on heating under reduced pressure; |
Conditions | Yield |
---|---|
In neat (no solvent) TiBe2Al2(OPri)14 disproportionates on heating under reduced pressure; |
triisopropoxytitanium(IV) chloride
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran ligand reacted with n-BuLi (1.1 equiv.) in THF at -78°C; treated with Ti compd. (1.1 equiv.) at -78°C; warmed to room temp.; not isolated; detd. by NMR spectra; |
triisopropoxytitanium(IV) chloride
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran ligand reacted with n-BuLi (1.1 equiv.) in THF at -78°C; treated with Ti compd. (1.1 equiv.) at -78°C; warmed to room temp.; not isolated; detd. by NMR spectra; |
triisopropoxytitanium(IV) chloride
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran ligand reacted with n-BuLi (1.1 equiv.) in THF at -78°C; treated with Ti compd. (1.1 equiv.) at -78°C; warmed to room temp.; not isolated; detd. by NMR spectra; |
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In neat (no solvent) under N2; heated under reduced pressure (ca. 1E-2 Torr); |
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In neat (no solvent) under N2; heated under reduced pressure (ca. 1E-2 Torr); |
Conditions | Yield |
---|---|
In dichloromethane dry N2-atmosphere; stirring of stoich. amts. (room temp., 1 h); evapn. (reduced pressure), dissoln. in pentane, pptn. on cooling, filtration, drying (vac.), recrystn. (pentane); elem. anal.; |
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In neat (no solvent) under N2; heated under reduced pressure (ca. 1E-2 Torr); |
A
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In neat (no solvent) under N2; heated under reduced pressure (ca. 1E-2 Torr); |
diisopropoxy-bis(N,N-diethylamine-N-carbodithioato)titanium(IV)
A
titanium(IV) isopropylate
B
isopropoxy-tris(N'-methylpiperidine-N-carbodithioato)titanium(IV)
Conditions | Yield |
---|---|
In chloroform-d1 identified by NMR; |
titanium(IV) isopropylate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: neat (no solvent) 2: dichloromethane 3: neat (no solvent) View Scheme | |
Multi-step reaction with 3 steps 1: neat (no solvent) 2: dichloromethane 3: neat (no solvent) View Scheme |
Conditions | Yield |
---|---|
With ethylenediamine In methanol |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 2h; | 100% |
titanium(IV) isopropylate
(S)-[1,1']-binaphthalenyl-2,2'-diol
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 18 - 25℃; for 1h; | 100% |
In dichloromethane at 20℃; for 1h; Molecular sieve; | 100% |
Conditions | Yield |
---|---|
In neat (no solvent) High Pressure; for 1 d at 200°C; XRD; | 100% |
Conditions | Yield |
---|---|
In gas byproducts: CH3CHCH2; decomposition at a pressure of ca. 0.01 mm of Hg at 700°C; org. compounds collected in a liquid-N2 trap; NMR; GC; mass spectra; | A n/a B 100% |
Conditions | Yield |
---|---|
In methanol N2-atmosphere; stirring (1 h); washing (hexanes), drying (vac.); | 100% |
In methanol under N2 atm. titanium(IV) isopropoxide was added to excess methanol and resulting slurry was stirred for 4 h; solvent was removed under vac., product was purified by recrystn. from hot methanol; | 96% |
titanium(IV) isopropylate
9-(Me3Si)fluorenyl-Si(OH)3
Conditions | Yield |
---|---|
With water In hexane under Ar atm. at room temp. Ti(OiPr)4 in hexane was added dropwise to suspn. 9-(Me3Si)Fluorenyl-Si(OH)3 and water in hexane, stirred for 15 h; volatiles were removed in vacuo, residue was dried in vacuo and recrystd. from hexane at -30°C; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In dichloromethane soln. of Ti-complex in CH2Cl2 was added to soln. of 4-t-butylphenol in CH2Cl2, ligand in CH2Cl2 was added, stirred for 10 min at room temp. under N2; concd. in vacuo, dried in vacuo with gentle heating for 3 h; | 100% |
titanium(IV) isopropylate
HOC(CF3)2CH2N(CH3)(CH2)2N(CH3)CH2C(CF3)2OH
Conditions | Yield |
---|---|
In toluene byproducts: i-PrOH; under Ar; soln. of ligand (1 equiv.) in toluene (-30°C) added dropwise over 5 min under stirring to soln. of Ti compd. in toluene (-30°C); warmed slowly to room temp. over 12 h under stirring; volatiles removed under vac.; washed with pentane; dried in vac.; elem. anal.; | 100% |
C6H4(NHCH2C6H2Cl2(OH))2
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In diethyl ether under N2, etheral soln. of ligand added to etheral soln. of metal compd.(1:1) at -30°C, warmed to room temp., stirred for 1 h; elem. anal.; | 100% |
C6H4(NHCH2C6H2(C(CH3)3)2(OH))2
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In diethyl ether under N2, etheral soln. of ligand added to etheral soln. of metal compd.(1:1) at -30°C, warmed to room temp., stirred for 1 h; recrystd. (pentane), elem. anal.; | 100% |
titanium(IV) isopropylate
HOC(CF3)2CH2N(CH3)(CH2)3N(CH3)CH2C(CF3)2OH
Conditions | Yield |
---|---|
In toluene byproducts: i-PrOH; under Ar; soln. of ligand (1 equiv.) in toluene (-30°C) added dropwise over 5 min under stirring to soln. of Ti compd. in toluene (-30°C); warmed slowly to room temp. over 12 h under stirring; volatiles removed under vac.; washed with pentane; dried in vac.; elem. anal.; | 100% |
titanium(IV) isopropylate
Conditions | Yield |
---|---|
In chloroform byproducts: propan-2-ol; under Ar; Ti(Oi-Pr)4 (3.8 mmol) added dropwise to soln. of dialkanolamine (3.8 mmol) in CHCl3 under stirring; mixt. refluxed for 7 h; oily mixt. of diastereomers obtained; | 100% |
Conditions | Yield |
---|---|
at 180℃; for 48h; Autoclave; | 100% |
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
titanium(IV) isopropylate
γ-diphenylphosphinopropyl alcohol
C36H46O4P2Ti
Conditions | Yield |
---|---|
In cyclohexane Inert atmosphere; Reflux; | 100% |
In cyclohexane for 0.5h; Schlenk technique; Inert atmosphere; Reflux; | 100% |
titanium(IV) isopropylate
methyl 2-oxo-2-phenylacetate
isopropyl benzoylformate
Conditions | Yield |
---|---|
In toluene at 0 - 20℃; Inert atmosphere; | 100% |
titanium(IV) isopropylate
N,N′-(1,1′-dithiobis(phenylene))bis(salicylideneimine)
[((SC6H4NCHC6H4O)2)Ti(OCH(CH3)2)2]
Conditions | Yield |
---|---|
In chloroform Sonication; (Ar); suspn. of ligand (1 equiv.) in CHCl3 was stirred for 1 min; Ti compd. (1 equiv.) was added; stirred for few sec; sonicated at room temp. for 10 min; evapd. (vac.); elem. anal.; | 100% |
titanium(IV) isopropylate
phthalic anhydride
isopropyl alcohol
Ti2(OiPr)6(μ2-OOCC6H4COOiPr)(η1-OOCC6H4COOiPr)(iPrOH)
Conditions | Yield |
---|---|
In neat (no solvent) Ti(OiPr)4 (3.8 mmol) added to suspn. of phthalic anhydride (3.8 mmol) iniPrOH under Ar, mixt. heated until clear soln. obtained, crystals obtai ned at room temp. within 24 h; detd. by 1H NMR, 13C NMR, IR, XRD; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; | 100% |
titanium(IV) isopropylate
C30H20Cl8N2O4Ti
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
at 20℃; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 16h; Reflux; | 100% |
titanium(IV) isopropylate
L-enterobactin
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 100% |
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