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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiry(1S)-3-(Methylamino)-1-phenylpropan-1-ol Application:Organic Chemicals
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inquiry(S)-3-hydroxy-N-methyl-3-phenylpropanamide
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether | 98% |
With lithium aluminium tetrahydride In tetrahydrofuran for 2h; Heating; | 97.6% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 25℃; | 90% |
With lithium aluminium tetrahydride In tetrahydrofuran for 6h; Reflux; | 89% |
(1S) 3-phenyl-3-hydroxypropyl methanesulfonate
methylamine
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 65℃; for 3h; | 96% |
In tetrahydrofuran; water at 70℃; | 93% |
In tetrahydrofuran; water at 70℃; for 4h; | 90% |
In tetrahydrofuran; water at 60 - 65℃; for 4h; | 82% |
β-Methylaminoethyl phenyl ketone hydrochloride
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With Rh[((S,S)-BenzP*)(cod)]SbF6; hydrogen; caesium carbonate; zinc(II) chloride In methanol at 20℃; under 19001.3 Torr; for 20h; Autoclave; enantioselective reaction; | 92% |
With hydrogen; potassium carbonate; [Rh{(SC,RP)-duanphos}(norbornadiene)]SbF6 In methanol at 20℃; under 7500.6 Torr; for 12h; | 90% |
With [Rh((S,S)-BenzP*)(cod)]SbF6; hydrogen; magnesium sulfate; potassium carbonate In ethyl acetate at 50℃; under 37503.8 Torr; for 1h; enantioselective reaction; | 80% |
3-(N-methylamino)propiophenone
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine) In acetonitrile at 20℃; for 5h; Solvent; Reagent/catalyst; | 89.93% |
(S)-N-(ethoxycarbonyl)-3-amino-1-phenyl-1-propanol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 1h; Heating; | 88% |
(S)-(-)-3-iodo-1-phenyl-1-propanol
methylamine
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
In tetrahydrofuran; water Ambient temperature; | 86% |
In tetrahydrofuran Ambient temperature; | 85% |
In tetrahydrofuran; water for 22h; |
(S)-(-)-N-(tert-butoxycarbonyl)-3-amino-1-phenylpropan-1-ol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 5.5h; Heating; | 78% |
3-chloro-1-phenylpropanol
methylamine
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With potassium iodide In methanol; water at 80℃; for 8h; | 75% |
With sodium iodide In water |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; water at 90℃; for 1.5h; | 67% |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran Heating; Yield given; | |
With lithium aluminium tetrahydride |
methylamine
3-hydroxy-3-phenylpropyl 4-methylbenzenesulfonate
A
(S)-N-methyl-3-amino-1-phenyl-1-propanol
B
(R)-N-methyl-3-phenyl-3-hydroxypropylamine
Conditions | Yield |
---|---|
Stage #1: 3-hydroxy-3-phenylpropyl 4-methylbenzenesulfonate With 3 A molecular sieve; oxygen; (-)-sparteine; palladium diacetate In toluene at 80℃; under 760 Torr; for 36h; Stage #2: methylamine With water In tetrahydrofuran at 65℃; |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 8h; Heating; | 4.10 g |
ethyl (3R)-3-hydroxy-3-phenylpropionate
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 70 percent / tetrahydrofuran; H2O / 70 °C 2: 90 percent / LiAlH4 / tetrahydrofuran / 0 - 25 °C View Scheme | |
Multi-step reaction with 4 steps 1: 80 percent / LiAlH4 / diethyl ether / Ambient temperature 2: 85 percent / Et3N / diethyl ether / 2 h / 0 °C 3: 90 percent / NaI / acetone / Heating 4: 86 percent / tetrahydrofuran; H2O / Ambient temperature View Scheme | |
Multi-step reaction with 3 steps 1: 80 percent / LiAlH4 / diethyl ether / Ambient temperature 2: 85 percent / Et3N / diethyl ether / 2 h / 0 °C 3: 90 percent / tetrahydrofuran; H2O / 4 h / 70 °C View Scheme |
(S)-3-hydroxy-3-phenylpropanenitrile
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 92 percent / borane-dimethyl sulfide complex / tetrahydrofuran / 4 h / 70 °C 2: aq. K2CO3 / CH2Cl2 / 0.5 h / 20 °C 3: 4.10 g / LiAlH4 / tetrahydrofuran / 8 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 85 percent / BH3*SMe2 / tetrahydrofuran / 2 h / Heating 2: 90 percent / K2CO3 / CH2Cl2; H2O / 0.58 h / 20 °C 3: 88 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: BH3*SMe2 / tetrahydrofuran / 2.5 h / Heating 3: LAH View Scheme |
(1S)-3-amino-1-phenyl-1-propanol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. K2CO3 / CH2Cl2 / 0.5 h / 20 °C 2: 4.10 g / LiAlH4 / tetrahydrofuran / 8 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 90 percent / K2CO3 / CH2Cl2; H2O / 0.58 h / 20 °C 2: 88 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme | |
Multi-step reaction with 2 steps 2: LAH View Scheme | |
Multi-step reaction with 2 steps 1: NaHCO3 2: LiAlH4 / tetrahydrofuran / Heating View Scheme |
acetophenone
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: HCl / ethanol / 110 °C 2: 90 percent / hydrogen; K2CO3 / [Rh{(SC,RP)-duanphos}(norbornadiene)]SbF6 / methanol / 12 h / 20 °C / 7500.6 Torr View Scheme | |
Multi-step reaction with 2 steps 1: toluene-4-sulfonic acid / ethanol / 20 h / 110 °C 2: Rh[((S,S)-BenzP*)(cod)]SbF6; zinc(II) chloride; caesium carbonate; hydrogen / methanol / 20 h / 20 °C / 19001.3 Torr / Autoclave View Scheme |
butyric acid 2-ethoxycarbonyl-1-phenyl-ethyl ester
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Candida rugosa lipase; MgCl2 / H2O; diisopropyl ether / 24 h / 30 °C 2: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / 20 °C 3: 85 percent / Et3N / diethyl ether / 3 h / -10 - 0 °C / cooling 4: 82 percent / tetrahydrofuran; H2O / 4 h / 60 - 65 °C View Scheme |
(3S) ethyl β-butyryloxy-β-phenyl propionate
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / 20 °C 2: 85 percent / Et3N / diethyl ether / 3 h / -10 - 0 °C / cooling 3: 82 percent / tetrahydrofuran; H2O / 4 h / 60 - 65 °C View Scheme |
Ethyl 3-hydroxy-3-phenylpropanoate
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: DCC; 4-(dimethylamino)pyridine / CH2Cl2 / 20 °C 2: Candida rugosa lipase; MgCl2 / H2O; diisopropyl ether / 24 h / 30 °C 3: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / 20 °C 4: 85 percent / Et3N / diethyl ether / 3 h / -10 - 0 °C / cooling 5: 82 percent / tetrahydrofuran; H2O / 4 h / 60 - 65 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: 85 percent / lithium aluminum hydride / tetrahydrofuran / 2 h 2.1: 95 percent / Et3N / CH2Cl2 / 0 h / -10 °C 3.1: O2; (-)-sparteine; 3 Angstroem sieves / Pd(OAc)2 / toluene / 36 h / 80 °C / 760 Torr 3.2: H2O / tetrahydrofuran / 65 °C View Scheme |
(S)-3-phenyl-1,3-propanediol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / Et3N / diethyl ether / 3 h / -10 - 0 °C / cooling 2: 82 percent / tetrahydrofuran; H2O / 4 h / 60 - 65 °C View Scheme | |
Multi-step reaction with 3 steps 1: 85 percent / Et3N / diethyl ether / 2 h / 0 °C 2: 90 percent / NaI / acetone / Heating 3: 86 percent / tetrahydrofuran; H2O / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: 85 percent / Et3N / diethyl ether / 2 h / 0 °C 2: 90 percent / tetrahydrofuran; H2O / 4 h / 70 °C View Scheme |
benzaldehyde
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: LDA / tetrahydrofuran; hexane / 1 h / -78 °C 1.2: tetrahydrofuran; hexane / 1 h / -78 °C 2.1: DCC; 4-(dimethylamino)pyridine / CH2Cl2 / 20 °C 3.1: Candida rugosa lipase; MgCl2 / H2O; diisopropyl ether / 24 h / 30 °C 4.1: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / 20 °C 5.1: 85 percent / Et3N / diethyl ether / 3 h / -10 - 0 °C / cooling 6.1: 82 percent / tetrahydrofuran; H2O / 4 h / 60 - 65 °C View Scheme |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenyl silane / tris(triphenylphosphine)rhodium(I) carbonyl hydride / tetrahydrofuran / 15 h / 20 °C 2: 67 percent / HCl / methanol; H2O / 1.5 h / 90 °C View Scheme |
3-hydroxy-3-phenylpropanenitrile
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: LiAlH4 / tetrahydrofuran / 5 h / Heating 2: 41 percent / Et3N / CH2Cl2 / 2 h / 23 °C 3: (-)-sparteine; O2; Molecular sieves 3A / Pd(nbd)Cl2 / toluene / 24 h / 80 °C / 760.05 Torr 4: 78 percent / LiAlH4 / tetrahydrofuran / 5.5 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen, NH3 / Raney Ni / ethanol / 90 °C / p(NH3) = 30 psi and p(H2) = 170 psi 2: NaHCO3 3: LiAlH4 / tetrahydrofuran / Heating View Scheme |
3-amino-1-phenylpropan-1-ol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 41 percent / Et3N / CH2Cl2 / 2 h / 23 °C 2: (-)-sparteine; O2; Molecular sieves 3A / Pd(nbd)Cl2 / toluene / 24 h / 80 °C / 760.05 Torr 3: 78 percent / LiAlH4 / tetrahydrofuran / 5.5 h / Heating View Scheme |
(3-oxo-3-phenylpropyl)carbamic acid tert-butyl ester
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 100 percent / NaBH4 / ethanol / 3 h / 0 - 23 °C 2: (-)-sparteine; O2; Molecular sieves 3A / Pd(nbd)Cl2 / toluene / 24 h / 80 °C / 760.05 Torr 3: 78 percent / LiAlH4 / tetrahydrofuran / 5.5 h / Heating View Scheme |
(+/-)-N-(tert-butoxycarbonyl)-3-amino-1-phenylpropan-1-ol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (-)-sparteine; O2; Molecular sieves 3A / Pd(nbd)Cl2 / toluene / 24 h / 80 °C / 760.05 Torr 2: 78 percent / LiAlH4 / tetrahydrofuran / 5.5 h / Heating View Scheme |
1-phenyl-1,3-propanediol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 95 percent / Et3N / CH2Cl2 / 0 h / -10 °C 2.1: O2; (-)-sparteine; 3 Angstroem sieves / Pd(OAc)2 / toluene / 36 h / 80 °C / 760 Torr 2.2: H2O / tetrahydrofuran / 65 °C View Scheme |
(R)-Styrene oxide
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 85.2 percent / Et3N / tetrahydrofuran / 18 h / Heating 2: BH3*SMe2 / tetrahydrofuran / 2.5 h / Heating 4: LAH View Scheme |
3-chloro-1-phenylpropanol
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 100 percent / NaI / acetone / Heating 2: 85 percent / tetrahydrofuran / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: sodium iodide / acetone / 17 h / Reflux 2: water; tetrahydrofuran / 22 h View Scheme |
hydrogenchloride
(S)-N-methyl-3-amino-1-phenyl-1-propanol
(-)-N-tert-butoxycarbonyl-N-methyl-3-phenyl-3-hydroxypropylamine
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; ethyl acetate | 97% |
di-tert-butyl dicarbonate
(S)-N-methyl-3-amino-1-phenyl-1-propanol
(-)-N-tert-butoxycarbonyl-N-methyl-3-phenyl-3-hydroxypropylamine
Conditions | Yield |
---|---|
In dichloromethane | 95% |
In dichloromethane for 2h; Heating; | 95% |
In tetrahydrofuran at 0 - 20℃; | 57% |
With triethylamine In tetrahydrofuran at 0 - 20℃; for 22h; |
4-Fluorobenzotrifluoride
(S)-N-methyl-3-amino-1-phenyl-1-propanol
(S)-fluoxetine
Conditions | Yield |
---|---|
Stage #1: (S)-N-methyl-3-amino-1-phenyl-1-propanol With sodium hydride In N,N-dimethyl acetamide; paraffin oil at 90℃; for 0.5h; Inert atmosphere; Stage #2: 4-Fluorobenzotrifluoride In N,N-dimethyl acetamide; paraffin oil at 100℃; for 5h; Inert atmosphere; | 91% |
With sodium hydride 1.) dimethylacetamide, 70 deg C, 30 min; 2) dimethylacetamide, 93 deg C, 2.25 h; Yield given. Multistep reaction; |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
4-chlorobenzotrifluoride
(S)-fluoxetine hydrochloride
Conditions | Yield |
---|---|
Stage #1: (S)-N-methyl-3-amino-1-phenyl-1-propanol With sodium hydride In dimethyl sulfoxide at 70℃; for 0.5h; Stage #2: 4-chlorobenzotrifluoride In dimethyl sulfoxide at 90℃; for 2h; | 90% |
With hydrogenchloride; sodium hydride 1) DMAC 2) EtOH; Multistep reaction; | |
1) DMSO, 50 deg C, 20 min, 2) DMSO, 90 deg C, 40 min; Yield given. Multistep reaction; | |
With hydrogenchloride; N,N-dimethyl acetamide; sodium hydride Yield given; |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
4-chlorobenzotrifluoride
(S)-fluoxetine
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 90 - 100℃; for 1.5h; | 84% |
With sodium hydride In dimethyl sulfoxide at 90 - 100℃; for 1h; | 71% |
With sodium hydride 1.) N,N-dimethylacetamid (DMAC), 90 deg C, 2.) 100-105 deg C; Yield given. Multistep reaction; |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
ortho-cresol
(R)-tomoxetine
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In toluene at 120℃; for 2h; Solvent; Reagent/catalyst; Temperature; Mitsunobu Displacement; | 79.45% |
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; for 12h; | 67% |
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; Mitsunobu Displacement; |
2-Fluorotoluene
(S)-N-methyl-3-amino-1-phenyl-1-propanol
Conditions | Yield |
---|---|
With sodium hydride 1) DMSO, 2) DMSO; Yield given. Multistep reaction; |
2-methylchlorobenzene
(S)-N-methyl-3-amino-1-phenyl-1-propanol
(S)-N-methyl-3-(2-methylphenoxy)-3-phenyl-1-propanamine
Conditions | Yield |
---|---|
With 2,4-dichlorophenoxyacetic acid dimethylamine; sodium hydride Multistep reaction; |
2-Chloroanisole
(S)-N-methyl-3-amino-1-phenyl-1-propanol
(S)-N-methyl-3-(2-methoxyphenoxy)-3-phenyl-1-propanamine
Conditions | Yield |
---|---|
With 2,4-dichlorophenoxyacetic acid dimethylamine; sodium hydride Multistep reaction; |
(S)-N-methyl-3-amino-1-phenyl-1-propanol
4-chlorobenzotrifluoride
A
(R)-fluoxetine
B
(S)-fluoxetine
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl acetamide Title compound not separated from byproducts.; |
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