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di-isopropyl ether
n-pentylsodium
A
sodium isopropylate
B
allyl sodium
Conditions | Yield |
---|---|
With pentane |
di-isopropyl ether
n-pentylsodium
pentane
A
sodium isopropylate
B
allyl sodium
Conditions | Yield |
---|---|
In isopropyl alcohol at 15 - 35℃; Kinetics; | |
In isopropyl alcohol at 25℃; Equilibrium constant; Thermodynamic data; ΔH(excit.), ΔS(excit.); |
Conditions | Yield |
---|---|
In isopropyl alcohol at 25℃; Equilibrium constant; |
A
6-Chlor-1-isopropoxy-2,4-dinitrobenzol
B
sodium isopropylate
Conditions | Yield |
---|---|
In isopropyl alcohol at 25℃; Equilibrium constant; |
A
1-Isopropoxy-6-isopropoxycarbonyl-2,4-dinitrobenzol
B
sodium isopropylate
Conditions | Yield |
---|---|
In isopropyl alcohol at 25℃; Equilibrium constant; |
A
2,4,6-trinitrophenyl isopropyl ether
B
sodium isopropylate
Conditions | Yield |
---|---|
With sodium perchlorate In isopropyl alcohol at 25℃; Equilibrium constant; |
Conditions | Yield |
---|---|
With sodium at 60 - 90℃; for 1h; Product distribution / selectivity; | |
With sodium hydride at 0℃; | |
With sodium hydride |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 20℃; for 4.25h; Reflux; Overall yield = 22.15 g; |
sodium isopropylate
[2-Chloro-1-methyl-2-phenyl-eth-(E)-ylidene]-isopropyl-amine
isopropyl N-isopropyl-3-phenylpropanimidate
Conditions | Yield |
---|---|
In isopropyl alcohol for 18h; Heating; | 100% |
sodium isopropylate
2-Chloro-3-(4,4-dimethyl-2-oxazolinyl)pyridine
3-(4,4-Dimethyl-2-oxazolinyl)-2-isopropyloxypyridine
Conditions | Yield |
---|---|
In tetrahydrofuran; isopropyl alcohol for 5h; Heating; | 100% |
Conditions | Yield |
---|---|
In isopropyl alcohol for 12h; Heating; | 100% |
sodium isopropylate
6-isopropyloxy-4,5-diphenyl-6H-1,2-thiazine
Conditions | Yield |
---|---|
In isopropyl alcohol at 0℃; | 100% |
methyl 3,7,12-triacetoxycholan-24-oate
sodium isopropylate
isopropyl 3α-hydroxy,7α,12α-diacetoxy-5β-cholan-24-oate
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; for 0.333333h; | 100% |
In isopropyl alcohol at 20℃; for 0.333333h; |
Conditions | Yield |
---|---|
In isopropyl alcohol at 0 - 20℃; | 100% |
sodium isopropylate
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; | 99% |
3-chloro-4-nitropyridine N-oxide
sodium isopropylate
Conditions | Yield |
---|---|
With isopropyl alcohol at 20 - 30℃; for 1h; | 98.8% |
sodium isopropylate
[6-Hydroxy-2,7,8-trimethyl-2-(4,8,12-trimethyltridecyl)chroman-5-yl]methyl bromide
Conditions | Yield |
---|---|
In ethanol; hexane; isopropyl alcohol at 0℃; for 1h; | 98% |
4-chloro-1,6-dimethyl-1H-pyrazolo[4,3-c]pyridin-3-amine
sodium isopropylate
isopropyl alcohol
4-isopropoxy-1,6-dimethyl-1H-pyrazolo[4,3-c]pyridin-3-amine
Conditions | Yield |
---|---|
for 18h; Reflux; | 98% |
sodium isopropylate
Conditions | Yield |
---|---|
In isopropyl alcohol at 60℃; for 4h; | 98% |
Conditions | Yield |
---|---|
96% |
2,4-dichloro-5-bromopyrimidine
sodium isopropylate
Conditions | Yield |
---|---|
In tetrahydrofuran; isopropyl alcohol at -20℃; for 1h; Inert atmosphere; | 96% |
75% |
sodium isopropylate
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; | 96% |
Conditions | Yield |
---|---|
to a soln. of Al-compd. a soln. of Na-i-PrO is added, mixt. is refluxed for 12 h, then allowed to cool to room temp. (N2); ppt. is filtered off, the filtrate is evapd. under vac. and cooled to 0°C, from this viscous soln. crystals are grown, elem. anal.; | 96% |
In isopropyl alcohol crystn. on mixing Al- and Na- compd. solns., alcohol excess decantation off; elem. anal.; X-ray diffraction; |
sodium isopropylate
Conditions | Yield |
---|---|
In dichloromethane; isopropyl alcohol a suspension of Pt-complex in THF was treated with sodium propane-2-oxide in propan-2-ol, stirred for 5 min, a further portion of sodium propane-2-oxide was added, warmed, stood for 2 h; evapd., H2O was added, recrystd. from CH2Cl2-EtOH; elem. anal.; | 96% |
sodium isopropylate
Dichlorophenylphosphine
di(isopropyl) phenylphosphonite
Conditions | Yield |
---|---|
In 1,4-dioxane at 10 - 50℃; for 5h; Temperature; Solvent; Concentration; Inert atmosphere; | 95.9% |
sodium isopropylate
2-bromo-6-(iodomethyl)pyridine
2-bromo-6-(isopropoxymethyl)pyridine
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; | 95% |
Conditions | Yield |
---|---|
In ethanol byproducts: NaCl; vacuum., mixing of alcoholic VOCl2 and soln. of NaO(i-Pr) in EtOH, room temp.; removal of pptd. NaCl (freezing, liquid N2), evapn. (ca. 40°C); elem. anal.; | 95% |
Conditions | Yield |
---|---|
In hexane; isopropyl alcohol; toluene To a soln. of (i-PrO)3VO in hexane a soln. of i-PrONa in a toluene/isopropyl alcohol mixt. was added under Ar.; Solvent was completely removed under vac., elem. anal.; | 95% |
Conditions | Yield |
---|---|
With calcium chloride In tetrahydrofuran byproducts: NaCl; under N2, soln. of Ca(AlH4)2 in THF added slowly to stirred suspn. of CaCl2, NaOC3H7 and Al(OC3H7)3 in THF, stirred and refluxed for 18 h; filtered, evapd. in vac., dried (2 h, room temp., 1E-2 Torr); elem. anal.; | 95% |
trans-(carbonyl)chlorobis[(phenylethynyl)di-t-butylphosphine]rhodium(I)
sodium isopropylate
carbonyl[2-(di-t-butylphosphino)-1-phenylethyleneoxo-OP][(phenylethynyl)di-t-butylphosphine]rhodium(I)
Conditions | Yield |
---|---|
In isopropyl alcohol refluxing Rh-complex with slight lack of i-PrONa (16 h); evapn., treatment of oil with H2O, filtration; elem. anal.; | 95% |
(η6-fluorobenzene)tricarbonylchromium
sodium isopropylate
isopropoxybenzene tricarbonyl chromium
Conditions | Yield |
---|---|
In dimethyl sulfoxide | 94.76% |
In dimethyl sulfoxide | 94.76% |
sodium isopropylate
2,6-diallyltetrahydropyran
5-ethoxy-4-isopropyloxymethyl-exo-10-oxatricyclo<5.2.1.02,6>deca-4,8-dien-3-one
Conditions | Yield |
---|---|
In isopropyl alcohol for 0.5h; Heating; | 94% |
sodium isopropylate
Conditions | Yield |
---|---|
With {nido-7,8-Me2C2B9H10}K In isopropyl alcohol under argon atmosphere, addn. of B-compd. to suspn. of i-PrONa (prepd. from dispersn. of NaH in nujol and i-PrOH), stirring (1 h, room temp.), addn. of Rh-compd., stirring (0.5 h), evapn. (vac.) addn. of acidified ether; sepn. of etheral layer, washing ether exts. with H2O, drying, evapn., chromy. (silica gel, ether), recrystn. (CH2Cl2/ether); | 94% |
Conditions | Yield |
---|---|
With tetrahydrofuran; calcium chloride In tetrahydrofuran; toluene byproducts: NaCl; under N2, soln. of Al(O-i-Pr)3 in toluene added slowly to stirred suspn. of NaAlH4, CaCl2 and NaO-i-Pr in toluene and THF, heated at 60°C and stirred for 5.5 h; filtered, evapd. in vac., dried (2 h, room temp., 1E-2 Torr); elem. anal.; | 94% |
With tetrahydrofuran; calcium chloride In tetrahydrofuran byproducts: NaCl; under N2, soln. of Al(O-i-Pr)3 in t-BuOMe added slowly to stirred suspn. of NaAlH4, CaCl2 and NaO-i-Pr in t-BuOMe and THF, heated at reflux andstirred for 4.5 h; filtered, evapd. in vac., dried (2 h, room temp., 1E-2 Torr); elem. anal.; | 92% |
trans-(carbonyl)chlorobis[(phenylethynyl)di-t-butylphosphine]iridium(I)
sodium isopropylate
carbonyl[2-(di-t-butylphosphino)-1-phenylethyleneoxo-OP][(phenylethynyl)di-t-butylphosphine]iridium(I)
Conditions | Yield |
---|---|
In isopropyl alcohol refluxing Ir-complex with slight lack of i-PrONa (16 h); evapn., treatment with H2O; elem. anal.; | 94% |
carbon monoxide
4-iodo-biphenyl
sodium isopropylate
4-phenylbenzoic acid isopropyl ester
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; isopropyl alcohol at 80℃; under 7600.51 Torr; for 24h; Autoclave; | 94% |
Conditions | Yield |
---|---|
In tetrahydrofuran; benzene at 20℃; for 1h; | 94% |
sodium isopropylate
2-fluoro-5-phenyl-3-trifluoromethylthiophene
Conditions | Yield |
---|---|
In 1,4-dioxane for 1h; | 93% |
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